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Molbank 2012, 2012(4), M782; doi:10.3390/M782
Short Note

3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

 and *
Department of Chemistry, University of Cyprus, P.O. Box 20537, 1678 Nicosia, Cyprus
* Author to whom correspondence should be addressed.
Received: 24 September 2012 / Accepted: 12 October 2012 / Published: 16 October 2012
Download PDF [117 KB, 7 November 2012; original version 16 October 2012]   |  

Abstract

3-Chloro-5-trifluoromethanesulfonate-4H-1,2,6-thiadiazin-4-one 3 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 5 (1 equiv.) in the presence of Pd(Ph3P)2Cl2 (5 mol%) in benzene at ca. 20 °C for 5 h to give 3-chloro-5-(4-dodecylthien-2-yl)-1,2,6-thiadiazinone 6 in 87% yield.
Keywords: 1,2,6-thiadiazines; thiophenes; heterocycles; oligomers 1,2,6-thiadiazines; thiophenes; heterocycles; oligomers
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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Ioannidou, H.A.; Koutentis, P.A. 3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one. Molbank 2012, 2012, M782.

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