Preliminary Study on the Preparation of Conductive Nanosized Calcium Carbonate Utilizing Biogas Slurry by a Synchronous Double Decomposition Coating Method
Abstract
:1. Introduction
2. Materials and Methods
2.1. Raw Materials and Chemical Reagents
2.2. Preparation of CNCC
2.3. Characterization Methods
3. Results
3.1. HA-NCC Formed in Biogas Slurry
3.2. Morphological Features of CNCC
3.3. Crystal Structure and Composition of CNCC
3.4. TGA and BET
3.5. Graphitization and Conductivity of CNCC
4. Discussion
4.1. A Meaningful Discovery in Biogas Slurry
4.2. Synchronous Double Decomposition Coating Method
4.3. CNCC
4.4. Limitations and Development Prospects
5. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Chemical Element | Mass Percentage of Chemical Element (%) | Oxide Component | Mass Percentage of Oxide Component (%) |
---|---|---|---|
Ca | 57.45 | CaO | 50.35 |
O | 22.01 | CO2 | 47.09 |
C | 17.97 | P2O5 | 0.95 |
Cl | 0.84 | Cl | 0.61 |
P | 0.56 | K2O | 0.29 |
Sr | 0.36 | SrO | 0.21 |
K | 0.34 | SO3 | 0.15 |
Na | 0.12 | Na2O | 0.12 |
Zn | 0.12 | ZnO | 0.07 |
Fe | 0.09 | SiO2 | 0.07 |
S | 0.08 | Fe2O3 | 0.06 |
Si | 0.04 | Al2O3 | 0.03 |
Al | 0.02 | - | - |
Total | 100.00 | Total | 100.00 |
Functional Materials | Resistivity/Ω·cm | Conductivity/S·cm−1 | References |
---|---|---|---|
CNCC | 2.62 × 106 | 3.8 × 10−7 | This study |
CaCO3 | >107 | <10−7 | [39] |
CaCO3-SiO2 | >107 | <10−7 | [39] |
Polymers | 1015~1017 | 10−15~10−17 | [15] |
Pure polyaniline (PANI) | 2.63 × 102 | 3.8 × 10−1 | [40] |
CaCO3-SiO2-PANI (1:1~3:1) | 1.79 × 103~1.75 × 104 | 5.6 × 10−2~5.7 × 10−3 | [41] |
PANI/CaCO3 composites | 1.0 × 105 | 1.0 × 10−5 | [26] |
CaCO3-Ni (0.47:1~1:1) | 1.2 × 106~3.4 × 1011 | 8.3 × 10−7~2.9 × 10−12 | [42] |
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Pan, F.; Xiao, H.; Huang, F.; Zhu, H.; Lei, J.; Ma, J. Preliminary Study on the Preparation of Conductive Nanosized Calcium Carbonate Utilizing Biogas Slurry by a Synchronous Double Decomposition Coating Method. Nanomaterials 2023, 13, 1938. https://doi.org/10.3390/nano13131938
Pan F, Xiao H, Huang F, Zhu H, Lei J, Ma J. Preliminary Study on the Preparation of Conductive Nanosized Calcium Carbonate Utilizing Biogas Slurry by a Synchronous Double Decomposition Coating Method. Nanomaterials. 2023; 13(13):1938. https://doi.org/10.3390/nano13131938
Chicago/Turabian StylePan, Fanghui, Han Xiao, Fei Huang, Hongguang Zhu, Jingjing Lei, and Jie Ma. 2023. "Preliminary Study on the Preparation of Conductive Nanosized Calcium Carbonate Utilizing Biogas Slurry by a Synchronous Double Decomposition Coating Method" Nanomaterials 13, no. 13: 1938. https://doi.org/10.3390/nano13131938