1. Introduction
Walnuts are the most widely planted nuts worldwide [
1]. They are rich in vitamins B and E, unsaturated fatty acids, tocopherols, phytosterols, flavonoids, etc., and the content of monounsaturated fatty acids and polyunsaturated fatty acids is the highest in the nut world [
2,
3,
4,
5]. It has obvious advantages in reducing cholesterol, preventing cardiovascular diseases, and is deeply welcomed by consumers. In 2020, the global planting area was approximately 1.3 million hectares, and the total export volume reached 4.42 million tons [
6]. China, the United States, and Turkey are the three major countries that grow walnuts in the world [
7]. China is the world’s largest producer of walnuts. According to the official website of the FAO, in 2020, China’s walnut planting area was 284,375 ha, with a total output of 110 million tons, accounting for 25% of the world’s total output [
6].
Walnut shelling is the key step in the walnut food industry. At present, walnut shelling technology and equipment still have the characteristics of a low rate of high-quality kernels (RHQK) and a poor rate of shelling crushing (RSC) [
8]. Damaged nuts not only cause great losses and reduce the economic benefits of walnuts, but also affect the quality of the walnuts and their products, which poses a great threat to food safety [
9]. As the walnut shell is mainly composed of lignin, cellulose, and hemicellulose, it is hard and thick, irregular in shape, with multiple partitions and a small gap between the shell and the kernel, which results in a difficult shelling process, slow development of walnut shelling machinery, and poor shelling quality. For a long time, China, Turkey, and other main walnut-growing countries have sold walnuts with shells, high transportation costs, and low added value of products [
10]. Presently, the processing rate of walnuts in Xinjiang, the main walnut-producing area in China, is only 2% [
11]. Consequently, the development of the walnut industry has been seriously restricted by the progress in shelling technology and equipment. Therefore, high-quality mechanized shelling of walnuts has become a trending issue worldwide.
Numerous studies have been conducted to obtain high-quality shelling. Ercisli, et al., studied the variety, edge length, and thickness of walnut; analyzed the influence law of these factors on walnut shelling; and obtained the force direction of the minimum rupture force [
12]; Khir, et al. studied the characteristics of walnut size and moisture content, and revealed the law of walnut shell rupture [
13]. Using a mechanical testing device, Sharifian et al. reported that the force loading speed, moisture content, and loading direction had a significant impact on the rupture of walnut shells and concluded that the best shelling results appeared with the moisture content of walnut at 21%, and a loading speed of 500 mm/min along the X direction [
14]. Koyuncu et al. studied the force, energy, and specific deformation before initial rupturing and kernel extraction quality by compressing walnuts with a universal testing machine and found that cracking nuts at the length position required less force and yielded the best kernel extraction quality [
15]. Li et al. designed a model of a conic basket walnut shelling device, carried out the relevant tests, and determined that the clearance of the shelling device, conic angle of the roller, walnut size, and walnut shell thickness were the key parameters affecting the shelling quality [
16]. Wang et al. studied the influence of key parameters of a conic basket shell-breaking equipment on the operation quality by using an orthogonal test, obtained the optimal parameters of the fixed cylinder speed, distance between the fixed cylinder and the moving cylinder, and the shelling operation quality under the best parameters [
17]. Liu et al. studied the mechanism of walnut shelling by shear extrusion using a flexible belt and designed a belt sheller for walnuts. Taking belt spacing, the speed difference between the two belts, and the extrusion angle as the key operation parameters, they carried out a single-factor test and an orthogonal test and obtained the optimal parameters of this type of belt-shelling equipment [
18]. Wang et al. studied the characteristics of a walnut crack based on the finite element method using a workbench, compared the results with the experimental method, and obtained the best direction of force for walnut cracking [
19].
Walnut shelling is the interaction between the key components of shelling equipment and walnut materials. The shelling process involves complex mechanisms and mutual mechanics. Existing research mostly separates the physical characteristics of walnut and the mechanical key parameters, but systematical studies, and optimization of multiple factors including the physical characteristics of walnut and parameters of the machinery are seldom seen. However, the mechanical analysis of the shelling process and physical characteristics of walnuts were not mentioned. Consequently, the separation between agricultural machinery and walnut agronomic characters has led to a slow improvement in walnut shelling machinery, resulting in a low profit for walnut farmers, which is a fatal blow to the development of the walnut industry in China. Therefore, the improvement of the shelling quality of walnut shellers is an urgent issue. To improve the shelling quality, it is necessary to systematically combine the analysis of the mechanical properties of walnut shells, research on the mechanical properties of walnuts, parameter design and optimization of key components, and mutual coupling effects of the factors on RHQK and RSC. However, tremendous experiments must be carried out while considering these factors together and studying them systematically, which costs a lot of time.
In this study, a key component of the walnut shelling device was designed based on the principle of friction extrusion. First, we assumed the mechanical extrusion model of walnut shelling, then analyzed the mechanics between the walnut and the key components to obtain reasonable parameters for the conic roller. It was assumed that the application of the Box–Behnken design (BBD) method would help simplify the complexity of the experiment and enable us optimize the system in affordable laboratory work. The Box–Behnken test was used to design the walnut shelling experiment, and the multi-objective optimization method was used to optimize the key parameters affecting the shelling quality, obtain the best quality of walnut shelling operation, and provide a reference for improving the operation quality of walnut shelling equipment.
2. Materials and Method
2.1. Walnut Sample Preparation
The walnuts that were used in this study were Wen185 varieties that are widely planted in Xinjiang Province, which is the main walnut-producing area in China. The walnut was ellipsoidal in shape with an average length of 4.7 cm, thickness of 3.7 cm, and width of 3.7 cm. The length, width and thickness are shown in
Figure 1. A total of 100 walnuts were randomly selected and tested, and the average single walnut weight was 15.8 g, the average shell thickness was 0.8 mm, and the kernel yield of walnut was 65.9% by manual shelling. The initial average moisture content of the walnuts was determined to be 16.95% (w.b.), following the standard for oilseeds [
20].
2.2. Mediating Moisture Contents of Walnuts and Mechanical Property Test
To study the mechanical properties of walnuts with different moisture contents, it is necessary to adjust their moisture content. This implies that for practical applications, a scheme involving wetting adjustment should be devised. Distilled water was sprayed on the walnuts (ASAE standards, 1999), which were then sealed in plastic bags and homogenized for 12 h at 5 °C. The amount of water (
Qw) that was added to the samples was calculated using Equation (1) (Kumar et al., 2016).
where
Qw is the mass of the added distilled water (kg),
Qp is the initial mass of the walnut sample (kg),
Mf is the final dry basis moisture content of the sample, and
Mi is the initial dry basis moisture content.
Rupture forces were tested using a universal mechanical testing machine (CTM-4503, Sansi Testing Technology Co., Ltd., Shenzhen, China). The walnut was positioned in alignment with the central point of the lower pressure plate. The upper plate was set to touch the top of the walnut. The feeding speed of the applied load was 5 mm·min−1. The stress-strain relationships of walnuts with different moisture contents were plotted during the test.
2.3. Mechanical Analysis of Walnut Shelling
The conic roller-shelling device is mainly composed of a shelling conic roller and a static roller, as presented in
Figure 2a.
Figure 2b,c show the shelling prototype. The walnuts enter the clearance between the shelling conic roller and the static roller, driven by the rotation of the shelling conic roller, and are rubbed and squeezed by the static and shelling conic roller to break the shell and release the nut shelling. In order to meet the requirements of the study, the required speed of the shelling conic roller can be obtained by the adjustment of a frequency converter, and the gap between the shelling conic roller and the static roller can be adjusted through the transmission and adjustment mechanism as showed in the red rectangle in
Figure 2b.
To select reasonable key parameters and optimize the design, a stress analysis of the walnut shelling process was carried out first. The walnut was assumed to be an ellipsoid based on the basic parameters of walnuts in
Section 2.1, and the coordinate system was established with the long axis and short axis of the ellipsoid as the
x-axis and
y-axis, respectively. The mechanical model of the walnut shelling analysis diagram is shown in
Figure 2d.
In
Figure 2d, A and B are the contact points of the walnut with the shelling conic and static rollers, respectively. Assuming that the walnut was in equilibrium at the moment of shell rupture:
where,
m is the mass of a walnut,
g;
is the acceleration due to gravity, m·s
−2;
is the elastic force of the contact surface when the walnut is in contact with the static roller,
N;
is the elastic force of the contact surface when the walnut is in contact with the shelling conic roller,
N;
is the included angle between the conical surface of the shelling conic roller and the vertical plane, °;
is the included angle between the static roller and the vertical plane, °;
is the friction force of shelling conic roller on walnut,
N;
is the friction force of the static roller on the walnut,
N;
is walnut volume, m
3;
is volume deformation of the walnut in contact with the static roller, m
3;
is volume deformation of the walnut in contact with the shelling conic roller, m
3;
is the dynamic friction factor between the walnut and the shelling conic roller;
is the elastic modulus of the walnut;
is the moment of the walnut, n·m;
is the diameter of the walnut,
m; and
is the static friction.
The total deformation of walnut is:
The volumetric strain of walnut is:
By combining Equations (2)–(7) and (10), we obtain:
The elastic modulus of the walnut was 10 MPa, the average mass of the walnuts were calculated as 2.1 g, the dynamic friction factor between the walnut and the shelling conic roller
was 0.23, and volume strain of walnut was 3.5 × 10
−4 [
16]. When the angles of the shelling conic roller and the static shelling conic roller are
5° and
18°, respectively,
,
,
, and
.
From the stress analysis, the walnut moves upward with an increase in force during the shelling process; therefore, the static friction force is opposite to this trend, and = . When designing the angle of the shelling conic roller , according to the characteristics of the sinusoidal function, the value of the sinusoidal function is more sensitive to the change in angle when the angle is small. This means that as is a very small angle, component will increase rapidly, and the static friction force will not be sufficient to overcome the upward movement of the walnut; the walnut will move upward, and the shelling process will stop. When the value is too large, the change rate of the distance between the shelling conic roller and the static roller will decrease, and the range of walnut shell size that is suitable for the shelling device will become narrower, resulting in poor quality of the shelling operation.
Based on the above analysis, it is necessary to reasonably select the angle of the shelling conic roller and static roller of the shelling device. By calculating and combining the range of the walnut rupture force, the angle of the static roller can be calculated as 16°, and the angle of the shelling conic roller will be greater than 5°.
2.4. Performance Evaluation
According to actual production needs and relevant standards, the RHQK and RSC of walnuts are important assessment indicators for shelling equipment. During the shelling test, three samples were taken randomly at the outlet of the walnut shelling equipment, and each sample was not less than 2 kg. Thereafter, walnuts with broken shells and high-quality kernels were manually selected. According to this standard, kernels that were greater than or equal to one-quarter are defined as high-quality kernels, as shown in
Figure 3.
This test mainly examines the rate of high-quality kernels and the shell crushing rate of walnuts. The calculation method is as follows:
where
is the total mass of the walnut sample, kg;
is the mass of cracked walnut, kg;
is the mass of high-quality kernel, kg; and
is the total mass of walnut kernel, kg.
2.5. Single-Factor Tests
The angles of the shelling conic roller, speeds of the shelling conic roller, clearance between the shelling conic roller and the static roller, and the moisture content of walnuts are the key parameters of shelling devices. A reasonable test range of the key parameters is key to obtaining the optimum combination of parameters. The more accurate that the selection range of the key parameters is, the better the optimization effect and quality will be
Section 2.2 indicated that the angle of the shelling conic roller is not less than 3°, but the optimal range of the angle and the other parameters need to be further clarified. A single-factor test was carried out on the walnut shelling process. In the single-factor test, other factors remained fixed. Each single-factor test was conducted five times, and the average value was recorded.
2.6. Box-Behnken Design
The Box–Behnken design is an experimental method that evaluates the nonlinear relationship between indicators and factors. It is widely used in the engineering field and is an economical experimental method for simplifying experiments [
21,
22]. The equations of test factors and response indicators were established according to the test results. The acquired workable range of each influential factor was further normalized to −1, 0, and 1, which corresponded to the lower limit, center point, and upper limit of the workable ranges. The number of BBD tests that were performed was:
where
is the number of factors, and
is the number of repetitions of the central test point that is used in estimating the test error. The results of the BBD experimental scheme, based on
Table 1, were obtained from Design-Expert 12 (version 12.0.3.0; Stat-Ease, Inc., Minneapolis, MN, USA), and presented in
Table 2. With this simplification, the total experimental work was reduced to 29 runs with
.
2.7. Construction of System Optimization Model
To prepare a reliable model for this study, we referenced relevant reports in the literature and proposed a polynomial equation as follows:
The BBD test obtains the nonlinear equation of the operation index and uses the significance analysis method to optimize and improve the equation. By defining the optimization objectives and boundary conditions, an optimization model of the walnut shelling operation quality was established, and the optimal solution was obtained via the optimization solution from Design-Expert.
2.8. Model Evaluation
The optimization results were verified and evaluated using production trial tests that were conducted on a walnut farm. The optimal moisture content of the walnut was adjusted based on the optimized results from the BBD test, and the sheller was set to the optimal parameters. Samples were taken every 10 min while the sheller was in a steady state. A total of two kilograms of the sample was collected for each trial to determine the RHQK and RSC.
5. Conclusions
The poor shelling quality of walnut shelling equipment restricts progress in the walnut processing industry. Improved walnut shelling quality is of great importance in reducing shelling loss, improving farmers’ income, and upgrading processed walnut quality. In this experiment, we assumed a mechanical model of walnut shelling and performed a force analysis to determine the key parameters affecting shelling quality. Via the experiment and variance analysis, we obtained the significant influencing parameters, acquired the mathematical model for the quality of the shelling operation, and optimized the key shelling parameters using the multi-objective optimization method. Surprisingly, the relative errors between the optimized results and the production test values of RHQK and SRC were 2.53% and 2.66%, respectively. The results implied that shelling quality and error were greatly improved compared to previous research results using the orthogonal test [
14,
15,
16,
17,
18,
19]. These findings further explained the feasibility of improving the shelling quality of walnuts by adjusting their moisture content. A comparison of the predicted and production test results also demonstrated the reliability of the assumptions from the mechanical analysis, the accuracy, and the reliability of the prediction model. The related methods can be used for optimizing the design of other nut-shelling equipment.
In this study, we proposed a mechanical model for walnut shelling and performed key parameter optimization and experimental verification. The single-factor and BBD tests were conducted using the angles of the shelling conic roller, speeds of the shelling conic roller, clearance between the shelling conic roller and the static roller, and the moisture content of walnuts. BBD, ANOVA, mathematical modeling, and multi-objective optimization were applied in the experiment. The ranking of factors that affected RHQK and RSC was as follows: clearance between the shelling conic roller and the static roller (X3) > moisture content of the walnuts (X4) > speeds of the shelling conic roller (X2) > angles of the shelling conic roller (X1) for RHQK > speeds of the shelling conic roller (X2) > clearance between the shelling conic roller and the static roller (X3) > moisture content of walnuts (X4) > angles of the shelling conic roller(X1) for RSC. The rank of significant interactive effects among the factors was as follows: angles of the shelling conic roller and speeds of the shelling conic roller (X1 X2) > speeds of the shelling conic roller, and clearance between the shelling conic roller and the static roller (X2 X3) for RHQK, clearance between the shelling conic roller and static roller (X2 X3) > clearance between shelling conic roller and the static roller, and moisture content of walnuts (X3 X4) > speeds of the shelling conic roller, and moisture content of walnuts (X2 X4) for RSC. Furthermore, the multi-objective optimization results were: angles of the shelling conic roller = 15.83°, speeds of the shelling conic roller = 17.93 rpm, clearance between the shelling conic roller and the static roller = 45 mm, and the moisture content of walnuts = 9.5%, yielding RHQK = 84.54% and RSC = 99.15%. A verification test of the optimal results further showed the feasibility and effectiveness of the proposed method. The method that was used in this study provides a reference for improving the shelling quality of other nuts.