Chemical Speciation of Aluminum in Wine by LC–ICP–MS
Abstract
:1. Introduction
2. Results and Discussion
2.1. Method Development for Speciation Analysis of Aluminum
2.2. Models vs. Standard Solution Analysis
2.2.1. Aluminum Fluoride Complexes
2.2.2. Aluminum Organic Complexes
2.2.3. Al/Citrate
2.2.4. Al/Oxalate
2.3. Wine Samples
2.3.1. Total Content of Aluminum, Fluorides, and Organic Ions
2.3.2. Speciation Analysis of Wine
3. Materials and Methods
3.1. Analytical System
3.2. Reagents and Standards
3.3. Total Content of Aluminum, Fluorides, and Organic Ions (Acetate, Citrate, Formate, and Oxalate)
3.4. Method Development for Speciation Analysis of Aluminum
3.4.1. Modeling and Model Solutions
3.4.2. pH Effect and Adjustment
3.5. Wine Samples
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Sample Availability: Samples of the compounds are available from the authors. |
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Karaś, K.; Zioła-Frankowska, A.; Frankowski, M. Chemical Speciation of Aluminum in Wine by LC–ICP–MS. Molecules 2020, 25, 1069. https://doi.org/10.3390/molecules25051069
Karaś K, Zioła-Frankowska A, Frankowski M. Chemical Speciation of Aluminum in Wine by LC–ICP–MS. Molecules. 2020; 25(5):1069. https://doi.org/10.3390/molecules25051069
Chicago/Turabian StyleKaraś, Katarzyna, Anetta Zioła-Frankowska, and Marcin Frankowski. 2020. "Chemical Speciation of Aluminum in Wine by LC–ICP–MS" Molecules 25, no. 5: 1069. https://doi.org/10.3390/molecules25051069