Bio-Composite Films Based on Carboxymethyl Chitosan Incorporated with Calcium Oxide: Synthesis and Antimicrobial Activity
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Methods
2.2.1. Synthesis of Carboxymethyl Chitosan
2.2.2. Synthesis of Calcium Oxide
2.2.3. Preparation of CMCH-CaO Bio-Composite Films
2.3. Characterizations
2.3.1. Chemical Structure
2.3.2. Morphology and Metal Composition
2.3.3. Crystal Structure
2.3.4. Thermal Stability
2.3.5. Mechanical Properties
2.3.6. Hydrophilic Property
2.3.7. Antimicrobial Activity
3. Results and Discussion
3.1. Chemical Structure of Synthesized CMCH and Synthesized CaO
3.2. Morphology of Synthesized CMCH and Synthesized CaO
3.3. XRD Pattern and Elements of Synthesized CaO
3.4. Chemical Structures of CMCH-CaO Bio-Composite Films
3.5. Morphology of CMCH-CaO Bio-Composite Films
3.6. Thermal Stability of CMCH-CaO Bio-Composite Films
3.7. Mechanical Properties of CMCH-CaO Bio-Composite Films
3.8. Hydrophilicity of CMCH-CaO Bio-Composite Films
3.9. Antimicrobial Activity of Synthesized CaO and CMCH-CaO Bio-Composite Films
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Data Availability Statement
Conflicts of Interest
References
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Samples | Tensile Strength (MPa) | Elongation at Break (%) |
---|---|---|
CMCH | 5.3 ± 0.4 | 76.0 ± 3.4 |
CMCH-CaO1% | 15.8 ± 0.8 | 59.2 ± 1.0 |
CMCH-CaO5% | 13.2 ± 0.8 | 79.1 ± 2.8 |
CMCH-CaO10% | 4.8 ± 0.2 | 49.1 ± 1.1 |
Samples | E. coli | S. aureus | ||
---|---|---|---|---|
Viable Cells (CFU/mL) | R (%) | Viable Cells (CFU/mL) | R (%) | |
CaO | N.D. | ≥99.9 | N.D. | ≥99.9 |
LDPE | 1.06 × 109 | - | 2.23 × 108 | - |
CMCH | 9.28 × 108 | 12.5 | 2.01 × 108 | 9.82 |
CMCH-CaO-1% | 1.87 × 108 | 82.4 | 5.56 × 107 | 75.1 |
CMCH-CaO-5% | 1.86 × 107 | 98.2 | 2.64 × 107 | 88.1 |
CMCH-CaO-10% | 1.32 × 107 | 98.8 | 1.82 × 108 | 91.8 |
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Thanakkasaranee, S.; Rachtanapun, P.; Rachtanapun, C.; Kanthiya, T.; Kasi, G.; Sommano, S.R.; Jantanasakulwong, K.; Seo, J. Bio-Composite Films Based on Carboxymethyl Chitosan Incorporated with Calcium Oxide: Synthesis and Antimicrobial Activity. Polymers 2024, 16, 2393. https://doi.org/10.3390/polym16172393
Thanakkasaranee S, Rachtanapun P, Rachtanapun C, Kanthiya T, Kasi G, Sommano SR, Jantanasakulwong K, Seo J. Bio-Composite Films Based on Carboxymethyl Chitosan Incorporated with Calcium Oxide: Synthesis and Antimicrobial Activity. Polymers. 2024; 16(17):2393. https://doi.org/10.3390/polym16172393
Chicago/Turabian StyleThanakkasaranee, Sarinthip, Pornchai Rachtanapun, Chitsiri Rachtanapun, Thidarat Kanthiya, Gopinath Kasi, Sarana Rose Sommano, Kittisak Jantanasakulwong, and Jongchul Seo. 2024. "Bio-Composite Films Based on Carboxymethyl Chitosan Incorporated with Calcium Oxide: Synthesis and Antimicrobial Activity" Polymers 16, no. 17: 2393. https://doi.org/10.3390/polym16172393