2.1.6. SCHCl3

BL (45 mg) was dissolved in the minimum quantity of anhydrous CHCl3 (0.35 mL) at 90 ◦C. The solution was cooled down inside the fridge (4–5 ◦C) until single crystal growing. This solvate was stable in the mother liquor. The single crystal was analyzed by SCXRD at low temperature to prevent its transformation into form SCHCl3-H2O.
