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Short Note
Peer-Review Record

3-(4-Bromophenyl)-1-carbamothioyl-5-(2-carbamothioylhydrazinyl)-4,5-dihydro-1H-pyrazole-5-carboxylic Acid

Molbank 2024, 2024(1), M1757; https://doi.org/10.3390/M1757
by Anastasia A. Andreeva, Maksim V. Dmitriev and Andrey N. Maslivets *
Reviewer 1: Anonymous
Molbank 2024, 2024(1), M1757; https://doi.org/10.3390/M1757
Submission received: 29 November 2023 / Revised: 18 December 2023 / Accepted: 19 December 2023 / Published: 2 January 2024
(This article belongs to the Collection Heterocycle Reactions)

Round 1

Reviewer 1 Report

Comments and Suggestions for Authors

The reviewed paper reports a simple synthesis of the new dihydropyrazole derivative 1. The manuscript is publishable; however, some corrections/additions are highly advisable.

The title product 1 is a chiral molecule, and accordingly, its NMR spectrum demonstrates the presence of the AB system for the diastereotopic methylene hydrogens (Supplementary Materials). On the other hand, the X-ray structure (Fig. 2) depicted one enantiomer only, while obviously a racemate was formed. This point should be clarified in the text.

Little correction: line 73: “and” should be placed instead of a Cyrillic letter: и

Comments on the Quality of English Language

No comments.

Author Response

Dear reviewer,

We have added a sentence: line 45, which tells about the formation of the racemate.

Corrected the letter in line 73

Thank you.

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