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Keywords = extrusion deformation

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18 pages, 19953 KB  
Article
Using a Combination of ECAP and HE Processes to Produce Isotropic Ultrafine-Grained Titanium
by Mariusz Kulczyk, Jacek Skiba, Sylwia Przybysz-Gloc, Łukasz Maj, Jakub Kawałko and Monika Skorupska
Materials 2025, 18(22), 5194; https://doi.org/10.3390/ma18225194 (registering DOI) - 15 Nov 2025
Abstract
This paper proposes a complex plastic forming process for grade 2 titanium using a combination of severe plastic deformation techniques, equal-channel angular pressing (ECAP) and hydrostatic extrusion (HE). The aim of the combination of these methods is to reduce the strength of the [...] Read more.
This paper proposes a complex plastic forming process for grade 2 titanium using a combination of severe plastic deformation techniques, equal-channel angular pressing (ECAP) and hydrostatic extrusion (HE). The aim of the combination of these methods is to reduce the strength of the phenomenon of microstructural anisotropy and the resulting anisotropy of mechanical properties characteristic of the HE process. Two routes of plastic deformation (HE and ECAP + HE) were compared using the same total strain rate of ε ~ 3.5. Results: The analysis of mechanical properties and microstructure studies using TEM and SEM/EBSD techniques showed that it is possible to obtain large microstructure refinement of titanium with almost identical mechanical properties via both studied techniques. In addition, this also leads to a significant improvement in the strength of UTS by ~ 1000 MPa, YS by ~ 945 MPa and ductility (E) by ~ 25%. These findings indicate that applying a sequential ECAP + HE strategy can effectively reduce anisotropy and improve the overall performance of grade 2 titanium. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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19 pages, 3551 KB  
Article
A New Kind of Thermosensitive Screen Used for Wellbore Stability
by Yanlong Zhao, Yuheng Wei, Xing Qin and Yifei Ran
Processes 2025, 13(11), 3674; https://doi.org/10.3390/pr13113674 - 13 Nov 2025
Viewed by 70
Abstract
In light of frequently occurring wellbore instability such as wellbore collapse and sand production that often occur in drilling and the completion of shale oil and gas development, we propose one-run shape memory thermosensitive screen technology that can expand spontaneously at a specific [...] Read more.
In light of frequently occurring wellbore instability such as wellbore collapse and sand production that often occur in drilling and the completion of shale oil and gas development, we propose one-run shape memory thermosensitive screen technology that can expand spontaneously at a specific temperature to help strengthen the formation. Based on the theory of thermal expansion and large deformation of shape memory materials, the expansion process of the thermosensitive screen is calculated by the finite element method. After expanding to the wellbore wall, the effects of the screen squeezing force on the formation production parameters are evaluated theoretically. The analysis shows that the radial compressive stress of the thermosensitive screen decreases with the increase in the radial distance, but as the original outer diameter of the thermosensitive screen is greater than the wellbore diameter, it can provide extrusion force for the wellbore wall. According to the in situ stress model, the extrusion force after the screen contacts the wellbore can effectively improve the stress distribution near the wellbore and reduce the impact of sand production caused by formation instability. Moreover, in shale oil and gas completion, it can effectively increase the bottom hole flowing pressure and drawdown pressure. Full article
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7 pages, 1413 KB  
Proceeding Paper
Oscillatory Shear Rheology of PE/PP/MWCNT Nanocomposites
by Dorottya Antaliczné Nagy, Balázs Ádám, Erika Varga, Pál Hansághy, Ferenc Palásti and László Tóth
Eng. Proc. 2025, 113(1), 51; https://doi.org/10.3390/engproc2025113051 - 10 Nov 2025
Viewed by 152
Abstract
The present paper focuses on the effect of carbon nanotubes (CNTs) on the rheological behavior of polyethylene/polypropylene (PE/PP) blends to improve PE/PP mixtures for industrial applications. In our research, 40 wt% HDPE-60 wt% PP blends were produced by extrusion, and 0.59%, 1.18%, and [...] Read more.
The present paper focuses on the effect of carbon nanotubes (CNTs) on the rheological behavior of polyethylene/polypropylene (PE/PP) blends to improve PE/PP mixtures for industrial applications. In our research, 40 wt% HDPE-60 wt% PP blends were produced by extrusion, and 0.59%, 1.18%, and 2.35% multiwalled carbon nanotubes (MWCNTs) were added. Oscillation rheometry was used to study the HDPE-PP-MWCNT nanocomposites and the unfilled polymers at temperatures of 210, 220, 230, 240, and 250 °C in the angular frequency range of 0.05–628.32 rad/s, with 5% deformation. It was demonstrated that in the presence of CNTs, both the complex viscosity and modulus values increase above the percolation threshold. Additionally, it was observed that the crossover modulus (Gx) for all mixtures decreases with increasing temperature. In addition, at 1.18% CNT content, a second crossover appears at all temperatures, and its value increases with temperature. Full article
(This article belongs to the Proceedings of The Sustainable Mobility and Transportation Symposium 2025)
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23 pages, 7124 KB  
Article
Design and Characterization of Yeast Protein–Polysaccharide Bioink Blends for 3D Printing
by Or Peleg-Evron, Noy Hen, Maya Davidovich-Pinhas, Shulamit Levenberg and Havazelet Bianco-Peled
Polysaccharides 2025, 6(4), 101; https://doi.org/10.3390/polysaccharides6040101 - 10 Nov 2025
Viewed by 279
Abstract
Yeast protein (YP) offers nutritional and sustainable benefits; however, its poor gelation properties limit its use in soft material formulations. This study investigates the rheological behavior and the formation of crosslinked networks using YP–polysaccharide mixtures for extrusion-based 3D printing. Binary bioink blends with [...] Read more.
Yeast protein (YP) offers nutritional and sustainable benefits; however, its poor gelation properties limit its use in soft material formulations. This study investigates the rheological behavior and the formation of crosslinked networks using YP–polysaccharide mixtures for extrusion-based 3D printing. Binary bioink blends with alginate (Alg) or xanthan gum (XG) showed enhanced viscosity and exhibited shear-thinning properties. However, a high concentration of Alg negatively affected the material’s thixotropic recovery. On the other hand, YP–XG bioink displayed more pronounced elastic behavior and demonstrated thixotropic recovery, though they lacked the capacity for ionic crosslinking. A triple bioink formulation consisting of 8% (w/v) YP, 2% (w/v) Alg, and 0.5% (w/v) XG effectively combined the advantages of both polysaccharides. Alg provided structural stability through calcium crosslinking, while XG offered rheological flexibility. These bioinks were successfully printed using embedded 3D printing and maintained their shape fidelity after printing. The crosslinked triple hydrogel exhibited good mechanical strength, volume retention after crosslinking, structural integrity under compression of up to 70%, and recovery after deformation that indicates high structural stability. This research presents an effective strategy to enhance the application of yeast-derived proteins in sustainable, animal-free 3D printed food products and other soft biomaterials. Full article
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29 pages, 5132 KB  
Article
Mechanism of a Composite Energy Field for Inhibiting Damage in High-Silicon Aluminum Alloy During Micro-Turning
by Jiaxin Zhao, Yan Gu, Yamei Liu, Lingling Han, Bin Fu, Xiaoming Zhang, Shuai Li, Jinlong Chen and Hongxin Guo
Micromachines 2025, 16(11), 1263; https://doi.org/10.3390/mi16111263 - 7 Nov 2025
Viewed by 241
Abstract
Composite materials are widely utilized for their excellent properties; however, the mismatch in phase response during processing often induces surface and subsurface damage. While reducing the cutting depth is a common strategy to improve quality, it shifts the material removal mechanism from shear [...] Read more.
Composite materials are widely utilized for their excellent properties; however, the mismatch in phase response during processing often induces surface and subsurface damage. While reducing the cutting depth is a common strategy to improve quality, it shifts the material removal mechanism from shear to ploughing–extrusion, which can, in fact, degrade the final surface integrity. Energy field assistance is a promising approach to suppress this issue, yet its underlying mechanism remains insufficiently understood. This study investigates high-silicon aluminum alloy by combining turning experiments with molecular dynamics simulations to elucidate the origin and evolution of damage under different energy fields, establishing a correlation between microscopic processes and observable defects. In conventional turning, damage propagation is driven by particle accumulation and dislocation interlocking. Ultrasonic vibration softens the material and confines plastic deformation to the near-surface region, although excessively high transient peaks can lead to process instability. Laser remelting turning disperses stress within the remelted layer, significantly inhibiting defect expansion, but its effectiveness is highly sensitive to variations in cutting depth. The hybrid approach, laser remelting ultrasonic vibration turning, leverages the dispersion buffering effect of the remelted layer and the localized plastic deformation from ultrasonication to reduce peak loads, control deformation depth, and suppress defects, while simultaneously mitigating the depth sensitivity of damage and maintaining removal efficiency. This work clarifies the mechanism by which a composite energy field controls damage in the micro-cutting of high-silicon aluminum alloy, providing practical guidance for the high-quality machining of composite materials. Full article
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23 pages, 9932 KB  
Article
Explicit Crystal Plasticity Modeling of Texture Evolution in Nonlinear Twist Extrusion
by Ülke Şimşek, Hiroyuki Miyamoto and Tuncay Yalçınkaya
Crystals 2025, 15(11), 950; https://doi.org/10.3390/cryst15110950 - 2 Nov 2025
Viewed by 363
Abstract
The Nonlinear Twist Extrusion (NLTE) method, a novel severe plastic deformation (SPD) technique, aims to enhance grain refinement and achieve a more uniform plastic strain distribution. Grain size and its uniform distribution strongly influence the physical properties of metals. Therefore, predicting texture evolution [...] Read more.
The Nonlinear Twist Extrusion (NLTE) method, a novel severe plastic deformation (SPD) technique, aims to enhance grain refinement and achieve a more uniform plastic strain distribution. Grain size and its uniform distribution strongly influence the physical properties of metals. Therefore, predicting texture evolution during processing is essential for optimizing forming parameters and improving material performance. In this study, a rate-dependent crystal plasticity formulation is implemented in an explicit framework in Abaqus finite element software, based on a finite strain approach with multiplicative decomposition of the deformation gradient. Crystal plasticity finite element (CPFEM) simulations are conducted on single-crystal copper under boundary conditions representing the NLTE process. The influence of dynamic friction coefficients on texture evolution is systematically investigated, and the results are compared with experimental observations. The study provides new insights into deformation mechanisms during NLTE and highlights the strong correlation between texture development and forming parameters. Full article
(This article belongs to the Section Crystalline Metals and Alloys)
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14 pages, 5309 KB  
Article
Bimodal Microstructure and Strengthening Mechanisms of a Mg-RE Alloy Processed by Asymmetric Upsetting–Extrusion
by Nanjiang Chen, Bingchun Jiang, Yuze Xi, Lei Jing, Liwei Lu and Yiquan Li
Materials 2025, 18(21), 5001; https://doi.org/10.3390/ma18215001 - 1 Nov 2025
Viewed by 469
Abstract
This study successfully produced a magnesium alloy bar featuring a bimodal microstructure with high strength via an asymmetric upsetting–extrusion process. The evolution of microstructure, texture, and mechanical properties was systematically investigated using finite element simulation, room-temperature tensile tests, optical microscopy, scanning electron microscopy, [...] Read more.
This study successfully produced a magnesium alloy bar featuring a bimodal microstructure with high strength via an asymmetric upsetting–extrusion process. The evolution of microstructure, texture, and mechanical properties was systematically investigated using finite element simulation, room-temperature tensile tests, optical microscopy, scanning electron microscopy, and electron backscatter diffraction. Results demonstrate that the bimodal structure forms under the combined effects of shear deformation in the upsetting stage and low-speed, high-ratio deformation in the extrusion stage. This structure consists of coarse deformed grains containing high-density dislocations surrounded by fine dynamically recrystallized grains. A strong <10-10>//ED basal fiber texture also developed, which effectively suppresses basal slip. Continuous dynamic recrystallization was the primary grain refinement mechanism. The 370 °C extruded alloy achieved a high tensile strength of 457.9 MPa, but its elongation was limited to 3.96%. This combination of strength and ductility is attributed to the synergistic influence of the bimodal microstructure, strong basal texture, and high dislocation density. Full article
(This article belongs to the Section Metals and Alloys)
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19 pages, 4788 KB  
Article
Effect of Hardening Rate on the Bendability and Fracture Response of AA6082 Aluminum Extrusions in the VDA238-100 Tight Radius Bend Test
by Jacqueline Noder, Kenneth Cheong, Cliff Butcher, Paul Rometsch and Warren J. Poole
Metals 2025, 15(11), 1199; https://doi.org/10.3390/met15111199 - 28 Oct 2025
Viewed by 320
Abstract
Understanding the microstructure–property relationship in aluminum extrusions is crucial to leverage their potential in automotive lightweighting. The sensitivity of the processing history to the microstructure and through-thickness variations poses a major challenge since it leads to strong directionality in plasticity and fracture. Reliable [...] Read more.
Understanding the microstructure–property relationship in aluminum extrusions is crucial to leverage their potential in automotive lightweighting. The sensitivity of the processing history to the microstructure and through-thickness variations poses a major challenge since it leads to strong directionality in plasticity and fracture. Reliable characterization of the mechanical response under relevant stress states is crucial for the development of modeling strategies and performance ranking in alloy design. To this end, tensile and 3-point bend tests were performed for an aluminum extrusion produced on a laboratory-scale extrusion press at Rio Tinto Aluminium. Direct measurements of surface strains during bending using stereoscopic digital image correlation revealed that a larger bend angle in the VDA238-100 test does not necessarily imply a higher fracture strain. The T4 sample tested in the extrusion direction sustained a bend angle of 104° compared to 68° in T6 for the same nominal bend severity (ratio of sheet thickness to punch radius), despite comparable major fracture strains of 0.60 and 0.58, respectively. It is proposed that the work-hardening behavior governs the strain distribution on the outer bend surface. The higher hardening rate in the T4 condition helped distribute deformation in the bend zone more uniformly. This delayed fracture to larger bend angles since strain is accumulated at a lower rate. To assess whether the effect of the hardening behavior is manifest at a microstructural lengthscale, microcomputed tomography (μ-CT) scans were conducted on interrupted bend samples. The distribution and severity of damage in the form of cracks on the outer bend surface were distinct to the temper and thus the hardening rate. Full article
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21 pages, 6582 KB  
Article
Research on the Application of the Taguchi-TOPSIS Method in the Multi-Objective Optimization of Punch Wear and Equivalent Stress in Cold Extrusion Forming of Thin-Walled Special-Shaped Holes
by Zhan Liu, Yuhong Yuan and Quan Wu
Metals 2025, 15(11), 1192; https://doi.org/10.3390/met15111192 - 26 Oct 2025
Viewed by 406
Abstract
In the cold extrusion forming of thin-walled, specially shaped holes in aviation motor brush boxes, non-uniform metal flow can easily induce local stress concentrations on the punch, thereby accelerating wear. Reducing the punch wear and equivalent stress is therefore critical for ensuring the [...] Read more.
In the cold extrusion forming of thin-walled, specially shaped holes in aviation motor brush boxes, non-uniform metal flow can easily induce local stress concentrations on the punch, thereby accelerating wear. Reducing the punch wear and equivalent stress is therefore critical for ensuring the forming quality of such thin-walled features and extending the service life of the mold. In this study, a slender punch with a specially shaped cross-section was selected as the research object. The Deform-3D Ver 11.0 software, incorporating the Archard wear model, was employed to investigate the effects of five process parameters—extrusion speed, punch cone angle, punch transition filet, friction coefficient, and punch hardness—on the wear depth and equivalent stress of the punch during the compound extrusion process. A total of 25 orthogonal experimental groups were designed, and the simulation results were analyzed using the Taguchi method combined with range analysis to determine the optimal parameter combination. Subsequently, a multi-objective correlation analysis of the signal-to-noise ratios for wear depth and equivalent stress was conducted using the TOPSIS approach. The analysis revealed that the optimal combination of process parameters was an extrusion speed of 12 mm·s−1, a punch cone angle of 50°, a punch transition filet radius of 1.8 mm, a friction coefficient of 0.12, and a punch hardness of 55 HRC. Compared with the initial process conditions, the integrated application of the Taguchi–TOPSIS method reduced the punch wear depth and equivalent stress by 21.68% and 42.58%, respectively. Verification through actual production confirmed that the wear conditions of the primary worn areas were in good agreement with on-site production observations. Full article
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21 pages, 6101 KB  
Article
The Mechanism of Microstructure Refinement and the Synergistic Strength–Ductility Enhancement in Al–Zn–Mg–Cu Alloys Processed by Continuous Rheo-Extrusion
by Ziren Wang, Jiazhi An, Mei Xu, Haixia Zhang, Guoli Wei, Chengliang Yang, Zhenpeng Wei, Wenzheng Shen and Wanwu Ding
Metals 2025, 15(11), 1167; https://doi.org/10.3390/met15111167 - 23 Oct 2025
Viewed by 317
Abstract
Al–Zn–Mg–Cu alloys are well known for their outstanding strength, toughness, and corrosion resistance, arising from the balanced addition of Mg, Zn, and Cu. However, conventional casting methods often lead to grain boundary segregation and the formation of coarse Fe-rich phases, which severely limit [...] Read more.
Al–Zn–Mg–Cu alloys are well known for their outstanding strength, toughness, and corrosion resistance, arising from the balanced addition of Mg, Zn, and Cu. However, conventional casting methods often lead to grain boundary segregation and the formation of coarse Fe-rich phases, which severely limit subsequent heat treatment and plastic processing. To overcome these drawbacks, this study systematically investigates the effects of the Continuous Rheo-Extrusion (CRE) process on the microstructure and mechanical performance of Al–Zn–Mg–Cu alloys using XRD, EBSD, SEM, and TEM analyses. The CRE process refines the average grain size from 53.5 μm to 16.1 μm and raises the fraction of high-angle grain boundaries to 88.8%. Moreover, coarse Fe-rich phases are fragmented to below 5 μm, while the elemental distribution of Zn, Mg, and Cu becomes more homogeneous, effectively reducing grain boundary segregation. The Al2Cu precipitates are refined from 106.3 nm to 11.7 nm, corresponding to an 88.9% size reduction. These microstructural optimizations yield a remarkable increase in tensile strength (from 204.7 ± 23.7 MPa to 338.0 ± 9.3 MPa) and elongation (from 11.4 ± 2.4% to 13.8 ± 1.3%). Quantitative analysis confirms that dislocation and precipitation strengthening are the dominant contributors to this improvement. Overall, the CRE process enhances microstructural uniformity through the synergistic effects of shear deformation, continuous dynamic recrystallization (CDRX), and dynamic precipitation, thereby providing a solid theoretical and practical foundation for short-process fabrication of high-strength, high-ductility Al–Zn–Mg–Cu alloys. Full article
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28 pages, 11028 KB  
Article
Effectiveness of Advanced Support at Tunnel Face in ADECO-RS Construction
by Xiaoyu Dou, Chong Xu, Jiaqi Guo, Xin Huang and An Zhang
Buildings 2025, 15(20), 3744; https://doi.org/10.3390/buildings15203744 - 17 Oct 2025
Viewed by 306
Abstract
Tunnel construction in weak and fractured strata often faces risks such as tunnel face instability and large deformation of surrounding rock, which are difficult to effectively control using conventional support methods. Based on the engineering background of the No. 8# TA Tunnel in [...] Read more.
Tunnel construction in weak and fractured strata often faces risks such as tunnel face instability and large deformation of surrounding rock, which are difficult to effectively control using conventional support methods. Based on the engineering background of the No. 8# TA Tunnel in the F3 section of Georgia’s E60 Highway, this study employed ADECO-RS and developed a 3D numerical model with finite difference software to simulate full-face tunnel excavation process. The influence of advanced reinforcement measures on the stability of the surrounding rock was systematically investigated. The control effectiveness of different advanced reinforcement schemes was evaluated by comparing the displacement field, stress field, and plastic zone distribution of the surrounding rock under three conditions: no support, advanced pipe roof support, and a combination of pipe roof and glass fiber bolts. A comprehensive quantitative analysis of the synergistic effect of the combined reinforcement was also performed. The results indicated that significant extrusion deformation of the tunnel face and vault settlement occurred after excavation. The pressure arch developed within a range of 17.5 to 22 m above the tunnel vault. The surrounding rock of this tunnel was classified as type B (short-term stable). Deformation primarily occurred within one tunnel diameter ahead of the face, with the deformation rate significantly reduced after support. Advanced pipe roof support effectively restrained surrounding rock deformation, while the combination of advanced pipe roof and glass fiber bolts delivered better performance: reducing final convergence by 73.10%, pre-convergence by 82.69%, and face extrusion by 87.66%. The combined support also contracted the pressure arch boundaries from 17.5 to 22 m to 6–12.5 m, reduced the extent of major principal stress deflection, and significantly shrinks the plastic zone. Glass fiber bolts played a key role in controlling plastic zone expansion and ensuring stability. This study provides theoretical and numerical references for safe construction and advanced support design in tunnels under complex geological conditions. Full article
(This article belongs to the Section Building Structures)
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21 pages, 6002 KB  
Article
Numerical Investigation on the Extrusion Process of Flexible Pipe Liners for Deep-Sea Mineral Transport
by Wanhai Xu, Congyan Meng, Shuangning You, Yexuan Ma and Yingying Wang
J. Mar. Sci. Eng. 2025, 13(10), 1970; https://doi.org/10.3390/jmse13101970 - 15 Oct 2025
Viewed by 367
Abstract
Flexible pipes have significant application potential in deep-sea mineral resource exploitation. As the innermost barrier of flexible pipes, the liner directly withstands abrasive wear from mineral particles. The extrusion quality of the liner is a decisive factor for the service life of the [...] Read more.
Flexible pipes have significant application potential in deep-sea mineral resource exploitation. As the innermost barrier of flexible pipes, the liner directly withstands abrasive wear from mineral particles. The extrusion quality of the liner is a decisive factor for the service life of the pipe and requires optimization of process parameters for improvement. However, the extrusion process of wear-resistant liners made of ultra-high molecular weight polyethylene (UHMWPE) involves complex thermo-mechanical coupling behavior, which creates major challenges in developing accurate numerical models that represent the entire process. To precisely simulate the extrusion process and guide process parameter optimization, this paper establishes a numerical simulation model for flexible pipe liner extrusion based on the Eulerian–Lagrangian coupling method. Simulations under various outlet temperature and screw speed conditions were carried out to reveal the evolution of mechanical behavior during extrusion and clarify the influence of key process parameters. The main conclusions can be summarized as follows. An increase in extrusion temperature reduces the maximum stress and promotes better molecular orientation and crystallinity in UHMWPE material, while the maximum heat flux remains essentially unchanged. An increase in screw speed has little effect on maximum material stress but leads to a significant increase in maximum heat flux. In addition, significant stress appears in the UHMWPE material at the extrusion die exit and is mainly concentrated in the unextruded material section. The numerical model effectively addresses the challenges of simulating material phase transition, large deformation and long-distance flow, which are difficult to capture with traditional methods. The findings offer a theoretical basis and technical guidance for optimizing extrusion process parameters and strengthening quality control in flexible pipe liner extrusion. Full article
(This article belongs to the Special Issue Safety Evaluation and Protection in Deep-Sea Resource Exploitation)
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15 pages, 2336 KB  
Article
Enhancing the Buckling Performance of Thin-Walled Plastic Structures Through Material Optimization
by Alexander Busch, Olaf Bruch and Dirk Reith
Polymers 2025, 17(19), 2697; https://doi.org/10.3390/polym17192697 - 7 Oct 2025
Viewed by 455
Abstract
Reducing material usage in plastic products is a key lever for improving resource efficiency and minimizing environmental impact. In thin-walled structures subjected to mechanical loading, material efficiency must be achieved without compromising structural performance. In particular, resistance to buckling, a critical failure mode, [...] Read more.
Reducing material usage in plastic products is a key lever for improving resource efficiency and minimizing environmental impact. In thin-walled structures subjected to mechanical loading, material efficiency must be achieved without compromising structural performance. In particular, resistance to buckling, a critical failure mode, must be taken into account during product development. Due to the large number of design and process variables, many of which are interdependent, optimization approaches are uncommon in the blow-molded packaging industry. This paper presents a sensitivity-based optimization approach to improve buckling resistance by modifying the product’s material distribution. Since the sensitivity is nonlinear and depends on the product’s deformation state, various methods are developed and tested to reduce the frame-wise sensitivity data to a single sensitivity vector suitable for optimization. These methods are then tested on common extrusion blow-molded products, achieving improvements in buckling load of up to 60%. This approach is transferable to other thin-walled structures across various engineering domains, offering a pathway toward lightweight yet load-compliant designs. Full article
(This article belongs to the Special Issue Mechanical Behaviors and Properties of Polymer Materials, 2nd Edition)
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18 pages, 4842 KB  
Article
Positron Annihilation Studies of Hydrostatically Extruded AA1050 Aluminum
by Ewa Dryzek, Mirosław Wróbel, Maciej Sarnek and Jacek Skiba
Materials 2025, 18(18), 4428; https://doi.org/10.3390/ma18184428 - 22 Sep 2025
Viewed by 389
Abstract
AA1050 aluminum was hydrostatically extruded at room temperature to true strains of 0.9 and 3.2, and at cryogenic temperature to a true strain of 0.9. As a result of the extrusion process, the yield strength (YS) increased by 130–160% to 120–130 MPa, and [...] Read more.
AA1050 aluminum was hydrostatically extruded at room temperature to true strains of 0.9 and 3.2, and at cryogenic temperature to a true strain of 0.9. As a result of the extrusion process, the yield strength (YS) increased by 130–160% to 120–130 MPa, and the ultimate tensile strength (UTS) rose by 64–81% to 125–140 MPa. The hardness reached 46–49 HV. YS and UTS values correspond to mechanical properties typical of the H6 or H8 temper designations, with unusually high elongation at break ranging from 15% to 16.4%. Differences in lattice parameters, crystallite size, and lattice strain between samples deformed under various conditions—as well as those annealed after deformation—were within the margin of measurement uncertainty. This indicated that differences in defect density between the samples were relatively small, due to dynamic recovery occurring during extrusion. However, positron annihilation spectroscopy demonstrated that the cryo-cooled material extruded at a true strain of 0.9, as well as the one extruded at RT at a true strain of 3.2, exhibited significantly higher mean lattice defect concentrations compared to the sample extruded at RT at a true strain of 0.9. The predominant defects detected were vacancies associated with dislocations. The extrusion parameters also significantly affected the crystallographic texture. In particular, they altered the relative proportions of the <111> and <100> components in the axial texture, with the <100> component becoming dominant in cryogenically extruded samples. This trend was further intensified during recrystallization, which enhanced the <100> component even more. Recrystallization of the deformed materials occurred in the temperature range of 520–570 K. The activation energy for grain boundary migration during recrystallization was estimated to be approximately 1.5 eV. Full article
(This article belongs to the Section Metals and Alloys)
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13 pages, 10178 KB  
Article
Non-Free Cutting Mechanism of Asymmetrical Nanogrooves Under Chip-Removal Interference in Amorphous Nickel Phosphorus
by Yupeng He, Yingzhao Cai, Minkun Huang, Benshuai Ruan, Peng Liu and Tianfeng Zhou
Micromachines 2025, 16(9), 1059; https://doi.org/10.3390/mi16091059 - 18 Sep 2025
Viewed by 451
Abstract
Asymmetrical nanogrooves are commonly employed as blazed gratings for precision measurement, optical communication, and optical sensing applications. Diamond cutting is a promising deterministic processing technology for nanogrooves with a triangular cross-section profile. Non-free cutting of nanogrooves makes it hard to suppress the cutting-caused [...] Read more.
Asymmetrical nanogrooves are commonly employed as blazed gratings for precision measurement, optical communication, and optical sensing applications. Diamond cutting is a promising deterministic processing technology for nanogrooves with a triangular cross-section profile. Non-free cutting of nanogrooves makes it hard to suppress the cutting-caused deformation because of the low stiffness of nanogrooves. Focusing on the influence of non-free cutting on the deformation of asymmetrical nanogrooves, this paper systematically investigates the asymmetrical nanogroove cutting in amorphous nickel phosphorous material through mechanism revelation, simulation analysis, and experimental discussion. The materials removal mechanism by two side edges with different slopes in the non-free cutting is revealed according to the shear interference. According to the relative feed direction between tool and workpiece, two types of feed cases in the asymmetrical nanogrooves, named D1 and D2, respectively, are investigated by comparison in terms of deformation mechanism, nanogrooves topography, and nodal stress of tool edges. The extrusion by tool edges and the squeeze by the chip flow mainly influence the deformation of nanogrooves. In the D1 case, the horizontal component of squeeze by the chip flow towards the rear just-fabricated nanogroove, and the severely deformed nanogrooves are stacking together. On the contrary, in the D2 case, the flowing chip squeezes the front uncut materials, relieving the cutting-caused deformation, and asymmetrical nanogrooves have clear V-shaped cross-section profiles. It is proven that the D2 strategy is more suitable for asymmetrical nanogroove machining. The work in this paper will contribute to further understanding of non-free cutting and the processing technology of asymmetrical nanogrooves. Full article
(This article belongs to the Special Issue Ultra-Precision Micro Cutting and Micro Polishing)
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