Study on Permeability Enhancement and Heat Transfer of Oil Sands Reservoir Based on Hydrophobic Nanofluids
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.1.1. Silica Nanoparticles and Nanofluid
2.1.2. Core
2.2. Experimental Method
2.2.1. Preparation of Nanofluids
- (1)
- Prepare or prepare base solution: NaCl solution with 3% mass fraction.
- (2)
- Weighing nanoparticles: Weigh the specified number of grams of nanoparticles and add them to the base solution prepared in advance, and then add a certain quality of cetyltrimethylammonium bromide solid particles.
- (3)
- Stirring: Stir slightly with a clean glass rod for 5 min to help the nanoparticles dissolve in the base solution.
- (4)
- Ultrasonic dispersion (Figure 1): Use an ultrasonic homogenizer (Figure 1b) to disperse for 2 h, the ultrasonic power is 240 W. The ultrasonic dispersion instrument model is SCIENTZ-1500F, manufactured by Ningbo Xinzhi Biotechnology Co., Ltd. (Ningbo, China) and the equipment is located at Northwest University, Xi’an City, Shaanxi Province, China. In order to avoid the overheating of ultrasonic, stop for 10 min after 15 min of ultrasonic each time to cool down the nanofluid naturally, complete the configuration after 8 times of ultrasonic, and then measure the PH value of the nanofluid with a PH meter. By interfering with the agglomeration and sedimentation of nanoparticles by ultrasound, dispersed and stable nanofluids can be obtained.
2.2.2. Triaxial Shear Seepage Experiment
- Axial force: 0–60 kN, measurement accuracy: ±1% (10–95% FS);
- Control mode:
- Equal strain control: 0.002–4 mm/min ± 10%;
- Equal stress control: 0 kN~60 kN, control accuracy ± 1%;
- Soil sample specifications: Φ101 × 200, Φ61.8 × 125, Φ39.1 × 80, Φ25 × 50 mm;
- Surrounding pressure: 0–1.99 MPa, control accuracy: ±0.5%FS, set value (0.01~1.95 MPa);
- Counter pressure: 0–0.99 MPa, control accuracy: ±0.5%FS, set value (0.01~0.99 MPa);
- Constant pressure difference control permeability;
- Constant flow permeation (0.02~30 mL/min);
- Volume change: 0–480 mL, digital display.
- (1)
- The oil sands cores were soaked in 3% NaCl solution and 0.05, 0.1, and 0.15 wt% nanofluids, respectively (Table 4).
- (2)
- According to the test requirements, be familiar with the functions of each valve of the instrument and the flow direction of the inlet and outlet liquid of the pipeline.
- (3)
- Determine the predetermined confining pressure value and pore pressure value of this test (Table 4).
- (4)
- Install the cores and energize each controller, and preheat for 10–20 min.
- (5)
- After the core is put into the pressure chamber (Figure 3), the confining pressure is raised to the specified value, the pore pressure is loaded to the specified value. After a period of consolidation, the permeability of the rock sample is tested, the permeability was tested by the steady-state method, and the differential pressure was 0.5 MPa following Darcy’s law. Then, the strain loading mode (loading rate of 0.1 mm/min) is used for triaxial compression after the permeability test is completed, and the loading is stopped when the axial strain is 3%, 6%, 9%, and 12%. The permeability of the rock sample is tested until the axial strain is 12%, the permeability test is completed, and the experiment is over. A total of five permeability tests are required.
2.2.3. Thermal Conductivity Experiment
3. Results and Discussion
3.1. Increased Permeability of Nanofluids
3.2. Increased Thermal Conductivity of Nanofluids
4. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Items | Metric Values |
---|---|
Appearance | White powder |
Silicon oxide content (%) | 98 |
Average particle size (nm) | 20 |
Specific surface area (m2/g) | ≥600 |
Core Number | Diameter (mm) | Length (mm) | Weight (g) | Density (g/cm3) | Volume (cm3) |
---|---|---|---|---|---|
1-1 | 25.18 | 52.3 | 47.04 | 1.81 | 26.03 |
1-2 | 25.1 | 52.4 | 47.04 | 1.82 | 25.91 |
1-3 | 25.02 | 52.36 | 47 | 1.83 | 25.73 |
1-4 | 25.04 | 51.8 | 44.03 | 1.73 | 25.50 |
1-5 | 25.06 | 52.8 | 47.03 | 1.81 | 26.03 |
1-6 | 25.1 | 53.2 | 46.71 | 1.78 | 26.31 |
1-7 | 25.02 | 52.5 | 46.47 | 1.80 | 25.80 |
1-8 | 25.16 | 53.02 | 46.96 | 1.78 | 26.35 |
Mineral Type | Non-Clay Minerals | |||||||
---|---|---|---|---|---|---|---|---|
Quartz | Feldspar | Dolomite | Calcite | Anhydrite | Plaster | Pyrite | Siderite | |
Mass Percentage (%) | 34.9 | 20.3 | 6.3 | 1.6 | 1.3 | 0.3 | 1.4 | 3.2 |
Mineral type | Clay minerals | |||||||
Aemon mixed layer | Illite | Kaolinite | Chlorite | |||||
Mass Percentage (%) | 1.5 | 9.8 | 8.3 | 11.1 |
Core Number | Nanofluid Concentration/wt% | Confining Pressure/MPa | Pore Pressure/MPa | Effective Confining/MPa |
---|---|---|---|---|
1 | 0 (3%NaCl) | 1 | 0.5 | 0.5 |
2 | 0 (3%NaCl) | 2 | 1 | 1 |
3 | 0.05 | 1 | 0.5 | 0.5 |
4 | 0.05 | 2 | 1 | 1 |
5 | 0.1 | 1 | 0.5 | 0.5 |
6 | 0.1 | 2 | 1 | 1 |
7 | 0.15 | 1 | 0.5 | 0.5 |
8 | 0.15 | 2 | 1 | 1 |
Technical Indicators | Parameters |
---|---|
Resolution | 0.005 W/(m·K) |
Measuring range | 0.001~10 W/(m·K) |
Repeatability | ±3% |
Accuracy | ±3% |
Temperature range | −160~150 °C |
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Gao, Y.; Chen, Z.; Liang, X.; Li, Y.; Shen, S.; Li, D.; Huang, Z. Study on Permeability Enhancement and Heat Transfer of Oil Sands Reservoir Based on Hydrophobic Nanofluids. Energies 2025, 18, 927. https://doi.org/10.3390/en18040927
Gao Y, Chen Z, Liang X, Li Y, Shen S, Li D, Huang Z. Study on Permeability Enhancement and Heat Transfer of Oil Sands Reservoir Based on Hydrophobic Nanofluids. Energies. 2025; 18(4):927. https://doi.org/10.3390/en18040927
Chicago/Turabian StyleGao, Yanfang, Zupeng Chen, Xuelin Liang, Yanchao Li, Shijie Shen, Dengke Li, and Zhi Huang. 2025. "Study on Permeability Enhancement and Heat Transfer of Oil Sands Reservoir Based on Hydrophobic Nanofluids" Energies 18, no. 4: 927. https://doi.org/10.3390/en18040927
APA StyleGao, Y., Chen, Z., Liang, X., Li, Y., Shen, S., Li, D., & Huang, Z. (2025). Study on Permeability Enhancement and Heat Transfer of Oil Sands Reservoir Based on Hydrophobic Nanofluids. Energies, 18(4), 927. https://doi.org/10.3390/en18040927