Physicochemical and Microstructural Characteristics of Sulfated Polysaccharide from Marine Microalga
Abstract
:1. Introduction
2. Materials and Methods
2.1. Size-Exclusion Chromatography with Multi-Angle Light Scattering
2.2. Dynamic Light Scattering (DLS) Analysis and Phase Analysis Light Scattering (PALS)
2.3. Fourier Transform Infrared (FTIR) Spectroscopy
2.4. Scanning Electron Microscopy
3. Results
3.1. Size-Exclusion Chromatography with Multi-Angle Light Scattering
3.2. Physical Properties
3.3. Fourier Transform Infrared (FTIR) Spectroscopy
3.4. Scanning Electron Microscopy (SEM)
4. Discussion
5. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Mw (kDa) | 1650 |
PI (Mw/Mn) | 1.34 |
[η] (mL/g) | 197 |
RG (nm) | 61 |
Rh (nm) | 36 |
C∞ | 4.2 |
q (nm) | 1.3 |
Mark–Houwink–Sakurada α | 0.5 |
Mark–Houwink–Sakurada K (mL/g) | 1.67 × 10−1 |
Zeta potential (ζ) (mV) | −5.80 ± 0.13 |
Electrophoretic mobility (µ) (µm cm/s V) | −0.45 ± 0.01 |
Conductivity (mS/cm) | 0.70 ± 0.01 |
Diffusion coefficient (D) (cm²/s) | 2.90 × 10−9 ± 1.90 × 10−10 |
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Fimbres-Olivarria, D.; Marquez-Escalante, J.; Martínez-Robinson, K.G.; Miranda-Arizmendi, V.; Anda-Flores, Y.D.; Rascon-Chu, A.; Brown-Bojorquez, F.; Carvajal-Millan, E. Physicochemical and Microstructural Characteristics of Sulfated Polysaccharide from Marine Microalga. Analytica 2023, 4, 527-537. https://doi.org/10.3390/analytica4040036
Fimbres-Olivarria D, Marquez-Escalante J, Martínez-Robinson KG, Miranda-Arizmendi V, Anda-Flores YD, Rascon-Chu A, Brown-Bojorquez F, Carvajal-Millan E. Physicochemical and Microstructural Characteristics of Sulfated Polysaccharide from Marine Microalga. Analytica. 2023; 4(4):527-537. https://doi.org/10.3390/analytica4040036
Chicago/Turabian StyleFimbres-Olivarria, Diana, Jorge Marquez-Escalante, Karla G. Martínez-Robinson, Valeria Miranda-Arizmendi, Yubia De Anda-Flores, Agustín Rascon-Chu, Francisco Brown-Bojorquez, and Elizabeth Carvajal-Millan. 2023. "Physicochemical and Microstructural Characteristics of Sulfated Polysaccharide from Marine Microalga" Analytica 4, no. 4: 527-537. https://doi.org/10.3390/analytica4040036