2.1. Selection of Materials and Specimen Design
The authors investigated the impact of four surface waterproofing treatments of different chemical compositions on three different types of brick-and-mortar samples and small masonry assemblies [
23] (see
Figure 2a). This testing programme focussed on hydrophobicity, water absorption, and water vapour permeability representing three major stages of moisture exposure life-cycle: first contact with water, wetting, and drying. The results show that out of four products that were tested, silane/siloxane blend cream is the most effective, with up to 96% reduction in water absorption, but, as a drawback, its hydrophobicity performance was found to be inconsistent and water vapour resistance increased by 18%, impairing vapour transmission for moisture stored within the fabric. On the other hand, specimens treated with the acrylic-based product showed satisfactory performance in hydrophobicity and water vapour transmission tests, showing good beading effect and ease of drying. However, the 40% reduction in water absorption indicated a comparatively poor performance. Given the very different performance and characteristics observed in the small specimens’ tests, these two surface waterproofing products were selected for the wall-scale tests reported here, to further the understanding of their impact on the dynamic process of wetting and drying of real-scale cavity walls exposed to WDR. The information provided by the manufacturer and a summary of bench test outcomes are given in
Table 1.
The outcomes of these bench tests were used to select vulnerable brick types, on the basis of comparatively lower water vapour resistance, showing consistency of performance with each applied waterproofing treatment [
34]. The Forterra Atherstone Red, is a fired clay brick with a smooth finish, of a standard size of 215 × 102.5 × 65 mm, with the manufacturer’s reported gross density equal to 1900 kg/m
3 and 15% frogged volume. Particle composition and manufacturing methods are both representative of bricks kilned in the 1960s to 1980s and are still commonly used in current construction practice in the UK [
35,
36]. Hydrated lime M4 mortar with a lime, cement, and sand ratio of 1:1:6, was used, representing typical mortars used in the 1960s and 1970s [
37].
The masonry cavity wall specimens were built in dimensions of 1.1 m × 1.1 m × 0.28 m, each wall consisting of two 102.5 mm thick leaves of bricks in stretcher bond and with a 75 mm cavity in between. Mortar bed and head joints were bucket-handled and 10 mm thick. The height of the wall specimens differed from the specifications recommended in [
38], which suggests a height of 2.4 m. The decision to limit the height of the specimen stems from the fact that taller specimens would result in a higher level of runoff in the lower portions of the walls [
39], while the emphasis of the present study is on determining the effect of WDR exposure conditions.
Six wall specimens were built by professional brick layers and cured in a constant environment maintained at 22 °C and 55% relative humidity for 28 days before applying the water-repellent treatments. After applying the treatment, the walls were further conditioned for 14 days. The walls were built at the end of 2018 and exposed to WDR tests during the summer of 2019 as part of a project sponsored by the Department for Business, Energy & Industrial Strategy (BEIS, [
36]) (
Figure 2b). The specimens were then stored in a curing room under variable environmental conditions until May 2022, before the set of tests reported here were performed. As the wall condition and quality of workmanship have a substantial impact on masonry as rainwater can easily penetrate cracks and reach the interior surface (see [
40]), the crack locations on test walls were recorded and mapped in detail.
The insulation material filling the cavity of the walls was closed-cell, expanded polystyrene (EPS) beads with a diameter around 2 mm, manufactured following [
41] and meeting the requirements of KIWA BDA Agrément. The installation of beads started with sealing the sides of the specimens with insulation tape from Pavatax, a thermal-resistant tape with high-strength adhesive; then, the insulation beads were poured into the cavity without use of adhesives, compacted until full, for a total of 1.4 kg of beads per cavity, achieving a density of 12 kg/m
3 ± 2 per installation recommended by [
41,
42]. The water vapour transmission factor (µ), measured according to [
43], for loose-fill EPS beads is 2, a value notably lower than the average of 18.23 observed in untreated masonry specimens reported by [
23]. Additionally, the 24 h water absorption, measured through partial immersion following [
44], method A, is found to be lower than 1 kg/m
3.
2.2. Test Setup
The progression of moisture from the outer surface of the outdoor leaf to the inner surface of the indoor leaf is affected by outdoor and indoor environmental conditions, including the differential in temperature and relative humidity of the two environments. To reproduce such conditions simultaneously while applying cyclic WDR to the specimens, the coupled environmental chambers of the integrated mechanical–climatic testing facility of the UCL StrEnTHE lab (
Figure 3) were used. The two bespoke WEISS chambers were connected by a shared mounting frame of 5 m × 4 m × 0.4 m with structural testing capacity. The outdoor chamber simulated environmental conditions from −30 to 70 °C with RH control from 5 to 98%, while the indoor chamber simulated 5 to 40 °C with RH from 20 to 98%. Each test batch included two specimens for a total of 12 specimens tested in two rounds. The first round included couples of uninsulated untreated reference walls, acrylic-treated walls, and silane/siloxane blend cream-treated walls. The same walls were then insulated and tested again in the second round (
Figure 3).
The WDR was dispersed via a three-layer built-in horizontal rain simulation system in the outdoor chamber, each layer equipped with six nozzles (
Figure 3c). The nozzles had a 400 mm horizontal interval and sprayed with 60° cone, the vertical height of each layer being adjustable. The bottom layer of 6 nozzles at a height of 600 mm from the chamber floor were used in these tests, aligned with the mid-height of the specimens, to ensure even and full coverage of the specimens’ surface through horizontal spraying. The nozzle spray pressure was enhanced by two fans installed behind the nozzles and set to achieve 6 m/s (22 Pa) wind speed for the rain.
Each wall specimen was built on a steel plate of 17.5 mm thickness, with four load cells installed under each corner of the wall and fixed to a base steel plate. Each load cell had a range up to 200 kg with an accuracy of ±0.04 kg, determining any weight change due to water absorption, redistribution, and evaporation separately for each leaf.
To understand the movement of moisture inside the specimens, each wall was monitored by five in-wall sensors installed in the outer leaf at various depths and heights, and one in the inner leaf at the centre, to record RH and T in both brick and mortar. One of the sensors in the mortar of the outer leaf had higher accuracy. Holes were drilled at sensor sizes at different depths from the inner leaf to the outer leaf and sealed with waterproof silicone putty after the sensors’ installation to prevent moisture leakage.
Load cell and in-wall sensor specifications and locations are given in
Table 2 and
Figure 4, respectively. All RH and T sensors measured in-wall conditions, providing an accurate representation of the moisture uptake in the outer leaf and hence a direct measure of the effectiveness of the superficial treatments as barriers to water absorption. All in-wall sensors and load cells were connected and logged simultaneously using the National Instrument LabView data acquisition system at a frequency of 30 s. All obtained data were further averaged at one reading per minute on each sensor. T and RH of both indoor and outdoor chambers were controlled and recorded by using the WEISS S!MPATI
® 4.80.1 software.
2.3. Test Protocol
Table 3 summarises the methods and specifications of commonly used WDR test standards on different building elements. The water application rate, wind pressure, and test duration differ with the climate/weather conditions represented, corresponding to three diverse test purposes:
Water tightness with a pass/fail criterion after exposure to given test conditions for a period of time;
Water tightness failure in static or dynamic conditions with different levels of wind pressure;
Record of absorption rate within a given test duration.
As the objective of this study is to identify the impact on water uptake in masonry cavity wall specimens of surface waterproofing treatments exposed to WDR, the quantification of absorption rate was deemed of vital importance to establish their performance.
Examples of different testing protocols from previous research were also examined. The work of [
52,
53] adheres to [
38] but uses different spray systems compared to the standard. The authors of [
52] deliver a much lower WDR application rate at 0.28 L/m
2·min in their test on external wood claddings compared to the 1.5 L/m
2·min required by [
38]. Ref. [
53] uses only driving rain, excluding runoff water while using specimen dimensions differing from the standard requirements. Similarly, Ref. [
54] introduces a spray rate of 1.44 L/m
2·min in high-velocity rainfall simulation, exceeding the 0.5 L/m
2·min required in [
51]. The authors of [
55] provide an overview of 30 test standards worldwide and note the lack of clarity on which type of test procedure renders the most realistic or severe test conditions. They consider that available standards provide testing procedures for the resistance to water penetration of either window and door elements (e.g., [
48]) or for generic façade systems (e.g., [
38]). Therefore, adjusting the test conditions based on the materials/elements being tested and the specific weather conditions of interest is deemed necessary and justified.
In the study by [
56], the peak WDR intensity, peak WDR wind pressure, and combined average for return periods up to 1 in 50 years for Belgium and the Netherlands were studied. The results indicate that procedures using both high wind pressure, i.e., 600 Pa, and high water dispersion, i.e., 2 L/m
2·min, as specified by standards such as [
45,
48], are extreme test conditions and are unlikely to occur under normal service conditions [
57], as high wind speeds and intense rainfall do not usually occur at the same time [
10]. Research involving on-site monitoring at different locations in the UK reported similar findings [
11,
58]. Therefore, it would be beneficial to study the behaviour of specimens exposed to high water applications and low wind pressure or vice versa in order to reduce the discrepancy between laboratory test results and real-world performance. Ref. [
59] tested clay brick masonry with reduced water application of 0.03–0.06 L/m
2·min with no wind load applied, resulting in no water penetration over six cycles of 210 min of wetting and 20 min of pause. Ref. [
60] tested historic masonry-infilled timber frames using low rates of spraying and wind speed, 0.375 L/m
2·min and 2 m/s, respectively, to encourage wetting of the walls while matching typical rainfall amounts for given return periods and to study the strength and stiffness deterioration of the load-bearing system, with up to 100 cycles of wetting and drying. Further research is needed to investigate the impact of wind speed and water application rate on water uptake and system performance.
Ref. [
61] carried out a comparative study of weather data including average annual rainfall, average annual wind speed, and WDR spell index for locations in very severe exposure areas across the UK. By excluding low-population-density locations, Swansea in South Wales was deemed typical of a mid-size city in a very severe exposure zone and was used to compare test protocols from the standards with historical weather data (see
Figure 1). Weather data for Swansea are available for a number of stations from the Met Office [
62]. According to the most recent dataset spanning the period 1991 to 2020, the average annual maximum and minimum temperatures are 13.72 °C and 8.81 °C, respectively, with annual mean wind speed of 6.85 m/s. Additionally, through Swansea City Council, data at hourly intervals are available for the period between 2012 and 2017. The highest hourly rainfall rate recorded is 7.8 mm/hour (0.13 L/m
2·min), while the highest hourly average wind speed is 17.5 m/s, yielding a pressure exerted of approximately 185 Pa. These measurements yield a water application rate significantly lower than the minimum rate recommended by the test standards shown in
Table 3. Considering indications from the literature discussed above, the average monthly wind speed of 6.85 m/s, recorded from 1991 to 2020 in Swansea, was considered the most suitable reference for the WDR test.
Surface waterproofing treatments form a hydrophobic layer on the exterior surface of the masonry to prevent/reduce the ingress of rainwater. Therefore, a test condition at a sustained water application rate was deemed more suitable to monitor the absorption rate, while lower wind speeds reduce the influence of splashing and bouncing of raindrops [
63]. From the water application rates shown in
Table 3, it can be inferred that in European standards, a spray rate of 2.0 L/m
2·min is the most common spray rate used to apply a constant and continuous film to the outside surface of the specimen.
As previously mentioned, the vapour pressure differential between indoors and outdoors, primarily resulting from the temperature differences, can have a significant effect on moisture movement in walls. By examining the data for Swansea, the average monthly temperature during the month with the highest rain and wind occurrence was 7.6 °C [
61]. To account for the average conditions as well as the extremes, while ensuring wide applicability of the results and accurate control of the environmental chambers, a consistent outdoor temperature of 15 °C was kept during the wetting period, while the water temperature was maintained at 6–7 °C and the indoor temperature was set at 20 °C.
Figure 5 shows the WDR setup of six nozzles and how nozzles spray cones overlap, causing parts of the specimens’ surface to be wetted to different degrees. Each nozzle was set to deliver 1 L/min of water, resulting in an average wetting rate at the walls equal to 1.91 L/m
2·min. During the actual testing, with the wind pressure provided by the fans, the water dispersion pattern and intensity can be different from the theoretical case. To confirm this, three WDR gauges were put at the centre and edges of both walls to measure the overall amount of water delivered to the wall surface during a wetting cycle. The average was measured at 2.25 L/m
2·min. Ref. [
38] prescribes that the deviation of the measured WDR application from the nominal values should not surpass 0.5 L/m
2·min, which was adhered to by all measured values as proven by the WDR gauge readings. Furthermore, the flow meter utilised in the setup complied with the standard’s requirement for ±10% accuracy in measuring the amount of supplied water.
In summary, the WDR test protocol in the outdoor chamber consisted of cyclic application of 10 min of wetting at a rate of 2.25 L/m
2·min at 15 °C every 60 min between conditioning intervals at a constant 20 °C, with a wind speed of 6 m/s (22 Pa). Indoor conditions were set at a constant of 20 °C and 50% RH. As shown in
Table 4, the WDR test was divided into four phases over 52 h: all walls were exposed to 2 WDR cycles in the first phase of the test, then conditioned for 20 h at 20 °C T, 50% RH in Phase 2; in Phase 3, untreated walls were exposed to 6 wetting cycles, while treated ones were exposed to 8 cycles, and again all underwent 22 h of drying with the same conditions in Phase 4. The drying times for Phases 2 and 4 took into account the observation that no significant weight loss could be observed after 20 h of drying.
Table 4 and
Table 5 summarise the rate and amount of water applied to each specimen in each phase. Phase 1 applies a total of 45 L/m
2 to the specimen, an amount within the range of 33–56.5 L/m
2 per spell, representative of a moderate exposure zone. Phase 3 represents an exposure rate of 135 L/m
2 and 180 L/m
2 per spell for untreated and treated specimens, respectively, in excess of both the severe exposure range (56.5–100 L/m
2) and the very severe exposure range threshold (100+ L/m
2), as defined in
Figure 1, and therefore representing extreme conditions.