Characterization of Palladium Nanoparticles Produced by Healthy and Microwave-Injured Cells of Desulfovibrio desulfuricans and Escherichia coli
Abstract
:1. Introduction
2. Materials and Methods
2.1. Bacterial Strains and Culture Conditions
2.2. Microwave Irradiation of E. coli and D. desulfuricans Cells
2.2.1. Microwave Irradiation Conditions
2.2.2. Microwave Irradiation of Resting Cells Suspended in MOPS Buffer
2.3. Preparation of Palladium-Challenged Cells
2.3.1. Palladium Solution
2.3.2. Formation of PdNanoparticles by Control and MW-Treated Cells
2.3.3. Residual Pd(II) Quantification Using the Tin(II) Chloride Method
2.4. High-Resolution Scanning Transmission Electron Microscopy (STEM) with HAADF (High-Angle Annular Dark Field) Detector and EDX Analysis
2.5. Image Processing, Lattice Spacing Determination and Particle Size Analysis
3. Results
3.1. Microwave-Injury of Bacteria
3.2. Examination of the Pd Nanoparticles Produced by Native and MW-Injured Cells of E. Coli MC4100 and D. Desulfuricans NCIMB 8307
3.3. Dispersity and Size Distribution of Pd Nanoparticles
3.4. Crystallinity and Lattice Spacing of Pd Nanoparticles
4. Discussion
5. Conclusions
Supplementary Materials
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Gomez-Bolivar, J.; Mikheenko, I.P.; Macaskie, L.E.; Merroun, M.L. Characterization of Palladium Nanoparticles Produced by Healthy and Microwave-Injured Cells of Desulfovibrio desulfuricans and Escherichia coli. Nanomaterials 2019, 9, 857. https://doi.org/10.3390/nano9060857
Gomez-Bolivar J, Mikheenko IP, Macaskie LE, Merroun ML. Characterization of Palladium Nanoparticles Produced by Healthy and Microwave-Injured Cells of Desulfovibrio desulfuricans and Escherichia coli. Nanomaterials. 2019; 9(6):857. https://doi.org/10.3390/nano9060857
Chicago/Turabian StyleGomez-Bolivar, Jaime, Iryna P. Mikheenko, Lynne E. Macaskie, and Mohamed L. Merroun. 2019. "Characterization of Palladium Nanoparticles Produced by Healthy and Microwave-Injured Cells of Desulfovibrio desulfuricans and Escherichia coli" Nanomaterials 9, no. 6: 857. https://doi.org/10.3390/nano9060857