Effects of Hydrothermal and Microwave Dual Treatment and Zein on the Enzymolysis of High Amylose Corn Starch
Abstract
:1. Introduction
2. Results and Discussion
2.1. Morphological Characteristics
2.2. Color
2.3. Particle Size
2.4. X-ray Diffraction
2.5. Viscosity
2.6. Thermal Properties
2.7. Enzymolysis
3. Conclusions
4. Materials and Methods
4.1. Materials
4.1.1. Preparation of the Hydro-Micro HACS
4.1.2. Preparation of the Zein and Hydro-Micro HACS Composite
4.2. Scanning Electron Microscopy (SEM)
4.3. Color
4.4. Particle Size
4.5. X-ray Diffraction
4.6. Viscosity
4.7. Thermal Properties
4.8. Enzymolysis
4.9. Statistical Analysis
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Sample | a* | b* | L* | Particle Size/μm | Viscosity/cP | Weight Loss Rate/% | Decomposition Temperature/°C | Crystallinity/% |
---|---|---|---|---|---|---|---|---|
HACS | −1.23 ± 0.01 a | 9.32 ± 0.01 b | 97.02 ± 1.01 a | 12.52 ± 1.06 b | 362 ± 1.00 a | 80.99 ± 1.11 a | 316.98 ± 2.08 b | 20.87 ± 0.15 a |
Hydro-micro-HACS | −1.24 ± 0.01 a | 9.33 ± 0.02 b | 97.03 ± 0.99 a | 12.68 ± 0.01 b | 270 ± 3.00 b | 80.29 ± 0.50 a | 317.84 ± 1.09 a | 16.98 ± 0.23 b |
Composite | −1.24 ± 0.02 a | 20.90 ± 3.01 a | 94.10 ± 2.02 b | 27.65 ± 2.96 a | 234 ± 3.00 c | 74.83 ± 2.30 b | 309.41 ± 2.10 c | 12.11 ± 0.12 c |
Sample | Peak1 | Peak2 | ||||||
---|---|---|---|---|---|---|---|---|
To/°C | Tp/°C | Tc/°C | ∆H (J/g) | To/°C | Tp/°C | Tc/°C | ∆H (J/g) | |
HACS | - | - | - | - | 132.95 ± 0.10 b | 133.05 ± 0.15 b | 139.16 ± 0.11 a | 13.34 ± 0.10 a |
Hydro-micro-HACS | - | - | - | - | 134.78 ± 0.18 a | 135.39 ± 0.10 a | 138.61 ± 0.09 b | 6.78 ± 0.12 b |
Composite | 84.77 ± 0.23 | 95.79 ± 0.21 | 104.97 ± 0.14 | 6.91 ± 0.20 | 134.76 ± 0.04 a | 135.23 ± 0.12 a | 138.62 ± 0.02 b | 5.65 ± 0.34 c |
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Liu, J.; Yang, Q.; Yuan, T.; Liu, Y.; Fang, G. Effects of Hydrothermal and Microwave Dual Treatment and Zein on the Enzymolysis of High Amylose Corn Starch. Gels 2022, 8, 29. https://doi.org/10.3390/gels8010029
Liu J, Yang Q, Yuan T, Liu Y, Fang G. Effects of Hydrothermal and Microwave Dual Treatment and Zein on the Enzymolysis of High Amylose Corn Starch. Gels. 2022; 8(1):29. https://doi.org/10.3390/gels8010029
Chicago/Turabian StyleLiu, Jie, Qiuye Yang, Tiantian Yuan, Yawei Liu, and Guihong Fang. 2022. "Effects of Hydrothermal and Microwave Dual Treatment and Zein on the Enzymolysis of High Amylose Corn Starch" Gels 8, no. 1: 29. https://doi.org/10.3390/gels8010029