UV-Light Mediated Biosynthesis of Silver Nanowires; Characterization, Dye Degradation Potential and Kinetic Studies
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Preparation of Psidium Guajava Seeds Extract
2.3. Synthesis of Silver Nanowires
2.4. Characterization of Ag Nanowire
2.5. Catalytic Potential of Ag-NWs
3. Results and Discussion
3.1. UV-Visible Analysis of Ag-NWs
3.2. FTIR Studies of Ag NWs
3.3. SEM analysis of Ag-NWs
3.4. XRD Analysis of Ag-NWs
3.5. Catalytic Potential of Ag-NWs
3.6. Kinetic Studies of Dye Degradation Reactions
3.6.1. Effect of Catalyst Dosage
3.6.2. Effect of MO Dye
4. Conclusions
5. Highlights
- UV-light-mediated green synthesis of Ag-NWs using Psidium guajava seed extract.
- Dimensions of Ag-NWs were 12–8 μm length and 200–500 nm diameter.
- Morphology of Ag-NWs was confirmed by SEM and XRD.
- Methyl orange dye degradation was achieved using Ag-NWs.
- Kinetics of degradation reaction was studied.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Sr. No. | Absorption Peaks | Functional Groups | References |
---|---|---|---|
1 | 3400–3300 cm−1 and 1600 cm−1 | —OH stretching of the alcohol and carboxylic acids | [49] |
2 | 2197 cm−1 and 1619 cm−1 | α, β-substituted unsaturated carbonyl | |
3 | 2161 cm−1 | iso-cyanate | |
4 | 2009 cm−1 | thio-cyanate | |
5 | 1735 cm−1 and 1647 cm−1 | ortho-substituted six-membered lactone | |
6 | 1430–1400 cm−1 | —OH bending of α, β-unsaturated carboxylic | |
7 | 1435 cm−1 | -C=C linkages |
Factor | Ag-NWs (mg/mL) | NaBH4 (mM) | MO Dye (mM) | kobs (min−1) | Half-Life Period (t1/2) R2 (min−1) |
---|---|---|---|---|---|
Ag-NWs | 0.60 | 17.6 | 0.082 | 0.1723 | 2.1032 0.98 |
1.28 | 17.6 | 0.082 | 0.1977 | 3.5053 0.98 | |
2.56 | 17.6 | 0.082 | 0.2003 | 3.4598 0.99 | |
3.84 | 17.6 | 0.082 | 0.2059 | 3.3657 0.99 | |
MO dye | 0.062 | 17.6 | 0.062 | 0.1825 | 3.7972 0.97 |
0.072 | 17.6 | 0.072 | 0.1872 | 3.7019 0.98 | |
0.082 | 17.6 | 0.082 | 0.1955 | 3.5447 0.99 | |
0.092 | 17.6 | 0.092 | 0.1592 | 4.3530 0.98 | |
0.102 | 17.6 | 0.102 | 0.1537 | 4.5087 0.97 |
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Ali, F.; Ali, Z.; Younas, U.; Ahmad, A.; Mooin-ud-din, G.; Pervaiz, M.; Luque, R.; Ahmad, I.; Ashraf, A.; Albaqami, M.D.; et al. UV-Light Mediated Biosynthesis of Silver Nanowires; Characterization, Dye Degradation Potential and Kinetic Studies. Sustainability 2021, 13, 13220. https://doi.org/10.3390/su132313220
Ali F, Ali Z, Younas U, Ahmad A, Mooin-ud-din G, Pervaiz M, Luque R, Ahmad I, Ashraf A, Albaqami MD, et al. UV-Light Mediated Biosynthesis of Silver Nanowires; Characterization, Dye Degradation Potential and Kinetic Studies. Sustainability. 2021; 13(23):13220. https://doi.org/10.3390/su132313220
Chicago/Turabian StyleAli, Faisal, Zahid Ali, Umer Younas, Awais Ahmad, Ghulam Mooin-ud-din, Muhammad Pervaiz, Rafael Luque, Ikram Ahmad, Adnan Ashraf, Munirah D. Albaqami, and et al. 2021. "UV-Light Mediated Biosynthesis of Silver Nanowires; Characterization, Dye Degradation Potential and Kinetic Studies" Sustainability 13, no. 23: 13220. https://doi.org/10.3390/su132313220