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Molecules 2012, 17(10), 11607-11615; doi:10.3390/molecules171011607

Microwave Assisted Synthesis of 2,2'-Arylene-substituted Bis(4H-3,1-Benzoxazin-4-one) Derivatives Using the Complex Cyanuric Chloride/N,N-Dimethylformamide

1
School of Chemical Science and Food Technology, Faculty of Science and Technology, University Kebangsaan Malaysia (UKM), Kuala Lumpur 43600, Malaysia
2
Department of Chemistry, Payame Noor University of Golpayegan, Isfahan 19395-4697, I. R., Iran
3
Malaysia-Japan international institute of Technology, University Technology Malaysia (UTM), Kuala Lumpur 54100, Malaysia
*
Author to whom correspondence should be addressed.
Received: 13 June 2012 / Revised: 13 September 2012 / Accepted: 24 September 2012 / Published: 28 September 2012
(This article belongs to the Section Organic Synthesis)
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Abstract

A new and efficient method has been designed to prepare 2,2'-arylene-substituted bis(4H-3,1-benzoxazin-4-one) derivatives by using the mixture of cyanuric chloride and N,N-dimethylformamide in a microwave-assisted reaction. The method used and presented here has good rate enhancement and excellent yields.
Keywords: bis(4H-3,1-benzoxazin-4-one); OLED; microwave; UV bis(4H-3,1-benzoxazin-4-one); OLED; microwave; UV
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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Shariat, M.; Samsudin, M.W.; Zakaria, Z. Microwave Assisted Synthesis of 2,2'-Arylene-substituted Bis(4H-3,1-Benzoxazin-4-one) Derivatives Using the Complex Cyanuric Chloride/N,N-Dimethylformamide. Molecules 2012, 17, 11607-11615.

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