Search Results (99)

Laser welding, a vital process in modern industry, offers significant technical and economic benefits, including improved part quality, precision, productivity, and cost reduction. This study significantly enhances our understanding of heat-treatable weldability (AA2024, AA2017, AA6061) and non-heat-treatable AA5083 aluminum alloys. It establishes a “weldability window” based on power density and interaction time, identifying three key domains: insufficient penetration, full penetration with regular weld, and irregular weld or cutoff. The study’s findings reveal that heat-treatable alloys soften in the fusion zone due to the dissolution of reinforcing precipitates during welding. In contrast, non-heat-treatable alloys exhibit hardening due to a fine dendritic microstructure. The fusion zone features fine dendrites, and in the heat-affected zone (HAZ), coarse particles and liquation at the fusion line are observed, particularly in AA6061 and 2024 alloys. The study also shows that the joint efficiency, a measure of the weld’s load-bearing capacity, is approximately 90% for the AA5083 alloy and 80% for the heat-treatable alloys. These findings significantly contribute to our understanding of welding processes. They can be used to optimize laser welding processes, thereby ensuring the production of high-quality and reliable joints in industrial applications. Full article

AlSi10Mg has been one of the most studied and employed aluminum alloys for additive manufacturing via laser powder-bed fusion (L-PBF). The optimization of manufacturing parameters is important for reducing internal defects, including porosity and inadequate surface finishes. In addition, heat treatments, such as T6, are often applied to this alloy, but they degrade the characteristic microstructure obtained via L-PBF additive manufacturing—the fine cellular structures—which may, in turn, detrimentally affect the material’s properties. In this context, a new alternative to this treatment, direct aging (DA), has shown promise in improving the mechanical properties of AlSi10Mg parts produced via L-PBF, since it preserves the cellular microstructure, precipitating silicon-rich nanoparticles within the cells. Understanding how different temperatures and heat treatment times influence the microstructure and, consequently, the properties remains a field to be explored in order to optimize the treatment conditions and achieve better mechanical properties. Thus, the objective of this study was to evaluate the influence of manufacturing parameters and heat treatments on the microstructure and mechanical properties of AlSi10Mg alloy. The optimized manufacturing conditions were 300 W power, 800 mm/s scan speed, 30 µm layer thickness, and an argon atmosphere, which led to lower porosity and better finishing. Samples were heat-treated via DA at 150 °C and 170 °C for different times, as well as undergoing a T6 treatment (solution at 520 °C followed by aging at 150 °C and 170 °C). Initially, the aging curves show higher hardness values for the direct aging condition, compared to the T6 and as-built conditions, reaching a peak hardness of 195 HV for 6h of direct aging. In this way, it was followed with microstructural characterization, which demonstrated that DA maintained the fine cell microstructure of L-PBF and promoted the precipitation of Si nanoparticles, which certainly contributed to the increase in hardness compared to T6, which promoted a structure with coarser precipitates. DA at 170 °C for 6 h increased the tensile strength to 430 MPa, compared to the as-built condition, with a slight loss of ductility. Full article

Aluminum–Magnesium (Al–Mg) alloys undergo sensitization, i.e., the precipitations of β-phase (Al₂Mg₃) at the grain boundaries, when exposed to elevated temperature. This microstructural change increases the susceptibility of Al–Mg alloys to intergranular corrosion, exfoliation, and stress corrosion cracking. This study introduces a time-frequency analysis (TFA) technique to determine the frequency-dependent ultrasonic attenuation parameter and correlate the frequency-attenuation slope to the Degree of Sensitization (DoS) developed in heat-treated Al–Mg alloy samples. Broadband pitch-catch signal was generated using a laser ultrasonic testing (LUT) system, from which the narrowband pitch-catch signal at different frequencies can be digitally generated. The attenuation parameters of sensitized Al–Mg samples were determined from these narrowband pitch-catch signals using the primary pulse-first echo (PP-FE) method. By identifying the frequency range within which the attenuation parameter is linearly proportional to the frequency, the slopes of the frequency-attenuation relationship were determined and correlated with the DoS values of the sample plates. The experimental results validate that the frequency-attenuation slope has a higher sensitivity and lower scattering as compared to other conventional ultrasonic attenuation measurement techniques. Full article

The existing Al-Ce heat-resistant alloys are not extensively utilized in high-temperature applications due to their poor room-temperature mechanical properties. In this study, the Al-10Ce-3Mg-5Zn alloy was enhanced using hot extrusion and heat treatment. The as-extruded alloy exhibited bimodal intermetallic compounds and grain structures. Additionally, high-density microcracks and twins were observed in the micron-sized intermetallic compounds. Compared with the as-cast state, the as-extruded alloy demonstrated a higher ultimate tensile strength (UTS) of 317 MPa and better elongation of 11.0%. Numerous nano-sized T phases precipitated in the α-Al matrix after the heat treatment, contributing to a further rise in UTS (365 MPa). The high strength of the alloy is primarily due to its strong strain hardening capacity, fine grain strengthening, and precipitation strengthening effect. The change in elongation mainly results from the expansion of pre-existing microcracks, twin deformation, and microstructural refinement. The heat-treated alloys exhibited superior strength retention ratios at elevated temperatures (64% at 200 °C) compared to conventional heat-resistant aluminum alloys. The results of this paper indicate that hot extrusion and heat treatment are effective for developing heat-resistant Al-Ce alloys with high room-temperature strength, offering a simple process suitable for industrial production. Full article

Aluminum alloy hot stamping technology has quickly become a research hotspot for many scholars due to its ability to solve key challenges such as poor formability, large rebound, and low dimensional accuracy of aluminum alloy sheets at room temperature. This work systematically reviews the progress of Hot-Forming-Quenching (HFQ^®) technology and its optimization processes. The effects of key forming parameters are summarized, including temperature, forming rate, friction, and crimping force on the forming properties of aluminum alloys. Additionally, an ontological model of thermal deformation behavior and damage evolution during hot forming is analyzed. A multifactorial strength prediction model, integrating grain size and reinforcement mechanisms, is highlighted for its ability to accurately predict post-forming yield strength. To address the limitations of HFQ^®, optimization methods for solid solution and aging heat-treatment stages are categorized and evaluated, along with their advantages and disadvantages. Furthermore, the latest advancements in two innovative hot stamping processes (Low-Temperature Hot Form and Quench (LT-HFQ^®) and pre-hardened hot forming (PHF)) are reviewed. LT-HFQ^® improves formability by pre-cooling the sheet while maintaining solution treatment, while PHF utilizes pre-hardened aluminum alloys, enabling brief heating, forming, and quenching to significantly reduce cycle time while ensuring component strength. Finally, by summarizing current technological progress and challenges, future directions for aluminum alloy hot stamping are outlined, including advancements in forming processes, material modeling, and optimization through multidisciplinary collaboration and artificial intelligence to drive further innovation. Full article

Al 7075 alloy (AA7075) exhibits excellent strength yet poses significant challenges for additive manufacturing (AM) due to its complex composition and propensity for defects during rapid solidification. To address these issues, this study introduces a novel AA7075 containing a small amount of Si fabricated by selective laser melting (SLM). Despite concerns about reduced melt-pool stability at low Si content, the alloy was successfully processed into defect-minimized samples. Systematic evaluations of as-built and heat-treated (direct aging, solid-solution, T6) samples revealed distinct microstructural evolution and clear improvements in mechanical properties and corrosion resistance. Specifically, as-built and direct aging conditions showed high strength but limited ductility and pronounced galvanic corrosion due to inhomogeneous microstructures. Conversely, solid-solution and T6 treatments effectively homogenized the microstructure, significantly enhancing ductility and reducing corrosion susceptibility, with the T6-treated samples exhibiting the most balanced mechanical and electrochemical performance. By maintaining a favorable microstructural balance while minimizing Si-induced brittleness, the low-Si AA7075 demonstrates improved SLM processability and robust performance. These findings offer a new pathway for optimizing AM aluminum alloys through tailored heat treatments. Full article

This research study aims to evaluate the wear and corrosive behaviour of aluminum 6061 alloy hybrid metal matrix composites after reinforcing them with graphene (0.5, 1 wt.%) and boron carbide (6 wt.%) at varying weight percentages. The hybrid composites were processed through ball milling and powder compaction, followed by a microwave sintering process, and T6 temper heat treatment was carried out to improve the properties. The properties were evaluated and analyzed using FE-SEM, Pin-on-Disc tribometer, surface roughness, salt spray test, and electrochemical tests. The results were evaluated prior to and subsequent to the T6 heat-treatment conditions. The T6 tempered sample S1 (Al6061-0.5% Gr-6% B₄C) exhibits a wear rate of 0.00107 mm³/Nm at 10 N and 0.00127 mm³/Nm at 20 N for 0.5 m/s sliding velocity. When the sliding velocity is 1 m/s, the wear rate is 0.00137 mm³/Nm at 10 N and 0.00187 mm³/Nm at 20 N load conditions. From the Tafel polarization results, the as-fabricated (F) condition demonstrates an Ecorr of −0.789 and an Icorr of 3.592 µA/cm² and a corrosion rate of 0.039 mm/year. Transitioning to the T6 condition further decreases Icorr to 2.514 µA/cm², Ecorr value of −0.814, and the corrosion rate to 0.027 mm/year. The results show that an increase in the addition of graphene wt.% from 0.5 to 1 to the Al 6061 alloy matrix deteriorated the wear and corrosive properties of the hybrid matrix composites. Full article

The present study was performed on real-life I4-aluminum cylinder heads produced industrially by applying the lost foam technique to Al-Si-Mg alloys (356 and 357). This work, in addition, introduces a new Al-Cu alloys coded 220 alloy. The main aim of this study is to analyze the effects of liquid metal treatment on the hardness and tensile properties of such castings. The effects of liquid metal treatment (modification with 200 ppm Sr, grain refining with 150 ppm B and degassing using pure Ar) of the castings produced by the lost foam technique on the tensile strength and hardness properties were evaluated. Hydrogen plays an important role in the formation of porosity. At the same time, the foam mold leaves an impression on the casting surface taking the shape of fine holes. In addition, segregation of hydrogen occurs in front of the solidification front. Thus, the porosity is a combination of hydrogen level and the solidification rate. Gains of 17% and 24% are observed for the hardness and yield strength for alloy 357 compared to alloy 356, caused by the difference in their magnesium (Mg) contents in the sense that, in the T6 heat-treated condition, precipitates in the form of ultra-fine Mg₂Si phase particles are formed. The enhancement in the mechanical properties of the used alloy depends mainly of the volume fraction of the precipitated Mg₂Si particles. The hardness of alloy 220 increases by 18% and the yield strength by 15% compared to that measured for alloy 356. In this case, the hardening phase Al₂Cu is responsible for this increase. Thus, this study demonstrates that liquid metal treatments significantly enhance the hardness and yield strength of Al-Si-Mg and Al-Cu alloys, with the gain attributed to refined microstructures and reduced porosity. Full article

Friction surfacing (FS) is increasingly recognized as an advanced technique for coating similar and dissimilar materials, enabling superior joint quality through plastic deformation and grain refinement. This study investigates the deposition of AA6082-T651 alloy on a medium-carbon steel EN14B substrate using FS, with process parameters optimized, and the effect of axial load, rotational speed, and traverse speed on coating integrity. The optimal sample was subjected to heat treatment (HT) at 550 °C for 24, 36, and 48 h to further enhance mechanical properties. Comprehensive microstructural and mechanical analyses were performed on both heat-treated and non-heat-treated samples using optical microscopy (OM), field emission scanning electron microscopy (FESEM) with energy-dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD), microhardness testing, and micro-tensile techniques. The optimized sample was processed with a 6 kN axial load, a rotational speed of 2700 rpm, and a traverse speed of 400 mm/min, and demonstrated superior bond quality and enhanced mechanical properties. The highest interfacial hardness values, 138 HV0.1 were achieved for the sample annealed for 48 h, under an axial load of 6 kN. Annealing for 48 h significantly improved atomic bonding at the aluminum–steel interface, confirmed by the formation of Fe₃Al intermetallic compounds detected via FESEM-EDS and XRD. These compounds were the primary reason for the enhancement in the mechanical properties of the FS deposit. Furthermore, the interrelationship between process and thermal parameters revealed that a peak temperature of 422 °C, heat input of 1.1 kJ/mm, and an axial load of 6 kN are critical for achieving optimal mechanical interlocking and superior coating quality. The findings highlight that optimized FS parameters and post-heat treatment are critical in achieving high-quality, durable coatings, with improved interfacial bonding and hardness, making the process suitable for structural applications. Full article

Nickel–aluminum (NiAl) alloys appear to be remarkably resistant to heat and corrosion, and are used in heat-treatment furnaces. This study utilizes molecular dynamics simulations to explore the structural characteristics of a nickel–aluminum (NiAl) alloy at varying heating rates during the heating process. During the heating process, the temperature increases from 300 K to 4000 K, surpassing the melting point. The effect of the heating rate is varied at 93, 62, 46, and 37 K/ps. The findings indicate that both the potential energy and volume of the NiAl system rise as it undergoes heating. Moreover, at the temperature 4000 K, the local face-centered cubic (fcc) and hexagonal close-packed (hcp) structures in the NiAl exhibit variations depending on the heating rates. The results highlight the importance of accounting for heating rates in the structural evolution of NiAl showing their thermal behavior for high-temperature applications. Full article

This study investigates the influence of various heat treatment regimes on the structure and microhardness of the aluminum alloy AlSi10Mg processed by the L-DED method. The study considers heat treatment regimes for solid solution in the temperature range of 500−540 °C with holding times of 30–120 min, as well as artificial aging regimes in the temperature range of 160−190 °C with holding times of 4–8 h. As a result of studying the structure and mechanical properties of the heat-treated samples, it became clear that the optimal regime can be considered the regime of 500 °C for 30 min followed by 190 °C for 6 h. This regime leads to the formation of a uniform structure with the breakage of the eutectic network into separate spherical silicon inclusions. The microhardness in this case is 90 HV, which is 55% higher than the initial state. Using TEM, it was established that the reason for the increase in hardness is the formation of nanoscale inclusions β″ (Mg₅Si₆). Full article

Three lightweight aluminum-based complex concentrated alloys with chemical compositions that have not been previously studied were manufactured and studied: Al₅₂Mg_9.6Zn₁₆Cu_15.5Si_6.9 w.t.% or Al₆₃Mg₁₃Zn₈Cu₈Si₈ a.t.% (alloy A), Al₄₄Mg₁₈Zn₁₉Cu₁₉ w.t.% or Al₅₅Mg₂₅Zn₁₀Cu₁₀ a.t.% (alloy B), and Al₄₇Mg_21.4Zn₁₂Cu_9.7Si_9.7 w.t.% or Al_52.7Mg_26.6Zn_5.6Cu_4.6Si_10.4 a.t.% (alloy AM), with low densities of 3.15 g/cm³, 3.18 g/cm³ and 2.73 g/cm³, respectively. During alloy design, the CALPHAD method was used to calculate a variety of phase diagrams for the various chemical compositions and to predict possible phases that may form in the alloy. The CALPHAD methodology results showed good agreement with the experimental results. The potential of the designed alloys to be used in some industrial applications was examined by manufacturing them using standard industrial techniques, something that is a rarity in this field. The alloys were produced using an induction furnace and pour mold casting process, while industrial-grade raw materials were utilized. Heat treatments with different soaking times were performed in order to evaluate the possibility of improving the mechanical properties of the alloys. Alloys A and AM were characterized by a multiphase microstructure with a dendritic FCC-Al matrix phase and various secondary phases (Q-AlCuMgSi, Al₂Cu and Mg₂Si), while alloy B consisted of a parent phase T-Mg₃₂(Al,Zn)₄₉ and the secondary phases α-Al and Mg₂Si. The microstructure of the cast alloys did not appear to be affected by the heat treatments compared to the corresponding as-cast specimens. However, alterations were observed in terms of the elemental composition of the phases in alloy A. In order to investigate and evaluate the mechanical properties of the as-cast and heat-treated alloys, hardness testing along with electrical conductivity measurements were conducted at room temperature. Among the as-cast samples, alloy AM had the highest hardness (246 HV₄), while among the heat-treated ones, alloy A showed the highest value (256 HV₄). The electrical conductivity of all the alloys increased after the heat treatment, with the highest increase occurring during the first 4 h of the heat treatment. Full article

The influence of temperature on the precipitation evolution in different zones of friction stir welded (FSW) heat-treatable aluminum alloys has been well investigated. However, the role of plastic deformation in affecting precipitation transformations remains less explored. To isolate the contribution of these factors and specifically assess the role of plastic deformation, an approach combining numerical and physical modeling techniques was used. Welding temperature cycles in the FSW weld zones calculated by means of a 3D finite element model were accurately reproduced using a Gleeble instrument. This approach was implemented under two scenarios such as the reproduction of the influence of temperature alone, and the combined effects of temperature and thermally induced plastic strain. The precipitation states and hardness obtained from these controlled experiments were compared to those observed in actual friction stir welds, providing a deeper understanding of the influence mechanisms at play. The results revealed that deformation significantly influences precipitation formation in the stir zone of both 2024 and 6082 alloys, with this effect extending to the heat-affected zone in the case of the 2024 alloy. Full article

Li-ion batteries are at risk of explosions caused by fires, primarily because of the high energy density of Li ions, which raises the temperature. Battery cases are typically made of plastic, aluminum, or SAF30400. Although plastic and aluminum aid weight reduction, their strength and melting points are low. SAF30400 offers excellent strength and corrosion resistance but suffers from work hardening and low high-temperature strength at 700 °C. Additionally, Ni used for plating has a low current density of 25% international copper alloy standard (ICAS). SAF2507 is suitable for use as a Li-ion battery case material because of its excellent strength and corrosion resistance. However, the heterogeneous microstructure of SAF2507 after casting and processing decreases the corrosion resistance, so it requires solution heat treatment. To address these issues, in this study, SAF2507 (780 MPa, 30%) is solution heat-treated at 1100 °C after casting and coated with Ag (ICAS 108.4%) using physical vapor deposition (PVD). Ag is applied at five different thicknesses: 0.5, 1.0, 1.5, 2.0, and 2.5 μm. The surface conditions and electrochemical properties are then examined for each coating thickness. The results indicate that the PVD-coated surface forms a uniform Ag layer, with electrical conductivity increasing from 1.9% ICAS to 72.3% ICAS depending on the Ag coating thickness. This enhancement in conductivity can improve Li-ion battery safety on charge and use. This result is expected to aid the development of advanced Li-ion battery systems in the future. Full article

In this paper, the feasibility of an innovative solid-state recycling process for aluminum alloy AA6063 chips through direct rolling is studied, with the aim of offering an environmentally sustainable alternative to conventional recycling processes. Aluminum chips, produced by milling an AA6063 billet without the use of lubricants, were first compacted using a hydraulic press with a 200 kN load and subsequently heat-treated at 570 °C for 6 h. The compacted chips were directly hot-rolled through several successive passes at 490 °C. The bulk material underwent the same rolling schedule to allow comparison of the samples and assess the process, in terms of mechanical properties and microstructure. All the rolled samples were tested by tensile and microhardness tests, whereas the microstructure was observed by an optical microscope and the EBSD-SEM technique. The fracture surface of all tested samples was analyzed by SEM. Recycled samples exhibited good mechanical properties, comparable to those of the bulk material. In particular, the bulk material showed an ultimate tensile strength of 218 MPa, in contrast to 177 MPa for the recycled chips, and comparable elongation at break. This study demonstrates that direct rolling of compacted aluminum chips is both technically feasible and has environmental benefits, offering a promising approach for sustainable aluminum recycling in industrial applications within a circular economy framework. Full article