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Volume 2006
Issue 5
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Molbank, Volume 2006, Issue 5 (September 2006) – 19 articles

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102 KiB  
Short Note
3-[(Benzylsulfonyl)methyl]aniline hydrochloride
by Daniel G. Grohmann and Bruce A. Hathaway
Molbank 2006, 2006(5), M503; https://doi.org/10.3390/M503 - 01 Sep 2006
Viewed by 3160
Abstract
In the course of our work to prepare inhibitors of the enzyme dihydrofolate reductase, we desired to prepare sulfone analogues of some similar sulfides [1, 2].[...] Full article
102 KiB  
Short Note
3-[(Phenylsulfonyl)methyl]aniline hydrochloride
by Daniel G. Grohmann and Bruce A. Hathaway
Molbank 2006, 2006(5), M502; https://doi.org/10.3390/M502 - 01 Sep 2006
Cited by 1 | Viewed by 3525
Abstract
In the course of our work to prepare inhibitors of the enzyme dihydrofolate reductase, we desired to prepare sulfone analogues of some previously reported sulfides [1, 2].[...] Full article
99 KiB  
Short Note
1-Nitro-3-[(benzylsulfonyl)methyl]benzene
by Daniel G. Grohmann and Bruce A. Hathaway
Molbank 2006, 2006(5), M501; https://doi.org/10.3390/M501 - 01 Sep 2006
Cited by 1 | Viewed by 3602
Abstract
In the course of our work to prepare inhibitors of the enzyme dihydrofolate reductase, we desired to prepare sulfone analogues of some similar sulfides [1, 2].[...] Full article
99 KiB  
Short Note
1-Nitro-3-[(phenylsulfonyl)methyl]benzene
by Daniel G. Grohmann and Bruce A. Hathaway
Molbank 2006, 2006(5), M500; https://doi.org/10.3390/M500 - 01 Sep 2006
Cited by 1 | Viewed by 3562
Abstract
In the course of our work to prepare inhibitors of the enzyme dihydrofolate reductase, we desired to prepare sulfone analogues of some previously reported sulfides [1, 2].[...] Full article
100 KiB  
Short Note
(4Z)-1-Benzyl (1,3-Dibenzyl)-4-(2-oxopropylidene)-1,3,4,5-tetrahydro-2H-1,5-benzodiazepin-2-one
by Ould Mohamed Sidya Mohamed Said, Bouhfid Rachid, Nicolas Joly, Vincent Lequart, Patrick Martin, M. Massoui and El Mokhtar Essassi
Molbank 2006, 2006(5), M499; https://doi.org/10.3390/M499 - 01 Sep 2006
Viewed by 4482
Abstract
We describe in this work the synthesis of new benzodiazepine derivatives susceptible to possess various pharmacological activities.[...] Full article
111 KiB  
Short Note
(4Z)-1-Propargyl(1,3-Dipropargyl)-4-(2-oxopropylidene)-1,3,4,5-tetrahydro-2H-1,5-benzodiazepin-2-one
by Ould Mohamed Sidya Mohamed Said, Bouhfid Rachid, Nicolas Joly, Vincent Lequart, Patrick Martin, M. Massoui and El Mokhtar Essassi
Molbank 2006, 2006(5), M498; https://doi.org/10.3390/M498 - 01 Sep 2006
Viewed by 4532
Abstract
We describe in this work the synthesis of new benzodiazepine derivatives susceptible to possess various pharmacological activities.[...] Full article
178 KiB  
Short Note
Synthesis and physical characterization of 1-(2,4-dimethoxyphenyl)-4-(4-nitrophenyl)-3-phenoxyazetidin-2-one
by A. A. Jarrahpour, A. F. Jalbout and S. Rezaei
Molbank 2006, 2006(5), M497; https://doi.org/10.3390/M497 - 01 Sep 2006
Viewed by 3156
Abstract
In this paper we propose the synthesis of 1-(2,4-dimethoxyphenyl)-4-(4-nitrophenyl)-3- phenoxyazetidin-2-one as a new monocyclic β-lactam. Its structure has been confirmed by IR, 1H-NMR, 13C-NMR and Mass spectroscopic data. In addition to its synthesis we present AM1 calculations to characterize the physical [...] Read more.
In this paper we propose the synthesis of 1-(2,4-dimethoxyphenyl)-4-(4-nitrophenyl)-3- phenoxyazetidin-2-one as a new monocyclic β-lactam. Its structure has been confirmed by IR, 1H-NMR, 13C-NMR and Mass spectroscopic data. In addition to its synthesis we present AM1 calculations to characterize the physical properties of the molecule. Full article
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86 KiB  
Short Note
3-[Benzyl-(1,5-dimethyl-1H-pyrazol-3-ylmethyl)-amino]-propionitrile
by Leila Herrag, Rachid Touzani, Abdelkrim Ramdani and Belkheir Hammouti
Molbank 2006, 2006(5), M496; https://doi.org/10.3390/M496 - 01 Sep 2006
Viewed by 3118
Abstract
The products of aza-type Michael addition, i.e., β-amino carbonyl compounds and their derivatives, are often used as peptide analogs or precursors of optically active amino acids, amino alcohols, diamines, and lactams [1].[...] Full article
87 KiB  
Short Note
3-[Benzyl-(3,5-dimethyl-pyrazol-1-ylmethyl)-amino]-propionitrile
by Leila Herrag, Rachid Touzani, Abdelkrim Ramdani and Belkheir Hammouti
Molbank 2006, 2006(5), M495; https://doi.org/10.3390/M495 - 01 Sep 2006
Viewed by 3113
Abstract
The products of aza-type Michael addition, i.e., β-amino carbonyl compounds and their derivatives, are often used as peptide analogs or precursors of optically active amino acids, amino alcohols, diamines, and lactams [1].[...] Full article
88 KiB  
Short Note
1-{[Benzyl-(2-cyano-ethyl)-amino]-methyl}-5-methyl-1H-pyrazole-3-carboxylic acid ethyl ester
by Leila Herrag, Rachid Touzani, Abdelkrim Ramdani and Belkheir Hammouti
Molbank 2006, 2006(5), M494; https://doi.org/10.3390/M494 - 01 Sep 2006
Viewed by 3038
Abstract
The products of aza-type Michael addition, i.e., β-amino carbonyl compounds and their derivatives, are often used as peptide analogs or precursors of optically active amino acids, amino alcohols, diamines, and lactams [1].[...] Full article
85 KiB  
Short Note
1-{[Benzyl-(2-cyano-ethyl)-amino]-methyl}-5-methyl-1H-pyrazole-3-carboxylic acid methyl ester
by Leila Herrag, Rachid Touzani, Abdelkrim Ramdani and Belkheir Hammouti
Molbank 2006, 2006(5), M493; https://doi.org/10.3390/M493 - 01 Sep 2006
Viewed by 3068
Abstract
The products of aza-type Michael addition, i.e., β-amino carbonyl compounds and their derivatives, are often used as peptide analogs or precursors of optically active amino acids, amino alcohols, diamines, and lactams [1].[...] Full article
92 KiB  
Short Note
Synthesis of 6,7-dimethoxy-3,4-diphenyl-2(1H)-quinazolinone from 1-(3,4-dimethoxyphenyl)-urea and benzoic acid in polyphosphoric acid
by Iliyan Ivanov
Molbank 2006, 2006(5), M492; https://doi.org/10.3390/M492 - 01 Sep 2006
Viewed by 3024
Abstract
The quinazoline skeleton, when selectively functionalized, is a building block for the preparation of numerous alkaloids and substances capable of exhibiting a wide variety of biological activity [1][...] Full article
322 KiB  
Short Note
New 1-(ethyl-ethanoate-yl)-5,5’-diisopropyl-3,3’-bipyrazole
by Ibrahim Bouabdallah, Ismail Zidane, Rachid Touzani, Abdelkrim Ramdani, Abraham F. Jalbout and B. Trzaskowski
Molbank 2006, 2006(5), M491; https://doi.org/10.3390/M491 - 01 Sep 2006
Viewed by 3999
Abstract
To a solution of 5,5’-diisopropyl-3,3’-bipyrazole 1 [1] (218 mg, 1 mmol) in DMSO (1 ml) was added solid potassium tert-butoxide (112 mg, 1 mmol) followed by addition of ethyle chloroacetate (123 mg, 1 mmol) in DMSO (1 ml) through a syringe[...] Full article
106 KiB  
Short Note
New 1-(4-nitrophenyl)-5,5’-diisopropyl-3,3’-bipyrazole
by Ibrahim Bouabdallah, Ismail Zidane, Rachid Touzani, Abdelkrim Ramdani, Abraham F. Jalbout and B. Trzaskowski
Molbank 2006, 2006(5), M490; https://doi.org/10.3390/M490 - 01 Sep 2006
Viewed by 4301
Abstract
To a solution of 5,5’-diisopropyl-3,3’-bipyrazole 1 [1] (109 mg, 0.5 mmol) in DMSO (2 ml) was added solid potassium tert-butoxide (61 mg, 0.5 mmol) followed by addition of 4-fluoronitrobenzene (70.5 mg, 0.5 mmol) in DMSO (1 ml) through a syringe, according to literature [...] Read more.
To a solution of 5,5’-diisopropyl-3,3’-bipyrazole 1 [1] (109 mg, 0.5 mmol) in DMSO (2 ml) was added solid potassium tert-butoxide (61 mg, 0.5 mmol) followed by addition of 4-fluoronitrobenzene (70.5 mg, 0.5 mmol) in DMSO (1 ml) through a syringe, according to literature procedure [2].[...] Full article
137 KiB  
Short Note
Synthesis, Physical Characterization, Antibacterial and Antifungal Activities of 2-((E)-1-(2-((E)-1-(2-Hydroxyphenyl)ethylideneamino) phenylamino) ethyl) phenol
by A. A. Jarrahpour, A. F. Jalbout, J. M. Brunel, C. Loncle, S. Rezaei and B. Trzaskowski Trzaskowski
Molbank 2006, 2006(5), M489; https://doi.org/10.3390/M489 - 01 Sep 2006
Viewed by 4120
Abstract
In this paper we report the synthesis of 2-((E)-1-(2-((E)-1-(2-hydroxyphenyethylideneamino) phenylamino) ethyl) phenol.In addition to its synthesis we present AM1 and B3LYP/6-31G* calculations to characterize the physical properties of this molecule. Finally, the antifungal and antibacterial activities of this derivative have been evaluated. Full article
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Figure 1

66 KiB  
Short Note
Synthesis of 4-[4-(4-nitrobenzylideneiminophenylene)phenyleneimino methylidene] phenol
by L. Marin and V. Cozan
Molbank 2006, 2006(5), M488; https://doi.org/10.3390/M488 - 01 Sep 2006
Viewed by 3313
Abstract
The azomethine 1 was prepared as described elsewhere [1].[...] Full article
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Figure 1

84 KiB  
Short Note
2-[N-(O-ethylaminophenyl) phenyl imidoyl methylylidene]-3,5-diphenyl-1,3,4-thiadiazole
by J. Nathantene Ghomsi, M. Lamine Doumbia, Noureddine Hamou Ahabchane and El Mokhtar Essassi
Molbank 2006, 2006(5), M487; https://doi.org/10.3390/M487 - 01 Sep 2006
Viewed by 3442
Abstract
4-phenyl-1,5-benzodiazepine-2-thione are used as starting materials in the synthesis of several heterocyclic compounds for potential biological actvities.[...] Full article
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Scheme 1

120 KiB  
Short Note
Synthesis of 6-chloro-2-(propargyloxy)quinoline-4-carboxylic acid and propargyl 6-chloro-2-(propargyloxy)quinoline-4-carboxylate
by R. Bouhfid and E.M. Essassi
Molbank 2006, 2006(5), M486; https://doi.org/10.3390/M486 - 01 Sep 2006
Cited by 1 | Viewed by 3277
Abstract
The quinoline ring systems are important structural units in naturally occurring alkaloids and synthetic analogues with interesting biological activities.[...] Full article
105 KiB  
Short Note
Synthesis of 6-chloro-2-oxo-1,2-dihydroquinoline-4-carbohydrazide
by R. Bouhfid and E.M. Essassi
Molbank 2006, 2006(5), M485; https://doi.org/10.3390/M485 - 01 Sep 2006
Viewed by 3065
Abstract
In previous works we have shown that hydrazides are highly useful starting materials and intermediates in the synthesis of several heterocyclic compounds1-3 of potential biological activities.[...] Full article
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