Preparation of Silver Antibacterial Agents with Different Forms and Their Effects on the Properties of Water-Based Primer on Tilia europaea Surface
Abstract
:1. Introduction
2. Experimental Materials and Methods
2.1. Experimental Materials
2.2. Preparation of Micron Silver Particles
2.3. Preparation of the Microcapsule of Urea Formaldehyde Resin-Coated Nano-Silver Solution
2.4. Preparation of Waterborne Wood Antibacterial Paint Film
2.5. Testing and Characterization
3. Results and Discussion
3.1. Microstructure Analysis
3.2. Color Difference, Gloss, Adhesion, and Impact Resistance of Antibacterial Coatings
3.3. Microstructure and Composition Analysis of Paint Film
3.4. Analysis of Antibacterial Rate
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Material | Molecular Formula | MW (g/mol) | CAS No. | Concentration | Producer |
---|---|---|---|---|---|
silver nitrate solid powder | AgNO3 | 169.87 | 7761-88-8 | 99.9% | Nanjing Chemical Reagent Co., Ltd., Nanjing, China |
concentrated ammonia | NH3∙H2O | 35.00 | 1336-21-6 | 25% | Tianjin Fuchen Chemical Reagent Factory, Tianjin, China |
nano-silver solution | - | - | - | 100 ppm | Luoyang Oulun Environmental Protection Technology Co., Ltd., Luoyang, China |
formaldehyde solution | CH2O | 30.03 | 50-00-0 | 37.0% | Tianjin University Mao Chemical Reagent Factory, Tianjin, China |
urea | CH4N2O | 60.06 | 57-13-6 | 99.9% | Tianjin Beichen Fangzheng Chemical Reagent Factory, Tianjin, China |
triethanolamine | C6H15NO3 | 149.19 | 102-71-6 | 99.9% | Xilong Science Co., Ltd., Wuxi, China |
absolute ethanol | C2H6O | 46.07 | 64-17-5 | 99.9% | Wuxi Yasheng Chemical Co., Ltd., Wuxi, China |
sodium dodecyl benzene sulfonate | C18H29NaO3S | 348.48 | 25155-30-0 | 99.9% | Wuxi Yatai United Chemical Co., Ltd., Wuxi, China |
waterborne acrylic resin | - | - | 9003-01-4 | - | Dulux Paint Co., Ltd., Shanghai, China |
citric acid monohydrate | C6H10O8 | 210.14 | 5949-29-1 | 99.9 | Kunshan Southeast Chemical Materials Co., Ltd., Kunshan, China |
Tilia europaea | - | - | - | - | Shanghai Puhui industry and Trade Co., Ltd., Shanghai, China |
nutrient broth | - | - | - | - | Guangdong huankai Microbial Technology Co., Ltd. Guangzhou, China |
eluent | NaCl | 58.4428 | 7647-14-5 | 0.85% | Sichuan Kelun Pharmaceutical Co., Ltd., Chengdu, China |
staphylococcus aureus AS1.89 | - | - | - | - | Beijing Baocang Biotechnology Co., Ltd., Beijing, China |
nutrient agar | - | - | - | - | Hangzhou microbial Reagent Co., Ltd., Hangzhou, China |
Percentage (%) | Mass of Primer (g) | Mass of Nano-Silver Solution and Other Antibacterial Agent (g) |
---|---|---|
0 | 3.00 | 0 |
1.0 | 2.97 | 0.03 |
4.0 | 2.88 | 0.12 |
7.0 | 2.79 | 0.21 |
10.0 | 2.70 | 0.30 |
13.0 | 2.61 | 0.39 |
16.0 | 2.52 | 0.48 |
Microcapsule Content (%) | Color Difference | Gloss (%) | Adhesion (Level) | Impact Resistance (kg·cm) |
---|---|---|---|---|
0 | 0.73 | 30.5 | 1 | 5.0 |
1.0 | 1.92 | 29.1 | 2 | 7.0 |
4.0 | 2.45 | 8.0 | 2 | 7.0 |
7.0 | 2.78 | 3.6 | 3 | 8.0 |
10.0 | 2.89 | 2.7 | 3 | 8.0 |
13.0 | 3.64 | 2.6 | 4 | 9.0 |
16.0 | 4.22 | 2.5 | 4 | 9.0 |
Nano-Silver Solution Content (%) | Color Difference | Gloss (%) | Adhesion (Level) | Impact Resistance (kg·cm) |
---|---|---|---|---|
0 | 0.73 | 30.5 | 1 | 5.0 |
1.0 | 1.27 | 29.7 | 1 | 6.0 |
4.0 | 1.37 | 26.4 | 2 | 7.0 |
7.0 | 1.57 | 20.8 | 3 | 7.0 |
10.0 | 1.60 | 17.5 | 3 | 8.0 |
13.0 | 2.09 | 14.7 | 3 | 8.0 |
16.0 | 2.11 | 11.2 | 3 | 8.0 |
Micron Silver Particle Content (%) | Color Difference | Gloss (%) | Adhesion (Level) | Impact Resistance (kg·cm) |
---|---|---|---|---|
0 | 0.73 | 30.5 | 1 | 5.0 |
1.0 | 3.64 | 14.1 | 1 | 7.0 |
4.0 | 4.08 | 7.2 | 2 | 10.0 |
7.0 | 5.32 | 4.4 | 2 | 11.0 |
10.0 | 5.92 | 2.8 | 3 | 12.0 |
13.0 | 7.09 | 1.6 | 3 | 13.0 |
16.0 | 8.91 | 1.2 | 3 | 14.0 |
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Yan, X.; Pan, P. Preparation of Silver Antibacterial Agents with Different Forms and Their Effects on the Properties of Water-Based Primer on Tilia europaea Surface. Coatings 2021, 11, 1066. https://doi.org/10.3390/coatings11091066
Yan X, Pan P. Preparation of Silver Antibacterial Agents with Different Forms and Their Effects on the Properties of Water-Based Primer on Tilia europaea Surface. Coatings. 2021; 11(9):1066. https://doi.org/10.3390/coatings11091066
Chicago/Turabian StyleYan, Xiaoxing, and Pan Pan. 2021. "Preparation of Silver Antibacterial Agents with Different Forms and Their Effects on the Properties of Water-Based Primer on Tilia europaea Surface" Coatings 11, no. 9: 1066. https://doi.org/10.3390/coatings11091066