Microstructure and Shear Strength of SiC Joint Brazed with LiAlSiO4 Reinforced AgCuTi Composite Filler
Abstract
:1. Introduction
2. Materials and Methods
3. Results and Discussion
4. Conclusions
- (1)
- When brazing SiC joints with AgCuTi/LAS composite brazing filler, the typical structure of the joints is SiC/Ti5Si3/TiC + TiCu2 + TiO2 + LAS + LiAlSi2O6 + Cu(s, s) + Ag(s, s)/Ti5Si3/TiC/SiC.
- (2)
- The maximum shear strength of the joint at 900 °C for 10 min is 106.47 MPa when 1 wt% LAS is added. This value is 4.7 times greater than the condition without LAS. The Ag–Cu eutectic structure reduces in size and undergoes agglomeration with the extension of the holding time and the increase in the LAS addition.
- (3)
- According to theoretical calculations, the addition of LAS can effectively reduce residual stresses in the SiC brazed joints. The residual stress is reduced from −0.794 GPa to 1.3 × 10−5 GPa with 1 wt% LAS addition.
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
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Position | Ag | Cu | Ti | Si | C | Possible Phase |
---|---|---|---|---|---|---|
A | 1.90 | 2.33 | 56.06 | 30.10 | 9.60 | Ti5Si3 |
B | 0.75 | 2.36 | 48.53 | 3.48 | 44.88 | TiC |
C | 2.38 | 96.80 | 0.82 | - | - | Cu (s, s) |
D | 83.97 | 14.92 | 1.11 | - | - | Ag (s, s) |
Position | Ag | Cu | Ti | Si | C | Al | O | Possible Phase |
---|---|---|---|---|---|---|---|---|
A | 3.07 | 4.80 | 54.1 | 26.51 | 11.53 | - | - | Ti5Si3 |
B | 3.72 | 5.49 | 47.66 | 0.81 | 42.32 | - | - | TiC |
C | 1.38 | 94.91 | 1.79 | - | - | - | - | Cu (s, s) |
D | 81.37 | 16.63 | 2.00 | - | - | - | - | Ag (s, s) |
E | 6.09 | 47.50 | 26.16 | 8.55 | 11.7 | - | - | TiCu2 |
F | 1.38 | 1.27 | 1.79 | 29.61 | - | 22.05 | 43.91 | LiAlSiO4 |
Material | Temperature (°C) | Yield Strength (MPa) | Density (g/cm3) | Poisson’s Ratio | Elastic Modulus (GPa) | CET (×10−6 K−1) |
---|---|---|---|---|---|---|
SiC | 900 | 300 | 3.1 | 0.2 | 420 | 4.8 |
AgCuTi | 20 | 9.76 | 0.363 | 67 | 20.5 | |
LAS | 190 | 2.67 | 0.25 | 64 | −6.1 |
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Jiang, J.; Wang, G.; Wang, M.; Zhao, Y. Microstructure and Shear Strength of SiC Joint Brazed with LiAlSiO4 Reinforced AgCuTi Composite Filler. Metals 2023, 13, 736. https://doi.org/10.3390/met13040736
Jiang J, Wang G, Wang M, Zhao Y. Microstructure and Shear Strength of SiC Joint Brazed with LiAlSiO4 Reinforced AgCuTi Composite Filler. Metals. 2023; 13(4):736. https://doi.org/10.3390/met13040736
Chicago/Turabian StyleJiang, Jian, Gang Wang, Mengmeng Wang, and Yu Zhao. 2023. "Microstructure and Shear Strength of SiC Joint Brazed with LiAlSiO4 Reinforced AgCuTi Composite Filler" Metals 13, no. 4: 736. https://doi.org/10.3390/met13040736