3.1. Effect of Bowl Rotating Speed
To investigate the effect of bowl rotating speed on the solids recovery in solid bowl centrifugation, four rotating speeds were tested, 2000 rpm, 3000 rpm, 4000 rpm and 5000 rpm, corresponding to relative centrifugal forces at 447 G, 1006 G, 1789 G and 2795 G, respectively. Three different feeds, Feed-1, Feed-3 and Feed-5, as shown in
Figure 2, were used in this investigation. The differential speed between the bowl and screw conveyor was 20 rpm, and the weir height was set at 15 mm. Feed rate, feed solids concentration and liquid dynamic viscosity were 0.0005 m
3/s, 10%
v/
v and 0.001 Pa·s, respectively. The solids recoveries at tested bowl rotating speeds are plotted in
Figure 3.
Figure 3 exhibits that a faster bowl rotating speed (i.e., a larger centrifugal force) can lead to a higher solids recovery for all tested feeds, and this finding is consistent with experimental observations made by others [
1,
2,
3]. Another observation from this batch of simulations was that the solids recovery was improved more significantly by increasing the bowl speed when the feed contains a large fraction of ultrafine particles. More specifically, the solids recovery rose by 9.50% for the finest feed (Feed-1) when the bowl speed increased from 3000 rpm to 4000 rpm, while a smaller improvement, 4.74%, was obtained for the coarsest feed (Feed-5) with the same bowl rotating speed adjustment.
By plotting the cut sizes of these simulations (see
Figure 4), one can note that the cut size was decreasing with an increase in bowl rotating speed. Meanwhile, cut sizes at a given bowl rotating speed were identical for the tested three feeds, indicating that the particle size distribution of the feed has a negligible impact on the cut size. When the cut size was only reduced from around 3.0 µm to about 2.3 µm by increasing the bowl rotating speed from 3000 rpm to 4000 rpm, the improved solids recovery was due to the higher fraction of ultrafines in the feed, especially those particles in the range of 2.3 µm to 3.0 µm. Furthermore, the decrease in the cut size became less significant even with a larger increase in the centrifugal force, if the bowl rotating speed was already at a high level. The implication of this finding is that one should choose the operating bowl rotating speed by balancing the solids recovery and the energy consumption, based on the feed particle sizes.
3.2. Effect of Differential Speed between the Bowl and Screw Conveyor
Seven differential speeds, from 10 rpm to 40 rpm with an interval of 5 rpm were tested to examine the influence of this parameter on solids recovery. Three feed solids concentrations (i.e., 2%, 5% and 10%
v/
v) and three different feed rates (i.e., 0.0003 m
3/s, 0.0005 m
3/s and 0.001 m
3/s) were tested for all seven differential speeds. Feed-3 was used in this batch of simulations. The bowl rotating speed, weir height and liquid dynamic viscosity were set at 4000 rpm, 15 mm and 0.001 Pa·s, respectively. The results of this batch of simulations are presented in
Figure 5.
From
Figure 5, it can be seen that the solids recovery tended to slightly decrease with an increase in the differential speed when the solids loading was low (i.e., low solids concentration or low feed rate). This trend was in agreement with the experimental results reported elsewhere [
1,
6,
7]. On the contrary,
Figure 5 also shows that an increase in the differential speed can lead to a higher solids recovery if the feed solids concentration was high or the feed rate was large. These trends were similar to the experimental observations made by Pinkerton et al. [
13]. As mentioned by Suhr et al. [
6] and Day [
7], the differential speed would affect both the sediment height and the levels of flow turbulence within the settling channel. Depending on which effect is the dominant one, different trends can result from increasing the differential speed of the SBC.
3.2.1. Effect of Differential Speed on Sediment Height
By plotting the heights of sediments in the flow channel, shown in
Figure 6, one can readily see that the sediment height along the whole sedimentation channel increased with a higher solids loading (i.e., with a high feed rate and/or high feed solids concentration). As a result, the effective volume for particle settling, which is the space in between the surface of slurry and the reversed flow, as illustrated in
Figure 1, was smaller if the sediment height was larger, resulting in a lower solids recovery. In this case, accelerating the differential speed can help with the solids discharge, thereby decreasing the sediment height. The solids recovery is, therefore, improved by increasing the differential speed.
3.2.2. Effect of Differential Speed on Backflow
A faster differential speed can also lead to a stronger backflow near the surface of the sediments, which can reduce the effective volume for particle settling. This phenomenon can be employed to explain the influence of the differential speed on the solids recovery at low solids loading scenarios. In these cases, even at slow differential speeds, the sediment height remains small, as shown in
Figure 6A,D. Thus, increasing the differential speed in these cases can have a limited effect on the sediment height reduction. On the contrary, a higher differential speed will have an adverse effect on the solids recovery due to the fact that the increased differential speed would induce a stronger backflow, resulting in a smaller effective volume for particle settling (as shown in
Figure 7A,D).
3.2.3. Effect of Differential Speed on Solids Recovery
As shown in
Figure 5A,B, opposite trends were found by increasing the differential speed at different solids loadings. To further investigate the causes of these conflicting trends, a detailed analysis of the effect of differential speed on sediment height and effective volume for particle settling was conducted, and the following findings were identified:
- (i)
When the solids loading is high (i.e., high feed solids concentration and/or high feed rate), the sediment height was high, resulting a small effective volume for particle settling. At this condition, a faster differential speed is preferred, as it can transfer the sediment at a higher rate, thereby reducing the sediment height and leading to a higher solids recovery.
- (ii)
When the solids loading of the SBC is low, however, the sediment height is also at a low level, and a higher differential speed can only reduce the height to a limited extent. On the contrary, the high differential speed introduces a stronger backflow, thus reducing the effective volume for particle settling (as shown in
Figure 7A,D). A lower solids recovery, therefore, results from increasing the differential speed in this case.
3.3. Effect of Weir Height
The study on the effect of the weir height on the solids recovery was carried out by testing 15 levels of weir heights, ranging from 5 mm to 60 mm, at three different feed solids loadings. The feed used in this batch of simulations was Feed-3 (see
Figure 2). Other parameters, including bowl rotating speed, differential speed and liquid dynamic viscosity, were set at 4000 rpm, 20 rpm and 0.001 Pa·s, respectively. The results of the batch simulations are shown in
Figure 8.
Figure 8 shows that the solids recovery first increased with increasing weir height for all three tested solids loadings, reaching a peak before decreasing at larger weir heights. These findings were consistent with the experimental results reported by Peeters and Weis [
11] that the solids recovery firstly improved with a deeper weir setting and more solids could be lost in the effluent if the weir height setting exceeded its optimal value. Apparently, the solids retention time within the SBC will be prolonged with a deeper pool depth (i.e., a higher weir setting), thereby improving the solids capture within the SBC [
1,
2]. However, the decreasing trend in solids recovery after the optimal weir height settings is contradicted with this theory, and further investigation on the causes of the declining trend is needed.
This downtrend could be due to two undesirable side effects of increasing the weir height. Firstly, the radial settling distance becomes larger than that of shallow pool depth for particles entering the sedimentation channel near the pool surface. As a result, the required settling times for those particles are longer, thus receiving a decreased solids recovery. Secondly, when the weir height is increased, particles within the upper part of the flow (i.e., near the water surface) will experience a lower acting centrifugal force due to the smaller distance from the particle’s current position to the rotating axis. Consequently, the separation size for particles entering the sedimentation channel at the upper part positions will be larger than that of a shallow weir height setting, resulting in a lower solids recovery.
Figure 9 shows the separation sizes of the SBC when the feed solids concentration and feed flow rate were 5% and 0.0005 m
3/s, respectively. It can be seen that the minimal cut size initially decreased with an increasing weir height, from 1.68 µm (with a weir height of 5 mm) to 0.65 µm (with a weir height of 20 mm), while the maximum cut size for the particles entering at the upper part of the sedimentation channel only increased by 0.35 µm. As a result, the solids recovery rose from 85.08% to 88.79% (see
Figure 8) when the weir height increased from 5 mm to 20 mm. On the other hand, with a further increase in the weir height, the maximal separation size for particles entering at the upper part of the sedimentation channel became significantly larger, from 3.16 µm (with a weir height of 20 mm) to 4.62 µm (with a weir height of 60 mm), as shown in
Figure 9. This increase in the cut size, therefore, led to a decrease in the solids recovery, by 6.6% (see
Figure 8), as more fine particles (<4.62 µm) were lost in the effluent.
In summary, increasing weir height can be beneficial to the solids recovery when the pool depth is shallow (i.e., low weir height settings), as more ultrafines can be recovered owing to the decrease in separation size. Increasing the weir height setting, however, can lead to a lower solids recovery when the weir height setting is already at a high level, due to the separation size becoming larger for particles entering the sedimentation channel at upper positions.
The finding of the impact of the weir height setting on the solids recovery can be used to explain the conflicting results reported by Klima et al. [
4] and Pedro [
12]. More specifically, the weir settings used in Ref. [
4] ranged from 3.38 mm to 15.88 mm and the diameter of the SBC employed in their study was 150 mm. These weir height settings can be regarded as within the ‘shallow’ weir range, and therefore, an increasing trend was observed when adjusting the weir height to a higher position. On the contrary, Pedro [
12] tested the solids removal for drilling muds in the SBC with a diameter of 355 mm, and three weir height settings, 38 mm, 55 mm and 78 mm were investigated. Apparently, these weir height settings were relatively high and the dominant factor affecting the solids recovery was the enlarged separation sizes for particles entering the sedimentation channel at the upper part. This explained why a declining trend was observed when increasing the weir height [
12].
3.4. Effect of Feed Rate and Feed Solids Concentration
The feed flowrate and feed solids concentration collectively determine the solids loading of the SBC, and both parameters can affect the solids recovery, as reported in several studies [
1,
2,
4,
5,
10]. In this batch of simulations, Feed-3 (see
Figure 2) was used, and five feed flowrates and seven levels of solids concentrations were tested, while other process variables were set as 4000 rpm, 20 rpm, 15 mm and 0.001 Pa·s for bowl rotating speed, differential speed, weir height and liquid dynamic viscosity, respectively. The results of this batch of simulations are presented in
Figure 10. It should be noted that the data for the feed rate at 0.001 m
3/s with 20% solids concentration feed was not available, as the solids loading exceeded the capacity of the simulated SBC.
Figure 10 shows that the solids recoveries were generally lower at higher solids loadings (e.g., higher feed rate and higher feed solids concentration). But the degrees of solids recovery changes were different. More specifically, when the feed rate was kept at 0.0001 m
3/s and the feed solids concentration was increased from 1% to 20%, the solids recovery only decreased by 2.46%. Meanwhile, at a constant low solids concentration, 1%, raising the feed flowrate from 0.0001 m
3/s to 0.001 m
3/s, can significantly reduce the solids recovery from 96.44% to 86.64%. These results suggested that it would be important to control the feed rate, thereby ensuring a longer retention time of the particles within the settling channel to achieve a higher solids recovery. Controlling the feed flowrate is critical, especially when the feed solids concentration is high.
Figure 11 gives the cut sizes of the simulated SBC at various feed flowrates and solids concentrations. One can see that cut sizes were larger when both the feed rate and solids concentration were at high levels. This increase in the cut size can be attributed to: (i) shortened particle residence time when increasing the feed rate and (ii) more severe hindered effect (i.e., stronger particle–particle interactions) when increasing the feed solids concentration.
3.5. Effect of Particle Size Distribution of the Feed
To test the influence of feed particle size on the solids recovery, five feeds with different particle size distributions (see
Figure 2) were used in this batch of simulations. Other process variables were set at 4000 rpm, 20 rpm, 15 mm, 0.0005 m
3/s, 5% and 0.001 Pa·s for bowl rotating speed, differential speed, weir height, feed rate, feed solids concentration and liquid dynamic viscosity, respectively.
Figure 12 presents the achieved solids recoveries and cut sizes with these feeds. The solids recovery increased with the feed becoming coarser, and this result was consistent with experimental outcomes reported elsewhere [
8,
9]. Despite the improvement in solids recovery, the cut size of the SBC remained at a narrow range, around 1.65 µm (see
Figure 12), indicating that the improved solids capture was mainly due to an increased fraction of coarser particles in the feed.
To further assess the impact of feed particle sizes on the solids recovery, four more different feeds with different particle size distributions but the same P50 were tested with other parameters being set at 4,000 rpm, 20 rpm, 15 mm, 0.0005 m
3/s, 5% and 0.001 Pa·s for bowl rotating speed, differential speed, weir height, feed rate, feed solids concentration and liquid dynamic viscosity, respectively. The particle size distributions of these four feeds (i.e., Feed-6 to Feed-9) are illustrated in
Figure 13A,B. One can see that: (i) the P50 was same for these four feeds, around 5 μm, (ii) Feed-6 contained more ultrafine particles (<2 μm), (iii) the majority size fraction of Feed-9 was the middle-sized particles (4 μm to 10 μm) and (iv) Feed-6 also had the largest proportion of coarse particles (>10 μm).
From
Figure 13C, one can note that the solids recovery of Feed-9 was 88.5% while that of Feed-6 was only 78.1% despite the fact that Feed-6 contained more coarse particles and all four feeds had the same P50. Meanwhile,
Figure 13C also shows that the cut sizes for these four feeds were around 1.67 µm. Combining the results for Feed-1 to Feed-5, it can be concluded that the cut size was indifferent to the feed size distributions tested and the solids recovery appeared to depend on the fraction of ultrafine particles (<1 µm) in the feed.
3.6. Effect of Liquid Dynamic Viscosity
Although the liquid viscosity can affect the solids recovery in solid bowl centrifugation [
7], there has been no detailed study of this variable. To attain a clearer picture on the influence of this parameter on centrifugal dewatering, a batch of centrifugation simulations was carried out with the liquid dynamic viscosity varying from 0.0001 Pa·s to 0.01 Pa·s. Feed-3 was used, and other process variables were set at 4000 rpm, 20 rpm, 15 mm, 0.0005 m
3/s and 5% for bowl rotating speed, differential speed, weir height, feed rate and feed solids concentration, respectively. The results of these simulations are presented in
Figure 14.
Figure 14 shows that the liquid viscosity had a significant impact on the solids recovery in solid bowl centrifugation, and a higher liquid viscosity would lead to a lower solids recovery. For instance, the solids recovery was reduced by 7.7 percentage points, from 89.2% to 81.5%, when the liquid viscosity was doubled from 0.001 Pa·s to 0.002 Pa·s. Meanwhile, there was an increase in cut size when increasing the liquid viscosity. The increase in cut size could be caused by the enhanced inertia of the liquid, as larger liquid inertia would reduce the settling speed of the particle. Consequently, only large particles which had a faster settling speed could settle onto the sediment at a given residence time. As a result, the solids recovery would be reduced by increasing the liquid viscosity.
In order to improve the solids recovery, adding flocculants into the feed slurry to enlarge the feed particles is commonly practiced in solid bowl centrifugation [
1,
10]. However, several researchers [
22,
23,
24] have found that the liquid viscosity could be also increased by adding flocculants into the feed slurries. The results from this batch of simulations suggested that the impact of the flocculant on the liquid viscosity of the feed slurry should be taken into consideration in the reagent selection process as higher liquid viscosity can have an adverse effect on the solids recovery.