Preliminary Study on Enzymatic-Based Cleaning of Cation-Exchange Membranes Used in Electrodialysis System in Red Wine Production
Abstract
:1. Introduction
2. Materials and Methods
2.1. Membranes
2.2. Enzymatic Agents
2.3. Chemicals
2.4. Protocols
2.5. Analysis
2.5.1. Ion-Exchange Capacity
2.5.2. Electric Conductivity
2.5.3. Contact Angle
3. Results and Discussion
3.1. Optimizing the Operating Conditions
3.2. Membrane Cleaning Using Three Enzymatic Solutions Successively and a Mixture of Two Compatible Enzymes
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Characteristics | CMX-Sb(n) | CMX-Sb(u) |
---|---|---|
IEC (mmol g−1) | 2.47 ± 0.13 | 1.40 ± 0.06 |
Tm (µm) | 177 ± 3 | 270 ± 4 |
κm (mS cm−1) | 13.4 ± 0.6 | 6.2 ± 0.4 |
θ (°) | 47 ± 1.3 | 49.3 ± 0.9 |
WC (%) | 26.1 ± 0.9 | 40.0 ± 2.1 |
f2 | 0.11 ± 0.01 | 0.04 ± 0.01 |
E (MPa) | 555 ± 11 | 264 ± 17 |
Rp (MPa) | 29 ± 3 | 11 ± 1 |
Cleaning Operations | Total Duration (h) | % κm (mS cm−1) | % IEC (mmol g−1) | % θ (°) |
---|---|---|---|---|
Rohalase® BXL | 20 | +45 | +23 | −16 |
Corolase® 7089 | 20 | +26 | +14 | −13 |
Tyrosinase® | 20 | +37 | +18 | −12 |
Successive cleanings | 30 (10 h/enzyme) | +50 | +33 | −15 |
Enzymes cocktail | 10 | +25 | +18 | −13 |
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Bdiri, M.; Bensghaier, A.; Chaabane, L.; Kozmai, A.; Baklouti, L.; Larchet, C. Preliminary Study on Enzymatic-Based Cleaning of Cation-Exchange Membranes Used in Electrodialysis System in Red Wine Production. Membranes 2019, 9, 114. https://doi.org/10.3390/membranes9090114
Bdiri M, Bensghaier A, Chaabane L, Kozmai A, Baklouti L, Larchet C. Preliminary Study on Enzymatic-Based Cleaning of Cation-Exchange Membranes Used in Electrodialysis System in Red Wine Production. Membranes. 2019; 9(9):114. https://doi.org/10.3390/membranes9090114
Chicago/Turabian StyleBdiri, Myriam, Asma Bensghaier, Lobna Chaabane, Anton Kozmai, Lassaad Baklouti, and Christian Larchet. 2019. "Preliminary Study on Enzymatic-Based Cleaning of Cation-Exchange Membranes Used in Electrodialysis System in Red Wine Production" Membranes 9, no. 9: 114. https://doi.org/10.3390/membranes9090114