4.3.2. Thermal Analysis

Thermal analysis (thermogravimetry and differential scanning calorimetry) were carried out simultaneously using TGA/DSC1 apparatus (Mettler Toledo, Columbus, OH, USA). Samples were fractioned, weighed (not less than 10 mg) and placed into 100 μL aluminum crucibles. The analyses were performed at an air atmosphere in a temperature range from 30 to 600 ◦C, with a heating rate of 10 ◦C per minute.
