Structural and Optical Properties of Ag Nanoparticles Synthesized by Thermal Treatment Method
Abstract
:1. Introduction
2. Results
2.1. Mechanism of Ag Nanoparticles Formation via Thermal Treatment Method
2.2. Thermal Analysis (TGA–DTG Measurement)
2.3. Phase Composition Analysis (FTIR Spectrosscopy)
2.4. Elemental Composition Analysis (EDX Spectrosscopy)
2.5. Structural Analysis (X-ray Diffraction (XRD))
2.6. Morphology and Size Distribution (TEM Images for Ag Nanoparticles)
2.7. Optical Properties
3. Materials and Methods
4. Conclusions
Acknowledgments
Author Contributions
Conflicts of Interest
References
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Temperature (°C ) | 2θ (Deg.) ± 0.01 | FWHM (Deg.) ± 0.01 | DXRD (nm) | DTEM (nm) |
---|---|---|---|---|
400 | 38.09 | 1.70 | 5.16 | 7.88 ± 4.50 |
500 | 38.08 | 1.87 | 4.70 | 5.57 ± 1.75 |
600 | 38.08 | 2.04 | 4.30 | 4.61 ± 1.96 |
700 | 38.05 | 2.38 | 3.69 | 3.75 ± 2.23 |
800 | 38.04 | 2.40 | 3.65 | 3.29 ± 1.84 |
Temperature (°C) | DTEM (nm) | Absorbance Wavelength (nm) | Conduction Band (eV) by Equation (2) | Conduction Band (eV) by Equation (3) |
---|---|---|---|---|
400 | 7.88 ± 4.50 | 450 | 2.75 | 2.75 |
500 | 5.57 ± 1.75 | 441 | 2.81 | 2.81 |
600 | 4.61 ± 1.96 | 438 | 2.83 | 2.83 |
700 | 3.75 ± 2.23 | 420 | 2.95 | 2.95 |
800 | 3.29 ± 1.84 | 407 | 3.04 | 3.04 |
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Gharibshahi, L.; Saion, E.; Gharibshahi, E.; Shaari, A.H.; Matori, K.A. Structural and Optical Properties of Ag Nanoparticles Synthesized by Thermal Treatment Method. Materials 2017, 10, 402. https://doi.org/10.3390/ma10040402
Gharibshahi L, Saion E, Gharibshahi E, Shaari AH, Matori KA. Structural and Optical Properties of Ag Nanoparticles Synthesized by Thermal Treatment Method. Materials. 2017; 10(4):402. https://doi.org/10.3390/ma10040402
Chicago/Turabian StyleGharibshahi, Leila, Elias Saion, Elham Gharibshahi, Abdul Halim Shaari, and Khamirul Amin Matori. 2017. "Structural and Optical Properties of Ag Nanoparticles Synthesized by Thermal Treatment Method" Materials 10, no. 4: 402. https://doi.org/10.3390/ma10040402