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Article

Thermal Treatment to Obtain 5-Hydroxymethyl Furfural (5-HMF), Furfural and Phenolic Compounds from Vinasse Waste from Agave

by
Miguel Angel Lorenzo-Santiago
1,
Jacobo Rodríguez-Campos
2,*,
Rodolfo Rendón-Villalobos
3,
Edgar García-Hernández
4,
Alba Adriana Vallejo-Cardona
5 and
Silvia Maribel Contreras-Ramos
1,*
1
Unidad de Tecnología Ambiental, Centro de Investigación y Asistencia en Tecnología y Diseño del Estado de Jalisco A.C. (CIATEJ), Normalistas No. 800, Colinas de la Normal, Guadalajara C.P. 44270, Jalisco, Mexico
2
Unidad de Servicios Analíticos y Metrológicos (CIATEJ), Normalistas No. 800, Colinas de la Normal, Guadalajara C.P. 44270, Jalisco, Mexico
3
Centro de Desarrollo de Productos Bióticos, Instituto Politécnico Nacional (IPN), Calle Ceprobi número 8, Colonia San Isidro C.P. 62731, Morelos, Mexico
4
Tecnológico Nacional de México, I.T. Zacatepec, Calzada Tecnológico No.27, Colonia Centro, Zacatepec C.P. 62780, Morelos, Mexico
5
Unidad de Biotecnología Médica y Farmacéutica, Centro de Investigación y Asistencia en Tecnología y Diseño del Estado de Jalisco A.C. (CIATEJ), Normalistas No. 800, Colinas de la Normal, Guadalajara C.P. 44270, Jalisco, Mexico
*
Authors to whom correspondence should be addressed.
Molecules 2023, 28(3), 1063; https://doi.org/10.3390/molecules28031063
Submission received: 21 December 2022 / Revised: 11 January 2023 / Accepted: 18 January 2023 / Published: 20 January 2023
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Abstract

Vinasses represent important final disposal problems due to their physical-chemical composition. This work analyzed the composition of tequila vinasses and increased 5-hydroxymethylfurfural, furfural, and phenolic compounds using thermal hydrolysis with hydrogen peroxide as a catalyst. A statistical Taguchi design was used, and a UPLC-MS (XEVO TQS Micro) analysis determined the presence and increase of the components. The treatment at 130 °C, 40 min, and 0.5% of catalyst presented the highest increase for 5-HMF (127 mg/L), furfural (3.07 mg/L), and phenol compounds as chlorogenic (0.36 mg/L), and vanillic acid (2.75 mg/L). Additionally, the highest removal of total sugars (57.3%), sucrose (99.3%), and COD (32.9%). For the treatment T130:30m:0P the syringic (0.74 mg/L) and coumaric (0.013 mg/L) acids obtained the highest increase, and the treatment T120:30m:1P increased 3-hydroxybenzoic (1.30 mg/L) and sinapic (0.06 mg/L) acid. The revaluation of vinasses through thermal treatments provides guidelines to reduce the impact generated on the environment.
Keywords: agro-industrial residues; phenolic compounds; furan derivatives; sugar transformation; tequila vinasse agro-industrial residues; phenolic compounds; furan derivatives; sugar transformation; tequila vinasse
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MDPI and ACS Style

Lorenzo-Santiago, M.A.; Rodríguez-Campos, J.; Rendón-Villalobos, R.; García-Hernández, E.; Vallejo-Cardona, A.A.; Contreras-Ramos, S.M. Thermal Treatment to Obtain 5-Hydroxymethyl Furfural (5-HMF), Furfural and Phenolic Compounds from Vinasse Waste from Agave. Molecules 2023, 28, 1063. https://doi.org/10.3390/molecules28031063

AMA Style

Lorenzo-Santiago MA, Rodríguez-Campos J, Rendón-Villalobos R, García-Hernández E, Vallejo-Cardona AA, Contreras-Ramos SM. Thermal Treatment to Obtain 5-Hydroxymethyl Furfural (5-HMF), Furfural and Phenolic Compounds from Vinasse Waste from Agave. Molecules. 2023; 28(3):1063. https://doi.org/10.3390/molecules28031063

Chicago/Turabian Style

Lorenzo-Santiago, Miguel Angel, Jacobo Rodríguez-Campos, Rodolfo Rendón-Villalobos, Edgar García-Hernández, Alba Adriana Vallejo-Cardona, and Silvia Maribel Contreras-Ramos. 2023. "Thermal Treatment to Obtain 5-Hydroxymethyl Furfural (5-HMF), Furfural and Phenolic Compounds from Vinasse Waste from Agave" Molecules 28, no. 3: 1063. https://doi.org/10.3390/molecules28031063

APA Style

Lorenzo-Santiago, M. A., Rodríguez-Campos, J., Rendón-Villalobos, R., García-Hernández, E., Vallejo-Cardona, A. A., & Contreras-Ramos, S. M. (2023). Thermal Treatment to Obtain 5-Hydroxymethyl Furfural (5-HMF), Furfural and Phenolic Compounds from Vinasse Waste from Agave. Molecules, 28(3), 1063. https://doi.org/10.3390/molecules28031063

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