Facile Synthesis of Mesoporous Silica at Room Temperature for CO2 Adsorption
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Porous Silica Synthesis Using the Calcination Process
2.3. Porous Silica Synthesis Using the Room-Temperature Process
2.4. Introduction of Amine Group
2.5. Characterization
3. Results and Discussion
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
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Sample Name | Surface Area (m2/g) | Pore Volume (cm3/g) | Average Pore Size 1 (nm) |
---|---|---|---|
T-MS-0 | 1139.911 | 0.443 | 3.417 |
R-MS-0 | 1072.455 | 0.845 | 3.058 |
Sample Name | Pore Volume (cm3/g) | EDS Data | CO2 Adsorption (mmol/g) | Mass Variation after Introducing Amine Functional Groups (g) | ||||
---|---|---|---|---|---|---|---|---|
Atom Si (%) | Atom N (%) | Atom C (%) | Atom O (%) | Before | After | |||
T-MS-N | 0.443 | 6.66 | 18.32 | 49.85 | 25.18 | 5.384 | 0.51 | 1.07 |
0.56 | ||||||||
R-MS-N | 0.845 | 8.65 | 22.98 | 48.06 | 20.31 | 11.296 | 0.49 | 1.07 |
0.58 |
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Kang, M.; Lee, J.-t.; Kim, M.-K.; Byun, M.; Bae, J.-Y. Facile Synthesis of Mesoporous Silica at Room Temperature for CO2 Adsorption. Micromachines 2022, 13, 926. https://doi.org/10.3390/mi13060926
Kang M, Lee J-t, Kim M-K, Byun M, Bae J-Y. Facile Synthesis of Mesoporous Silica at Room Temperature for CO2 Adsorption. Micromachines. 2022; 13(6):926. https://doi.org/10.3390/mi13060926
Chicago/Turabian StyleKang, Misun, Jong-tak Lee, Min-Kyoung Kim, Myunghwan Byun, and Jae-Young Bae. 2022. "Facile Synthesis of Mesoporous Silica at Room Temperature for CO2 Adsorption" Micromachines 13, no. 6: 926. https://doi.org/10.3390/mi13060926