Study on Preparation of Regenerated Cellulose Fiber from Biomass Based on Mixed Solvents
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Experimental Process Principle
2.3. All of Experimental Process Route
2.4. Experimental Process Conditions
2.5. Experimental Calculation Formula
2.5.1. Viscosity Analysis of Cupric Ammonia
2.5.2. α-Cellulose Analysis
2.5.3. Analysis of Pentosan Content
2.5.4. Reaction Performance Analysis
2.6. Data Processing
3. Results and Discussion
3.1. Preparation and Analysis of Arundo donax L. Pulp
3.2. Analysis of Indexes of Cellulose Dissolution Process
3.3. Performance Analysis of Cellulose Spinning Viscose Liquid
3.4. Analysis of Solidification Bath Process
3.5. Physical Property Analysis of Regenerated Cellulose Fiber from Biomass Arundo donax L.
3.6. Analysis of Antimicrobial Properties of Biomass-Regenerated Cellulose Fiber from Arundo donax L.
3.7. Analysis of Antiviral Properties of Biomass Regenerated Cellulose Fiber from Arundo donax L.
4. Conclusions
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
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Types | Value | |
---|---|---|
Ingredients | ||
holocellulose (%) | 72.98 ± 2.80 | |
α-cellulose (%) | 55.2 ± 0.7 | |
moisture (%) | 4.56 ± 0.17 | |
Benzene-alcohol extract (%) | 1.69 ± 0.13 | |
Lignin (%) | 20.03 ± 0.14 | |
Ash (%) | 3.56 ± 0.16 |
Types | Arundo donax L. Pulp | American COSMO Wood Pulp | South African (Broad-Leaved) Wood Pulp |
---|---|---|---|
α-cellulose (%) | 91.35 ± 0.15 | 91.15 ± 0.35 | 94.25 ± 0.15 |
moisture content (%) | 14.6 ± 0.2 | 7.2 ± 0.1 | 7.3 ± 0.1 |
Ash (%) | 0.11 ± 0.01 | 0.05 ± 0.02 | 0.04 ± 0.01 |
Iron content (PPM) | 13.0 ± 1.0 | 6.0 ± 1.0 | 5.5 ± 0.5 |
Cupric ammonia viscosity (mPa·S) | 8.4 ± 0.1 | 23.1 ± 0.7 | 11.5 ± 0.4 |
Whiteness (%) | 82.4 ± 0.4 | 93.8 ± 0.3 | 92.5 ± 0.5 |
Constant weight (g/m2) | 798.5 ± 5.5 | 728.0 ± 7.0 | 1011.0 ± 7.0 |
Alkali absorption value(%) | 607.0 ± 1.0 | 520.0 ± 2.0 | 539.5 ± 1.5 |
Middle big dust (one/kg) | 1.5 ± 0.1 | 0.0 ± 0.0 | 0.0 ± 0.0 |
Little dust (mm2/kg) | 74.0 ± 2.0 | 12.5 ± 0.5 | 13.0 ± 0.0 |
Pentose (%) | 4.28 ± 0.15 | 2.72 ± 0.06 | / |
Reactivity (s) | 15.5 ± 0.5 | 7.5 ± 0.5 | / |
Percentage of Arundo donax L. Pulp | Activation Time (h) | TH:DS | Defoaming Time (h) | Aromatic Polyoxyethylene Ether (mL/kg) |
---|---|---|---|---|
30~50% | 2~3 | 1:9 | 8~10 | (1~3)/(1~10) |
30~50% | 2~3 | 2:8 | 8~10 | (1~3)/(1~10) |
30~50% | 2~3 | 3:7 | 8~10 | (1~3)/(1~10) |
30~50% | 2~3 | 4:6 | 8~10 | (1~3)/(1~10) |
30~50% | 2~3 | 5:5 | 8~10 | (1~3)/(1~10) |
Test Item | Standard Antibacterial Value | Actual Value | Effect Evaluation |
---|---|---|---|
Escherichia coli (ATCC 6538) | ≥70% | >99% | with antimicrobial effect |
Staphylococcus aureus (ATCC 10231) | ≥70% | >99% | with antimicrobial effect |
Candida albicans (8099) | ≥60% | >99% | with antimicrobial effect |
Name of Experimental Virus | Antivirus Activity Value | Anti-Virus Activity Rate (%) | Effectiveness Evaluation |
---|---|---|---|
Influenza A virus H3N2 (ATCC VR-1679) | >4.85 | 99.99% | with antiviral effect |
Influenza A virus H1N1 (ATCC VR-1469) | >5.05 | 99.99% | with antiviral effect |
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Xiao, J.; Li, P.; Zhang, X.; Wang, X. Study on Preparation of Regenerated Cellulose Fiber from Biomass Based on Mixed Solvents. Materials 2024, 17, 819. https://doi.org/10.3390/ma17040819
Xiao J, Li P, Zhang X, Wang X. Study on Preparation of Regenerated Cellulose Fiber from Biomass Based on Mixed Solvents. Materials. 2024; 17(4):819. https://doi.org/10.3390/ma17040819
Chicago/Turabian StyleXiao, Junjiang, Pengcheng Li, Xiaotao Zhang, and Ximing Wang. 2024. "Study on Preparation of Regenerated Cellulose Fiber from Biomass Based on Mixed Solvents" Materials 17, no. 4: 819. https://doi.org/10.3390/ma17040819