Variation in Micro-Pores during Dynamic Consolidation and Compression of Soft Marine Soil
Abstract
:1. Introduction
2. Materials and Methods
2.1. Test Materials
2.2. Test Instrument
- (1)
- The automatic consolidation and expansion test instrument consisted of a pressure chamber, acquisition system, computer, and other components, as shown in Figure 2. The sample was installed in the pressure chamber. After setting the test conditions, the sample cyclic loading test was performed through the built-in control panel to collect the readings from the force and displacement sensors, controlling the stepper motor, and with the high-speed and accurate micro-stepper motor imposing a vertical load on the sample.
- (2)
- In this study, a QUANTA FEG 650 field emission scanning electron microscope (FEI company, Eindhoven, The Netherlands), depicted in Figure 3, was used to study the pores of the soft marine soil. An SEM is primarily composed of vacuum, electron beam, and imaging systems. The electron beam system emits high-energy incident electrons to bombard the material surface, producing secondary and backscattered electrons, which are received by the probe for imaging.
2.3. Test Plan
2.3.1. Dynamic Consolidation Compression Test
2.3.2. SEM Test
- (1)
- A total of 17 groups of undisturbed soft marine soil samples under different test conditions were obtained for drying treatment. A horizontal section of the sample was selected as the observation surface. When the soil sample was in a semi-solid state, we selected the core of the sample to cut into strips with a 5 × 1 × 1 cm cross-section. Then, drying was continued.
- (2)
- After drying, to ensure that the observation section was not disturbed, the samples were cut into 5 × 5 × 2 mm microscopic samples and polished. Then, we used a washing ear ball to blow away loose floating particles.
- (3)
- Before scanning, due to the poor electrical conductivity of the soft clay, to ensure the quality of the micro-images, we coated the dry soil surface with a layer of 20–50 nm gold film as a conductive material.
2.4. Image Acquisition
2.5. SEM Image Processing
3. Qualitative Analysis of the Microstructure of Soft Marine Soil under Cyclic Loading
4. Quantitative Analysis of the Microstructure of Soft Marine Soil under Cyclic Loading
4.1. Introduction of Microstructure Parameters
- (1)
- Diameter (D) is the most basic characteristic of pore size. The pore diameter is the average length of two points on the edge of the pore profile passing through the centroid, which can be directly measured using IPP.
- (2)
- Area (S) is also a basic characteristic of pore size. The pore area is the area surrounded by the edge of the pore profile, which can be directly measured using IPP.
- (3)
- Roundness (R0) is used to describe how close the target shape is to a circle. Roundness is calculated as:R0 = L2/(4πS),
- (4)
- Directional frequency (Pi(α)).To represent the variation in the distribution intensity of the unit in a certain direction, we divided 0°~180° into N equal parts (locations). The angle range of each location representing the direction is α = 180°/N. Thus, the directional distribution frequency of the ith location unit in N locations within 0°~180° can be calculated:
- (5)
- Probability entropy (Hm).Shi et al. [24] introduced the concept of probabilistic entropy in modern system theory to the study of microstructures and used Hm to represent the ordered arrangement of soil microstructure units, as defined in Formula (3):
4.2. Pore Equivalent Diameter Distribution
4.3. Pore Area Distribution
4.4. Pore Roundness
4.5. Directional Frequency
4.6. Probability Entropy
5. Conclusions
- (1)
- Before cyclic loading, the microscopic images of soft marine soil show flocculation and a honeycomb flocculation structure. The aggregates are mostly flocculent, and the pores between particles are large, forming a local weakening area. After cyclic loading, the macropores decrease, and the structure becomes denser. The fragmentation of large particles and the aggregation of small particles occur simultaneously, and the aggregate structures of soil particles are inlaid with each other.
- (2)
- After cyclic loading, the large pores are squeezed and broken, resulting in decreases in pore diameter and pore roundness, and an increase in uniformity. At this time, the internal structure of soft marine soil gradually stabilizes. With increases in p0, ζ, and OCR, the compression effect of the soil is more obvious, and the degree of change in the above microstructure parameters is larger.
- (3)
- After cyclic loading, the directional frequency Pi (10) of the pores in a certain location at 0° to 180° increases significantly. This shows that, after loading, the pores in soft marine soil develop in a certain direction, giving the pores directional property. As the consolidation confining pressure, cyclic dynamic stress ratio, and over-consolidation ratio increase, the porosity probability entropy decreases. This shows that, after loading, the pores of the soft marine soil become more orderly, and the strain growth also increases. The microscopic test results further verify the macroscopic strain law.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
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Weight (kN·m−3) | Moisture Content (%) | Specific Gravity | Plastic Limit | Liquid Limit (%) | Plasticity Index | Liquidity Index | |
---|---|---|---|---|---|---|---|
Mean | 15.7 | 62.47 | 2.74 | 27.0 | 44.6 | 17.6 | 2.01 |
Group | Soil Sample Number | p0 (kPa) | ζ | Number of Vibrations | OCR |
---|---|---|---|---|---|
SEM-A | A0 | Undisturbed soft marine soil (unloaded) | |||
A1 | 100 | 3 | 20.000 | 1 | |
A2 | 200 | 3 | 20.000 | 1 | |
A3 | 300 | 3 | 20.000 | 1 | |
A4 | 400 | 3 | 20.000 | 1 | |
A5 | 500 | 3 | 20.000 | 1 | |
SEM-B | B0 | Undisturbed soft marine soil (unloaded) | |||
B1 | 100 | 3 | 20.000 | 1 | |
B2 | 100 | 6 | 20.000 | 1 | |
B3 | 100 | 8 | 20.000 | 1 | |
B4 | 100 | 10 | 20.000 | 1 | |
B5 | 100 | 15 | 20.000 | 1 | |
SEM-C | C0 | Undisturbed soft marine soil (unloaded) | |||
C1 | 100 | 3 | 20.000 | 1 | |
C2 | 300 | 3 | 20.000 | 3 | |
C3 | 600 | 6 | 20.000 | 6 | |
C4 | 900 | 9 | 20.000 | 9 |
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Dai, C.-X.; Zhang, Q.-F.; He, S.-H.; Zhang, A.; Shan, H.-F.; Xia, T.-D. Variation in Micro-Pores during Dynamic Consolidation and Compression of Soft Marine Soil. J. Mar. Sci. Eng. 2021, 9, 750. https://doi.org/10.3390/jmse9070750
Dai C-X, Zhang Q-F, He S-H, Zhang A, Shan H-F, Xia T-D. Variation in Micro-Pores during Dynamic Consolidation and Compression of Soft Marine Soil. Journal of Marine Science and Engineering. 2021; 9(7):750. https://doi.org/10.3390/jmse9070750
Chicago/Turabian StyleDai, Chen-Xiang, Qiong-Fang Zhang, Shao-Heng He, An Zhang, Hua-Feng Shan, and Tang-Dai Xia. 2021. "Variation in Micro-Pores during Dynamic Consolidation and Compression of Soft Marine Soil" Journal of Marine Science and Engineering 9, no. 7: 750. https://doi.org/10.3390/jmse9070750
APA StyleDai, C. -X., Zhang, Q. -F., He, S. -H., Zhang, A., Shan, H. -F., & Xia, T. -D. (2021). Variation in Micro-Pores during Dynamic Consolidation and Compression of Soft Marine Soil. Journal of Marine Science and Engineering, 9(7), 750. https://doi.org/10.3390/jmse9070750