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Short Note
Peer-Review Record

3-(3-Bromophenyl)-7-acetoxycoumarin

Molbank 2022, 2022(4), M1513; https://doi.org/10.3390/M1513
by Petri A. Turhanen 1,*, Liisa P. Nousiainen 2 and Juri M. Timonen 1,3,*
Reviewer 1: Anonymous
Reviewer 2: Anonymous
Molbank 2022, 2022(4), M1513; https://doi.org/10.3390/M1513
Submission received: 8 November 2022 / Revised: 23 November 2022 / Accepted: 25 November 2022 / Published: 2 December 2022

Round 1

Reviewer 1 Report

A straightforward contribution that is overall well-presented.

Note: I indicated that full characterization of the compound been not carried out simply because the X-ray structure of the compound is missing. Beyond that I just have a suggestion: Line 41: "gave rise" rather than "rose"?

 

Author Response

Please see the attachment.

Author Response File: Author Response.pdf

Reviewer 2 Report

This manuscript describes 3-(3-bromophenyl)-7-acetoxycoumarin, which is a new molecule, based on the well-known and robust approach for the synthesis coumarin. The product isolation was carried out without chromatography. This compound is of interest for the further construction of coumarin derivatives. The structure and purity of the molecule is confirmed by a complete set of spectral data. I recommend the manuscript for the publication in Molbank.

1) Reference for the review on 3-phenylcoumarins should be added (for example, 10.3390/molecules26216755).

2) Can the reaction be carried out without a microwave reactor?

Author Response

Please see the attachment.

Author Response File: Author Response.pdf

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