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Molbank 2012, 2012(4), M784; doi:10.3390/M784
Short Note

3,5-Bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

 and *
Department of Chemistry, University of Cyprus, P.O. Box 20537, 1678 Nicosia, Cyprus
* Author to whom correspondence should be addressed.
Received: 24 September 2012 / Accepted: 7 November 2012 / Published: 8 November 2012
Download PDF [104 KB, 9 November 2012; original version 8 November 2012]

Abstract

3,5-Dichloro-4H-1,2,6-thiadiazin-4-one 1 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 4 (2.2 equiv.) and Pd(Ph3P)2Cl2 (5 mol%) in acetonitrile at ca. 82 °C to give 3,5-bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one 5 in 93% yield.
Keywords: 1,2,6-thiadiazines; thiophenes; heterocycles; oligomers 1,2,6-thiadiazines; thiophenes; heterocycles; oligomers
This is an open access article distributed under the Creative Commons Attribution License (CC BY) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Ioannidou, H.A.; Koutentis, P.A. 3,5-Bis(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one. Molbank 2012, 2012, M784.

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