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ChemEngineering, Volume 7, Issue 5

2023 October - 27 articles

Cover Story: Ceritinib, an active ingredient in the treatment of lung cancer, was formed as a result of pH modification during the cooling crystallization of a ceritinib dihydrochloride solution. By carrying out processes in various solvent systems, several polymorphs were produced. A combination of forms B and C was generated in an ethanol–water system, resulting in smaller crystals. The acetone–water system produced pure form A, which has larger crystals and is more applicable for forthcoming studies. To additionally enhance granulometric properties, ceritinib form A was recrystallized in tetrahydrofuran at different temperatures using antisolvent crystallization. Crystallization at a higher saturation temperature results in larger and more compact crystals, which enhances filtration and drying. View this paper
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Articles (27)

  • Article
  • Open Access
3 Citations
3,061 Views
15 Pages

Numerical Analysis of Gas Hold-Up of Two-Phase Ebullated Bed Reactor

  • Riyadh S. Almukhtar,
  • Ali Amer Yahya,
  • Omar S. Mahdy,
  • Hasan Shakir Majdi,
  • Gaidaa S. Mahdi,
  • Asawer A. Alwasiti,
  • Zainab Y. Shnain,
  • Majid Mohammadi,
  • Adnan A. AbdulRazak and
  • Sajda S. Alsaedi
  • + 3 authors

Due to the significant increase in heavy feedstocks being transported to refineries and the hydrocracking process, the significance of adopting an ebullated bed reactor has been reemphasized in recent years. The predictive modelling of gas hold-up in...

  • Article
  • Open Access
6 Citations
3,948 Views
31 Pages

Adaptive Mesh Refinement Strategies for Cost-Effective Eddy-Resolving Transient Simulations of Spray Dryers

  • Jairo Andrés Gutiérrez Suárez,
  • Carlos Humberto Galeano Urueña and
  • Alexánder Gómez Mejía

The use of adaptive meshing strategies to perform cost-effective transient simulations of spray drying processes is evaluated. These simulations are often computationally expensive, given the large differences between the characteristic times of the...

  • Article
  • Open Access
5 Citations
2,879 Views
17 Pages

The focus of this study was to examine antisolvent effects, which hold significance in particulate processes, such as crystallization and precipitation. In the first section, an experimental investigation revealed that C1–C4 primary alcohols si...

  • Article
  • Open Access
20 Citations
8,459 Views
12 Pages

Medical sutures are important surgical aids for promoting wound closure and establishing the ideal environment for wound healing. Several key factors must be considered in medical sutures, including the material of choice for the wound closure, the t...

  • Article
  • Open Access
23 Citations
5,583 Views
27 Pages

Role of Stearic Acid as the Crystal Habit Modifier in Candelilla Wax-Groundnut Oil Oleogels

  • Diksha Chaturvedi,
  • Deepti Bharti,
  • Somali Dhal,
  • Deblu Sahu,
  • Haladhar Behera,
  • Minaketan Sahoo,
  • Doman Kim,
  • Maciej Jarzębski,
  • Arfat Anis and
  • Kunal Pal
  • + 2 authors

This study investigated the effects of incorporating stearic acid (SAC) in candelilla wax (CW) and groundnut oil (GO) oleogel with potential health benefits as an alternative to saturated fats in processed foods. Results showed that SAC possesses cry...

  • Review
  • Open Access
2 Citations
2,710 Views
15 Pages

Energy-Intensive Materials with Mechanically Activated Components

  • Bakkara Ayagoz,
  • Sadykov Bakhtiyar,
  • Artykbaeva Aida,
  • Kamunur Kaster,
  • Batkal Aisulu and
  • Kalmuratova Bakhyt

The production and study of highly dispersed aluminum-based powders represents one of contemporary science’s priority fields. This is primarily driven by the practical necessity to develop new materials, a feat that, in some cases, can only be...

  • Article
  • Open Access
3 Citations
2,244 Views
13 Pages

Synthesis and Research of Critical Parameters of Bi-HTSC Ceramics Based on Glass Phase Obtained by IR Heating

  • Daniyar Uskenbaev,
  • Adolf Nogai,
  • Alisher Uskenbayev,
  • Kairatbek Zhetpisbayev,
  • Eleonora Nogai,
  • Pavel Dunayev,
  • Ainur Zhetpisbayeva and
  • Artur Nogai

In this paper influence of the excess Ca and Cu cations on the critical temperature (Tc) and critical transport current density (Jc) of high-temperature superconducting ceramics of the compositions (HTSC) Bi1.6Pb0.4Sr2Ca2.1Cu3.1Oy, Bi1.6Pb0.4Sr2Ca2.2...

  • Article
  • Open Access
7 Citations
6,101 Views
18 Pages

Chemical Composition of Different Extracts from Echinacea purpurea (L.) Moench Roots and Evaluation of Their Antimicrobial Activity

  • Nadezhda Petkova,
  • Ani Petrova,
  • Ivan Ivanov,
  • Ivanka Hambarlyiska,
  • Yulian Tumbarski,
  • Ivayla Dincheva,
  • Manol Ognyanov and
  • Petko Denev

This research aimed to reveal the chemical composition of different fractions obtained by sequential extraction of purple coneflower (Echinacea purpurea) roots and to evaluate the antimicrobial activity of some of them. Hexane, chloroform, ethyl acet...

  • Article
  • Open Access
4 Citations
3,088 Views
21 Pages

Natural gas liquids are a by-product of natural gas preparation, one of the most common and environmentally friendly energy sources. In natural gas fields located in remote areas, there is no resource-efficient way to use natural gas liquids. However...

  • Article
  • Open Access
23 Citations
4,336 Views
20 Pages

Investigating the Effect of Thermal Annealing and Changing the Concentration of GO in GO/PVA Nanocomposites on Their Structural, Electrical, and Optical Properties

  • Lala Gahramanli,
  • Mustafa Muradov,
  • Goncha Eyvazova,
  • Mahammad Baghir Baghirov,
  • Sevinj Mammadyarova,
  • Gunel Aliyeva,
  • Elman Hajiyev,
  • Faig Mammadov and
  • Stefano Bellucci

The present research involves producing graphene oxide (GO) using the Hummers method, generating a composite using GO and PVA, and analyzing these composites’ structural and optical characteristics. PVA and GO were used in varied percentages to...

  • Article
  • Open Access
3 Citations
3,244 Views
15 Pages

Electrokinetic Forces as an Electrical Measure of Chemical Aging Potential in Granular Materials

  • Miguel Castilla-Barbosa,
  • Orlando Rincón-Arango and
  • Manuel Ocampo-Terreros

The zeta potential of soils is an electric potential in the double-layer interface and is a physical property exhibited by any particle related to electrochemical attractive forces. On the other hand, the chemical aging phenomenon is seen as the chie...

  • Article
  • Open Access
3 Citations
2,419 Views
18 Pages

A Phytochemical Approach to the Removal of Contaminants from Industrial Dyeing Wastewater

  • Néstor A. Urbina-Suarez,
  • Cristian J. Salcedo-Pabón,
  • Jefferson E. Contreras-Ropero,
  • German L. López-Barrera,
  • Janet B. García-Martínez,
  • Andrés F. Barajas-Solano and
  • Fiderman Machuca-Martínez

This study investigates the influence of photoperiod and wastewater concentration on the growth of microalgae and cyanobacteria for the removal of environmentally significant parameters (COD, BOD, Cr, Fe, color, chlorides, nitrogen compounds, and pho...

  • Article
  • Open Access
18 Citations
2,363 Views
15 Pages

This article is devoted to the construction and statistical analysis of models that express the relationship between performance indicators and a large number of geological and technological factors. The volume of additionally produced oil, the volum...

  • Perspective
  • Open Access
2 Citations
2,717 Views
12 Pages

Multistep flow catalytic reactions in organic chemistry integrate multiple sequential organic reactions to enhance cost-efficiency, time management, and labour resources, all while boosting effectiveness and environmental sustainability. Similar to h...

  • Feature Paper
  • Article
  • Open Access
7 Citations
5,007 Views
18 Pages

This study presents the numerical simulation, optimization, preparation, and characterization of Cu(In, Ga)Se2 (CIGS) thin-film solar cells (TFSCs). Different cell parameters were investigated, including Ga/(Ga+In) (GGI) ratios, the thicknesses of CI...

  • Article
  • Open Access
12 Citations
3,354 Views
15 Pages

Bicarbonate-Activated Hydrogen Peroxide for an Azo Dye Degradation: Experimental Design

  • Karla Y. Mora-Bonilla,
  • Iván F. Macías-Quiroga,
  • Nancy R. Sanabria-González and
  • María T. Dávila-Arias

The present study investigated the degradation of an aqueous Allura Red AC (AR–AC) solution by activating hydrogen peroxide with bicarbonate using cobalt ion (Co2+) as the catalyst. Four independent variables (H2O2, NaHCO3, Co2+, and dye concen...

  • Article
  • Open Access
4 Citations
2,778 Views
13 Pages

Enhancing Heat Transfer Performance in Simulated Fischer–Tropsch Fluidized Bed Reactor through Tubes Ends Modifications

  • Laith S. Sabri,
  • Abbas J. Sultan,
  • Jamal M. Ali,
  • Hasan Shakir Majdi and
  • Muthanna H. Al-Dahhan

Fluidized bed reactors are essential in a wide range of industrial applications, encompassing processes such as Fischer–Tropsch synthesis and catalytic cracking. The optimization of performance and reduction in energy consumption in these react...

  • Article
  • Open Access
6 Citations
2,794 Views
15 Pages

Because of the specific thermodynamic properties of active pharmaceutical ingredients, the process of crystallization often meets implementation challenges in the pharmaceutical industry. Therefore, it is essential to select the appropriate method an...

  • Article
  • Open Access
1 Citations
3,660 Views
11 Pages

Red pepper powder is used as a spice added to various types of foods to improve the spiciness and aroma of foods. The unique aroma and spiciness of red pepper are related to the contents of bioactive compounds, including alkaloids, phenolic compounds...

  • Article
  • Open Access
7 Citations
2,843 Views
15 Pages

Chitosan–Resole–Pectin Aerogel in Methylene Blue Removal: Modeling and Optimization Using an Artificial Neuron Network

  • Jean Flores-Gómez,
  • Mario Villegas-Ruvalcaba,
  • José Blancas-Flores and
  • Juan Morales-Rivera

In this study, a novel chitosan–resole–pectin aerogel (CS–R–P) was created from a sol–gel reaction with a solution of Cs and P with resole by a freeze-drying technique, and this adsorbent was proposed for the removal of...

  • Article
  • Open Access
2 Citations
2,498 Views
11 Pages

Rheological measurements under an applied magnetic field were used to investigate the changes to the internal structure and stability of an aqueous ferrofluid. The ferrofluid was prepared by dispersing 1.8 wt.% of maghemite nanoparticles with a size...

  • Article
  • Open Access
4 Citations
2,568 Views
19 Pages

Polylactic acid (PLA), the second most produced biopolymer, was selected for the fabrication of mixed-matrix membranes (MMMs) via the incorporation of HKUST-1 metal–organic framework (MOF) particles into a PLA matrix with the aim of improving m...

  • Article
  • Open Access
1 Citations
2,308 Views
11 Pages

Dissolved inorganic nitrogen (DIN) species are key components of the nitrogen cycle and are the main nitrogen pollutants in groundwater. This study investigated the interconversion and removal of the principal DIN compounds (NO3, NO2 an...

  • Article
  • Open Access
1 Citations
5,873 Views
23 Pages

Stabilization of condensate is a highly energy-consuming process compared to other oil and gas processes. There is a need to reduce this energy consumption. Therefore, the present work aims to simulate the stabilization unit in terms of available ene...

  • Review
  • Open Access
18 Citations
7,258 Views
32 Pages

Methylene blue (MB) is a hazardous chemical that is widely found in wastewater, and its removal is critical. One of the most common methods to remove MB is adsorption. To enhance the adsorption process, magnetic adsorbents, particularly those based o...

  • Article
  • Open Access
11 Citations
4,159 Views
12 Pages

Chemical and Process Inherent Safety Analysis of Large-Scale Suspension Poly(Vinyl Chloride) Production

  • Ángel Darío González-Delgado,
  • Eduardo Aguilar-Vásquez and
  • Miguel Ramos-Olmos

In this work, a safety assessment was carried out for the suspension polymerization method, known for the lack of studies about its sustainable performance and long history of chemical accidents. Therefore, a safety analysis was conducted using the i...

  • Article
  • Open Access
5 Citations
3,880 Views
14 Pages

Effects of Phosphate and Thermal Treatments on the Characteristics of Activated Carbon Manufactured from Durian (Durio zibethinus) Peel

  • Astrilia Damayanti,
  • Ria Wulansarie,
  • Zuhriyan Ash Shiddieqy Bahlawan,
  • Suharta,
  • Mutia Royana,
  • Mikhaella Wai Nostra Mannohara Basuki,
  • Bayu Nugroho and
  • Ahmad Lutvi Andri

The availability of fossil energy is dwindling, so renewable fuels are the alternative choices, one of which is bioethanol. To increase the purity of the ethanol produced via the fermentation process, activated carbon (AC) was made from durian (Durio...

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ChemEngineering - ISSN 2305-7084