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Search Results (583)

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Keywords = high-power microwave

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21 pages, 6275 KB  
Article
Design of a Low-Cost Flat E-Band Down-Converter with Variable Conversion Gain
by Mehrdad Harifi-Mood, Mansoor Dashti Ardakani, Djilali Hammou, Emilia Moldovan, Bryan Hosein and Serioja O. Tatu
Sensors 2025, 25(17), 5492; https://doi.org/10.3390/s25175492 - 3 Sep 2025
Abstract
This paper presents the design and implementation of a wideband diode-based down-converter operating from 60 to 90 GHz with a variable flat conversion gain. The proposed down-converter is implemented utilizing the Miniature Hybrid-Microwave Integrated Circuit (MHMIC) technology. It is composed of a wideband [...] Read more.
This paper presents the design and implementation of a wideband diode-based down-converter operating from 60 to 90 GHz with a variable flat conversion gain. The proposed down-converter is implemented utilizing the Miniature Hybrid-Microwave Integrated Circuit (MHMIC) technology. It is composed of a wideband double-balanced mixer, a Local Oscillator (LO) chain, and a differential TransImpedance Amplifier (TIA) with a variable gain. The designed mixer uses a novel topology exhibiting minimum reflection and high isolation between the RF and LO ports across a wide operating frequency of 30 GHz. In this topology, two balanced detectors generate the differential IF signal with minimum reflection. The characteristic impedance (Z0) of the mixer is set to be 70.7Ω, to minimize trace widths to reduce the mutual coupling and increasing the bandwidth. The OPA 657 is the core of the designed differential TIA with a variable gain. In addition, the LO chain of the down-converter utilized a combination of an active (×2) and a passive (×3) multiplier to generate enough RF power in the desired frequency range. Also, a WR-12 waveguide to Substrate Integrated Waveguide (SIW) transition is designed for the RF and LO ports that operates through the E-band. The proposed down-converter demonstrates excellent performance, with a high isolation between RF and LO ports exceeding 22 dB and a maximum conversion gain of 5 dB, and a response with a variation of ±5 dB across the band. The proposed mixer exhibits a return loss of better than 10 dB at both RF and LO ports, and it consumes a power of 560 mW. Full article
(This article belongs to the Special Issue Recent Development of Millimeter-Wave Technologies)
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22 pages, 6251 KB  
Article
A Modulated Marx Generator Capable of Outputting Quasi-Square Waves
by Rupei Li, Zilong Pan, Xiang Zhou, Rong Chen and Xinbing Cheng
Electronics 2025, 14(17), 3517; https://doi.org/10.3390/electronics14173517 - 2 Sep 2025
Abstract
A pulse generator capable of outputting quasi-square-wave pulses at the hundred-nanosecond scale is designed. With the development of high-power microwaves, the pulse flat-top is required to be more and more stable. However, at the hundred-nanosecond scale, an equal-value pulse-forming network is prone to [...] Read more.
A pulse generator capable of outputting quasi-square-wave pulses at the hundred-nanosecond scale is designed. With the development of high-power microwaves, the pulse flat-top is required to be more and more stable. However, at the hundred-nanosecond scale, an equal-value pulse-forming network is prone to being affected by stray parameters in the output waveform. To meet this requirement, a Marx generator and an anti-resonant network is used as the pulse boosting component and the pulse modulation component, respectively. Taking advantage of the anti-resonant network’s fewer sections and good modulation effect, the output waveform of the Marx generator is improved. The modulation ability of two-section and three-section modulation networks on waveforms, the output characteristics of two-section modulation networks, and the effect of stray parameters on the modulation network are explored. The experimental results show that both networks were able to achieve a quasi-square waveform of 100 kV on a 50 Ω load. Compared to the two-section network (165 ns pulse width, 41 ns rise time, 54.54% waveform flatness), the proposed three-section network achieves a pulse width of 185 ns with faster rise time (25 ns) and better waveform flatness (63.78%). Both topologies generate 100 kV quasi-square pulses on 50 Ω loads, with the three-section design demonstrating superior waveform control. In the repetition experiment, the pulse power source achieved stable operation at a repetition frequency of 20 Hz, and a quasi-square waveform with an output voltage of 100 kV was obtained. Finally, compared with previous studies, the modulated Marx generator based on an anti-resonant network has better waveform modulation effect and fewer network sections when generating a Square wave pulse of 100–200 ns. Full article
(This article belongs to the Section Power Electronics)
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29 pages, 9470 KB  
Review
Millimeter-Wave Antennas for 5G Wireless Communications: Technologies, Challenges, and Future Trends
by Yutao Yang, Minmin Mao, Junran Xu, Huan Liu, Jianhua Wang and Kaixin Song
Sensors 2025, 25(17), 5424; https://doi.org/10.3390/s25175424 - 2 Sep 2025
Viewed by 37
Abstract
With the rapid evolution of 5G wireless communications, millimeter-wave (mmWave) technology has become a crucial enabler for high-speed, low-latency, and large-scale connectivity. As the critical interface for signal transmission, mmWave antennas directly affect system performance, reliability, and application scope. This paper reviews the [...] Read more.
With the rapid evolution of 5G wireless communications, millimeter-wave (mmWave) technology has become a crucial enabler for high-speed, low-latency, and large-scale connectivity. As the critical interface for signal transmission, mmWave antennas directly affect system performance, reliability, and application scope. This paper reviews the current state of mmWave antenna technologies in 5G systems, focusing on antenna types, design considerations, and integration strategies. We discuss how the multiple-input multiple-output (MIMO) architectures and advanced beamforming techniques enhance system capacity and link robustness. State-of-the-art integration methods, such as antenna-in-package (AiP) and chip-level integration, are examined for their importance in achieving compact and high-performance mmWave systems. Material selection and fabrication technologies—including low-loss substrates like polytetrafluoroethylene (PTFE), hydrocarbon-based materials, liquid crystal polymer (LCP), and microwave dielectric ceramics, as well as emerging processes such as low-temperature co-fired ceramics (LTCC), 3D printing, and micro-electro-mechanical systems (MEMS)—are also analyzed. Key challenges include propagation path limitations, power consumption and thermal management in highly integrated systems, cost–performance trade-offs for mass production, and interoperability standardization across vendors. Finally, we outline future research directions, including intelligent beam management, reconfigurable antennas, AI-driven designs, and hybrid mmWave–sub-6 GHz systems, highlighting the vital role of mmWave antennas in shaping next-generation wireless networks. Full article
(This article belongs to the Special Issue Millimeter-Wave Antennas for 5G)
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0 pages, 1396 KB  
Proceeding Paper
Wireless Power Harvesting Skin
by Ioannis Gavriilidis, Adamantios Karakilidis, Apostolos-Christos Tsafaras and Theodoros Kaifas
Eng. Proc. 2025, 104(1), 69; https://doi.org/10.3390/engproc2025104069 - 29 Aug 2025
Abstract
Contributing to the quest for renewable energy harvesting, we present, in the work at hand, a conceptual model of a large-scale wireless microwave power harvester that takes the structure of a smart reconfigurable harvesting surface. This structure is assembled by numerous elementary harvesters [...] Read more.
Contributing to the quest for renewable energy harvesting, we present, in the work at hand, a conceptual model of a large-scale wireless microwave power harvester that takes the structure of a smart reconfigurable harvesting surface. This structure is assembled by numerous elementary harvesters that, as a whole, present both wide solid angle coverage and high receiving antenna gain. This is achieved by employing two levels of organization, both in the horizontal and in the vertical planes. The horizontal plane, which is the host receiving surface, is tiled by employing square radiators and forms hierarchical subarray structures. At the same time, hieratical structures are also employed in the vertical plane where the beamforming network collects the received power in a drainage-basin fashion (one receiving port is fed by its assigned and also its neighboring antenna elements) achieving, in this way, increased efficiency. The presented results verify the contributed design. Full article
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25 pages, 7877 KB  
Article
Microwave Drying of Tricholoma Matsutake: Dielectric Properties, Mechanism, and Process Optimization
by Siyu Gong, Yifan Niu, Chao Yuwen and Bingguo Liu
Foods 2025, 14(17), 3054; https://doi.org/10.3390/foods14173054 - 29 Aug 2025
Viewed by 289
Abstract
Efficient drying is crucial for the preservation and high-value utilization of tricholoma matsutake (TM). Traditional hot-air drying is inefficient, energy-intensive, and prone to quality degradation. This study investigates the application of microwave drying for TM, systematically analyzing its dielectric properties and moisture states, [...] Read more.
Efficient drying is crucial for the preservation and high-value utilization of tricholoma matsutake (TM). Traditional hot-air drying is inefficient, energy-intensive, and prone to quality degradation. This study investigates the application of microwave drying for TM, systematically analyzing its dielectric properties and moisture states, and elucidating the dielectric response mechanisms during drying. Response surface methodology (RSM) was employed to optimize key process parameters, including microwave power, drying time, and sample mass, and to validate the feasibility of the optimized process for industrial applications. Results revealed that the dehydration process of TM comprises three distinct stages, with free water evaporation contributing 69.8% of the total weight loss. Dielectric properties correlated strongly with apparent density and temperature, with the loss tangent (tanδ) increasing by 213.0% at higher temperatures, confirming dipole loss as the primary heating mechanism. Under optimized drying conditions (power: 620.00 W, time: 2.70 min, mass: 13.2 g), a dehydration rate (DR) of 85.41% was achieved, with a 1.50% deviation from the model-predicted values. The optimized process effectively maintained the relative integrity of the microstructure of TM, with the C/O ratio increasing from 1.03 to 1.31. Steam pressure-driven moisture migration was identified as the primary mechanism facilitating microwave-enhanced dehydration. Pilot-scale experiments scaled up the processing capacity to 15 kg/h and confirmed that the new process reduced total costs by 38% compared to traditional hot-air drying. The study developed an efficient and reliable microwave drying model, supporting industrial-scale TM processing. Full article
(This article belongs to the Section Food Engineering and Technology)
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24 pages, 7836 KB  
Article
Experimental Investigation into the Law of Rock Breaking Through the Combination of Microwave Irradiation and Cutting Tools Under Multiple Conditions
by Xiang-Xin Su, Zheng-Wei Li, Yang-Yi Zhou and Shi-Ping Li
Buildings 2025, 15(17), 3082; https://doi.org/10.3390/buildings15173082 - 28 Aug 2025
Viewed by 260
Abstract
Microwave irradiation of rocks can reduce the strength of rocks and ease their subsequent excavation. Exploring the combination of microwave and cutting tools for rock breaking under different conditions is important to the practical engineering application of microwaves. Based on a true triaxial [...] Read more.
Microwave irradiation of rocks can reduce the strength of rocks and ease their subsequent excavation. Exploring the combination of microwave and cutting tools for rock breaking under different conditions is important to the practical engineering application of microwaves. Based on a true triaxial microwave-assisted dual-mode mechanical rock-breaking test system, high-power microwave irradiation of rocks was investigated under different true triaxial stresses, durations of microwave irradiation, and cutting tool conditions such as mechanical drilling tools and tunnel boring machine (TBM) hobs. This research provides important data support for improving the rock-breaking efficiency of mine mining and tunneling as well as mechanical cutting tools and TBM hobs. In this experiment, Chifeng basalt with a relatively high strength was adopted as the research object. A 15 kW (2.45-GHz) open high-power microwave device was used to irradiate 200 mm × 200 mm × 200 mm cubic Chifeng basalt samples under conditions of different burial depths, and a cone drill bit was used for staged excavation. After microwave irradiation of Chifeng basalt measuring 400 mm × 400 mm × 400 mm, a 4-inch (102 mm) rotary cutter was employed to conduct round-by-circle cutting and rock-breaking tests in the microwave irradiation area. The results show that under true triaxial stress, the law of rock breaking by microwave irradiation combined with cone drill bits is as follows: the cutting force shows a trend of increasing–decreasing–increasing again–decreasing again. After microwave irradiation combined with hob cutting, the effective range of the influence of the hob is within the third cutting circle, with a range of diameters of approximately 200 mm. The results also indicate that the open microwave device can pre-crack rocks under deep stress, and there is obvious crack propagation. This research has good applicability to microwave-combined cantilever road-headers and TBM as well as in the mining field, and has a promising development prospect. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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12 pages, 3228 KB  
Communication
Green and Efficient Lithium Extraction from Spent NCM Batteries via Electromagnetic Radiation
by Ling Tong, Gui-Rong Zhang, Da-Shuai Li, Xing-Yu Huang, Yuan-Long Liu and Yan-Qing Cheng
Materials 2025, 18(17), 3975; https://doi.org/10.3390/ma18173975 - 25 Aug 2025
Viewed by 513
Abstract
The conventional recycling of spent lithium-ion batteries (LIBs) is hindered by high energy consumption and severe environmental pollution. In this study, a novel method utilizing high-frequency electromagnetic radiation was proposed to process the black mass derived from spent NCM-LIBs, significantly reducing both energy [...] Read more.
The conventional recycling of spent lithium-ion batteries (LIBs) is hindered by high energy consumption and severe environmental pollution. In this study, a novel method utilizing high-frequency electromagnetic radiation was proposed to process the black mass derived from spent NCM-LIBs, significantly reducing both energy consumption and chemical reagent usage. Conductive carbon black was introduced as an electromagnetic-wave-absorbing additive to improve the electromagnetic energy into thermal energy conversion efficiency during electromagnetic radiation. As a result, the decomposition and reduction of NCM materials can be completed within just 10 min at a microwave power of 500 W. Following electromagnetic irradiation, lithium was efficiently extracted via simple water leaching, achieving an extraction efficiency of 88.24%. Furthermore, a microwave heating device based on traveling-wave propagation was developed. Unlike conventional small-scale microwave systems that employ resonant cavities, this design enables improved heating uniformity, higher efficiency, and greater scalability for industrial microwave-assisted chemical processes. Full article
(This article belongs to the Special Issue Recycling and Electrode Materials of Lithium Batteries)
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16 pages, 1328 KB  
Article
Low-Frequency Noise Characteristics of Graphene/h-BN/Si Junctions
by Justinas Glemža, Ingrida Pliaterytė, Jonas Matukas, Rimantas Gudaitis, Andrius Vasiliauskas, Šarūnas Jankauskas and Šarūnas Meškinis
Crystals 2025, 15(9), 747; https://doi.org/10.3390/cryst15090747 - 22 Aug 2025
Viewed by 451
Abstract
Graphene/h-BN/Si heterostructures show considerable potential for future use in infrared detection and photovoltaic technologies due to their adjustable electrical behavior and well-matched interfacial structure. The near-lattice match between graphene and hexagonal boron nitride (h-BN) enables the deposition of low-defect-density graphene on h-BN surfaces. [...] Read more.
Graphene/h-BN/Si heterostructures show considerable potential for future use in infrared detection and photovoltaic technologies due to their adjustable electrical behavior and well-matched interfacial structure. The near-lattice match between graphene and hexagonal boron nitride (h-BN) enables the deposition of low-defect-density graphene on h-BN surfaces. This study presents a thorough exploration of the low-frequency electrical noise behavior of graphene/h-BN/Si heterojunctions under both forward and reverse bias conditions at room temperature. Graphene nanolayers were directly grown on h-BN films using microwave plasma-enhanced CVD. The h-BN layers were formed by reactive high-power impulse magnetron sputtering (HIPIMS). Four h-BN thicknesses were examined: 1 nm, 3 nm, 5 nm, and 15 nm. A reference graphene/Si junction (without h-BN) prepared under identical synthesis conditions was also studied for comparison. Low-frequency noise analysis enabled the identification of dominant charge transport mechanisms in the different device structures. Our results demonstrate that grain boundaries act as dominant defects contributing to increased noise intensity under high forward bias. Statistical analysis of voltage noise spectral density across multiple samples, supported by Raman spectroscopy, reveals that hydrogen-related defects significantly contribute to 1/f noise in the linear region of the junction’s current–voltage characteristics. This study provides the first in-depth insight into the impact of h-BN interlayers on low-frequency noise in graphene/Si heterojunctions. Full article
(This article belongs to the Special Issue Recent Advances in Graphene and Other Two-Dimensional Materials)
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19 pages, 4384 KB  
Article
Dynamic Temperature-Responsive MW Pulsing for Uniform and Energy-Efficient Plant-Based Food Drying
by Mohammad U. H. Joardder and Azharul Karim
Energies 2025, 18(16), 4391; https://doi.org/10.3390/en18164391 - 18 Aug 2025
Viewed by 324
Abstract
This study conducts a simulation-based approach to improve microwave (MW) convective drying using a temperature-responsive pulse ratio (TRPR) method. Traditional fixed-time pulse ratio (TimePR) techniques often result in uneven heating and reduced product quality due to uncontrolled temperature spikes. To address this, a [...] Read more.
This study conducts a simulation-based approach to improve microwave (MW) convective drying using a temperature-responsive pulse ratio (TRPR) method. Traditional fixed-time pulse ratio (TimePR) techniques often result in uneven heating and reduced product quality due to uncontrolled temperature spikes. To address this, a physics-based model was developed using COMSOL Multiphysics 6.3, executed on a high-performance computing (HPC) platform. The TRPR algorithm dynamically adjusts MW ON/OFF cycles based on internal temperature feedback, maintaining the maximum point temperature below a critical threshold of 75 °C. The model geometry, food materials (apple) properties, and boundary conditions were defined to reflect realistic drying scenarios. Simulation results show that TRPR significantly improves temperature and moisture uniformity across the sample. The TRPR method showed superior thermal stability over time-based regulation, maintaining a lower maximum COV of 0.026 compared to 0.045. These values are also well below the COV range of 0.05–0.26 reported in recent studies. Moreover, the TRPR system maintained a constant microwave energy efficiency of 40.7% across all power levels, outperforming the time-based system, which showed lower and slightly declining efficiency from 36.18% to 36.29%, along with higher energy consumption without proportional thermal or moisture removal benefits. These findings highlight the potential of the temperature-responsive pulse ratio (TRPR) method to enhance drying performance, reduce energy consumption, and improve product quality in microwave-assisted food processing. This approach presents a scalable and adaptable solution for future integration into intelligent drying systems. Full article
(This article belongs to the Section B: Energy and Environment)
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14 pages, 3884 KB  
Article
Microwave-Enhanced Catalytic Performance of Benzene Oxidation on MOF-Derived Mn/Ce-Co Oxides
by Shefeng Li, Pengyi Zhao, Ziyang Liu, Chang Wang, Linling Wang and Siyu Ding
Molecules 2025, 30(16), 3388; https://doi.org/10.3390/molecules30163388 - 15 Aug 2025
Viewed by 456
Abstract
Microwave-assisted processing has shown tremendous promise in accelerating chemical reactions and reducing energy consumption through targeted dielectric heating. This study develops MOF-derived Mn-Co and Ce-Co oxide catalysts for energy-efficient benzene oxidation via microwave catalysis. The MnCo spinel oxides (particularly MnCo11-400) exhibit superior microwave [...] Read more.
Microwave-assisted processing has shown tremendous promise in accelerating chemical reactions and reducing energy consumption through targeted dielectric heating. This study develops MOF-derived Mn-Co and Ce-Co oxide catalysts for energy-efficient benzene oxidation via microwave catalysis. The MnCo spinel oxides (particularly MnCo11-400) exhibit superior microwave absorption and catalytic activity due to enhanced oxygen mobility and tailored dielectric properties. Microwave irradiation enables rapid benzene mineralization over the MnCo11-400 catalyst, achieving 78% conversion at 30 W and complete conversion at 50 W, demonstrating exceptional energy efficiency at low power inputs. Microwaves significantly lower the reaction temperature compared to conventional thermal catalysis (ΔT = 100–250 °C). Stability tests confirm robustness over repeated power cycling (80% conversion retained after 3 × 1 h on/off cycles). Furthermore, an adsorption–microwave oxidation synergistic strategy is demonstrated: pre-adsorbed low-concentration benzene (1.15 mmol) at ambient temperature undergoes complete mineralization within 20 min under 30 W microwave irradiation. The intermittent microwave operation achieves equivalent benzene removal to continuous thermal processing while significantly reducing energy demand. This work establishes MOF-derived spinel oxides as high-performance microwave catalysts for low-temperature VOC abatement. Full article
(This article belongs to the Section Organometallic Chemistry)
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19 pages, 539 KB  
Article
Drying Kinetics and Physicochemical Characteristics of Dehydrated Jerusalem Artichoke (Helianthus tuberosus L.)
by Stanisław Rudy, Dariusz Dziki, Beata Biernacka, Renata Polak, Andrzej Krzykowski, Marek Domin, Grzegorz Rudzki and Magdalena Kachel-Górecka
Processes 2025, 13(8), 2553; https://doi.org/10.3390/pr13082553 - 13 Aug 2025
Viewed by 382
Abstract
Jerusalem artichoke (Helianthus tuberosus L.) is a valuable source of inulin and fructooligosaccharides—compounds with well-documented prebiotic and functional food properties. However, its high moisture content significantly limits storage stability. This study aimed to assess the effects of drying method and process temperature [...] Read more.
Jerusalem artichoke (Helianthus tuberosus L.) is a valuable source of inulin and fructooligosaccharides—compounds with well-documented prebiotic and functional food properties. However, its high moisture content significantly limits storage stability. This study aimed to assess the effects of drying method and process temperature on the drying kinetics and selected physicochemical properties of Jerusalem artichoke. Convective drying (AD) and combined convective–microwave drying (AMD), using a microwave power of 100 W, were employed. Drying was conducted at air temperatures of 40 °C, 60 °C, and 80 °C. Among the mathematical models evaluated, the Page model provided the best fit to the experimental drying data for both methods. Samples dried at 80 °C using the AMD technique exhibited the most pronounced changes in color, significant polyphenol losses, and a substantial reduction in antioxidant capacity compared to the fresh material. The lowest polyphenol degradation and the highest retention were observed in products dried at 40 °C using both AD and AMD methods. Notably, the AMD method significantly reduced drying time and improved the grindability of the dried Jerusalem artichoke samples. Although AMD contributed to certain quality deterioration, it also promoted a higher degree of particle size reduction. However, this increased degree of particle size reduction had only a limited effect on the extraction efficiency of fructooligosaccharides and inulin. The results of the present study suggest that AMD may serve as a competitive alternative to AD for drying Jerusalem artichoke, particularly when processing time and grindability are critical considerations. Full article
(This article belongs to the Special Issue Drying Kinetics and Quality Control in Food Processing, 2nd Edition)
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14 pages, 3367 KB  
Article
Realization of a 27.5 °C Atmospheric Microwave Plasma Jet at 8 W for Surface Modification of Thermosensitive Polymers
by Dongxue Han, Wencong Zhang, Yong Yang, Yuantao Huang, Jiangqi Yu, Li Wu, Wenyan Tian and Huacheng Zhu
Polymers 2025, 17(16), 2183; https://doi.org/10.3390/polym17162183 - 9 Aug 2025
Viewed by 472
Abstract
Atmospheric pressure plasma jets (APPJs) enable efficient solvent-free surface modification to enhance the wettability, adhesion, and biocompatibility of polymers. However, conventional APPJs often generate high temperatures and energetic particles, which lead to melting, surface degradation, and molecular damage of thermosensitive polymers, thus limiting [...] Read more.
Atmospheric pressure plasma jets (APPJs) enable efficient solvent-free surface modification to enhance the wettability, adhesion, and biocompatibility of polymers. However, conventional APPJs often generate high temperatures and energetic particles, which lead to melting, surface degradation, and molecular damage of thermosensitive polymers, thus limiting their scope of application. This study demonstrates an optimized atmospheric pressure microwave plasma jet (MPJ) operating at 8 W microwave power, achieving gas temperatures as low as 27.5 °C—only 2 °C above ambient. Direct skin contacts with the plasma jet for 150 s resulted in a maximum temperature of 35 °C without discomfort. In addition, the MPJ significantly enhances the surface hydrophilicity of TPU, PVC, and POM materials without causing damage. The designed MPJ has low gas temperature and good discharge stability, providing a new solution for plasma surface modification of thermosensitive materials. Full article
(This article belongs to the Special Issue Recent Progress in Surface Treatment for Polymer Materials by Plasmas)
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37 pages, 9111 KB  
Article
Conformal On-Body Antenna System Integrated with Deep Learning for Non-Invasive Breast Cancer Detection
by Marwa H. Sharaf, Manuel Arrebola, Khalid F. A. Hussein, Asmaa E. Farahat and Álvaro F. Vaquero
Sensors 2025, 25(15), 4670; https://doi.org/10.3390/s25154670 - 28 Jul 2025
Viewed by 528
Abstract
Breast cancer detection through non-invasive and accurate techniques remains a critical challenge in medical diagnostics. This study introduces a deep learning-based framework that leverages a microwave radar system equipped with an arc-shaped array of six antennas to estimate key tumor parameters, including position, [...] Read more.
Breast cancer detection through non-invasive and accurate techniques remains a critical challenge in medical diagnostics. This study introduces a deep learning-based framework that leverages a microwave radar system equipped with an arc-shaped array of six antennas to estimate key tumor parameters, including position, size, and depth. This research begins with the evolutionary design of an ultra-wideband octagram ring patch antenna optimized for enhanced tumor detection sensitivity in directional near-field coupling scenarios. The antenna is fabricated and experimentally evaluated, with its performance validated through S-parameter measurements, far-field radiation characterization, and efficiency analysis to ensure effective signal propagation and interaction with breast tissue. Specific Absorption Rate (SAR) distributions within breast tissues are comprehensively assessed, and power adjustment strategies are implemented to comply with electromagnetic exposure safety limits. The dataset for the deep learning model comprises simulated self and mutual S-parameters capturing tumor-induced variations over a broad frequency spectrum. A core innovation of this work is the development of the Attention-Based Feature Separation (ABFS) model, which dynamically identifies optimal frequency sub-bands and disentangles discriminative features tailored to each tumor parameter. A multi-branch neural network processes these features to achieve precise tumor localization and size estimation. Compared to conventional attention mechanisms, the proposed ABFS architecture demonstrates superior prediction accuracy and interpretability. The proposed approach achieves high estimation accuracy and computational efficiency in simulation studies, underscoring the promise of integrating deep learning with conformal microwave imaging for safe, effective, and non-invasive breast cancer detection. Full article
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27 pages, 1179 KB  
Article
Properties of Plant Extracts from Adriatic Maritime Zone for Innovative Food and Packaging Applications: Insights into Bioactive Profiles, Protective Effects, Antioxidant Potentials and Antimicrobial Activity
by Petra Babić, Tea Sokač Cvetnić, Iva Čanak, Mia Dujmović, Mojca Čakić Semenčić, Filip Šupljika, Zoja Vranješ, Frédéric Debeaufort, Nasreddine Benbettaieb, Emilie Descours and Mia Kurek
Antioxidants 2025, 14(8), 906; https://doi.org/10.3390/antiox14080906 - 24 Jul 2025
Viewed by 424
Abstract
Knowledge about the composition (volatile and non-volatile) and functionality of natural extracts from Mediterranean plants serves as a basis for their further application. In this study, five selected plants were used for the extraction of plant metabolites. Leaves and flowers of Critmum maritimum [...] Read more.
Knowledge about the composition (volatile and non-volatile) and functionality of natural extracts from Mediterranean plants serves as a basis for their further application. In this study, five selected plants were used for the extraction of plant metabolites. Leaves and flowers of Critmum maritimum, Rosmarinus officinalis, Olea europea, Phylliera latifolia and Mellisa officinalis were collected, and a total of 12 extracts were prepared. Extractions were performed under microwave-assisted conditions, with two solvent types: water (W) and a hydroalcoholic (ethanolic) solution (HA). Detailed extract analysis was conducted. Phenolics were analyzed by detecting individual bioactive compounds using high-performance liquid chromatography and by calculating total phenolic and total flavonoid content through spectrophotometric analysis. Higher concentrations of total phenolics and total flavonoids were obtained in the hydroalcoholic extracts, with the significantly highest total phenolic and flavonoid values in the rosemary hydroalcoholic extract (3321.21 mgGAE/L) and sea fennel flower extract (1794.63 mgQE/L), respectively; and the lowest phenolics in the water extract of olive leaves (204.55 mgGAE/L) and flavonoids in the water extracts of sea fennel leaves, rosemary, olive and mock privet (around 100 mgQE/L). Volatile organic compounds (VOC) were detected using HS-SPME/GC–MS (Headspace Solid-Phase Microextraction coupled with Gas Chromatography-Mass Spectrometry), and antioxidant capacity was estimated using DPPH (2,2-diphenyl-1-picrylhydrazyl assay) and FRAP (Ferric Reducing Antioxidant Power) methods. HS-SPME/GC–MS analysis of samples revealed that sea fennel had more versatile profile, with the presence of 66 and 36 VOCs in W and HA sea fennel leaf extracts, 52 and 25 in W and HA sea fennel flower extracts, 57 in rosemary W and 40 in HA, 20 in olive leaf W and 9 in HA, 27 in W mock privet and 11 in HA, and 35 in lemon balm W and 10 in HA extract. The lowest values of chlorophyll a were observed in sea fennel leaves (2.52 mg/L) and rosemary (2.21 mg/L), and chlorophyll b was lowest in sea fennel leaf and flower (2.47 and 2.25 mg/L, respectively), while the highest was determined in olive (6.62 mg/L). Highest values for antioxidant activity, determined via the FRAP method, were obtained in the HA plant extracts (up to 11,216 mgAAE/L for lemon balm), excluding the sea fennel leaf (2758 mgAAE/L) and rosemary (2616 mgAAE/L). Considering the application of these plants for fresh fish preservation, antimicrobial activity of water extracts was assessed against Vibrio fischeri JCM 18803, Vibrio alginolyticus 3050, Aeromonas hydrophila JCM 1027, Moraxella lacunata JCM 20914 and Yersinia ruckeri JCM 15110. No activity was observed against Y. ruckeri and P. aeruginosa, while the sea fennel leaf showed inhibition against V. fisheri (inhibition zone of 24 mm); sea fennel flower was active against M. lacunata (inhibition zone of 14.5 mm) and A. hydrophila (inhibition zone of 20 mm); and rosemary and lemon balm showed inhibition only against V. fisheri (inhibition zone from 18 to 30 mm). This study supports the preparation of natural extracts from Mediterranean plants using green technology, resulting in extracts rich in polyphenolics with strong antioxidant potential, but with no clear significant antimicrobial efficiency at the tested concentrations. Full article
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17 pages, 3269 KB  
Article
Microwave-Assisted Degradation of Azo Dyes Using NiO Catalysts
by Celinia de Carvalho Chan, Lamiaa F. Alsalem, Mshaal Almalki, Irina Bozhinovska, James S. Hayward, Stephen S. N. Williams and Jonathan K. Bartley
Catalysts 2025, 15(8), 702; https://doi.org/10.3390/catal15080702 - 24 Jul 2025
Cited by 1 | Viewed by 621
Abstract
Catalysts are ubiquitous in manufacturing industries and gas phase pollutant abatement but are not widely used in wastewater treatment, as high temperatures and concentrated waste streams are needed to achieve the reaction degradation rates required. Heating water is energy intensive, and alternative, low [...] Read more.
Catalysts are ubiquitous in manufacturing industries and gas phase pollutant abatement but are not widely used in wastewater treatment, as high temperatures and concentrated waste streams are needed to achieve the reaction degradation rates required. Heating water is energy intensive, and alternative, low temperature solutions have been investigated, collectively known as advanced oxidation processes. However, many of these advanced oxidation processes use expensive oxidants such as perchlorate, hydroxy radicals or ozone to react with contaminants, and therefore have high running costs. This study has investigated microwave catalysis as a low-energy, low-cost technology for water treatment using NiO catalysts that can be heated in the microwave field to drive the decomposition of azo-dye contaminants. Using this methodology for the microwave-assisted degradation of two azo dyes (azorubine and methyl orange), conversions of >95% were achieved in only 10 s with 100 W microwave power. Full article
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