Capsaicin-Modified Fluorosilicone Based Acrylate Coating for Marine Anti-Biofouling
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Round 1
Reviewer 1 Report
- The authors should explain the novelty of the work with more details.
- The grammatical and typo errors should be revised.
- Mention some of the surface factors affecting the strength of adhesion in the 3.2. Mechanical properties section.
- What was the surface roughness of glass and steel substrate used for adhesion. Because surface roughness plays an important role in adhesion.
Author Response
Please see the attachment.
Author Response File: Author Response.pdf
Reviewer 2 Report
- The authors described on page 2 in lines 46-48,
- The authors should describe the materials, such as liquid LB media and PBS, used for antibacterial assays in the Experimental section. The authors should describe the details of SEM and EDS analysis in the Experimental section.
- It was described in the Experimental section that the monomers were mixed with AIBN at 75 degrees, however, the temperature was shown at 70 degrees in Figure 1. Which is correct?
- The authors should show J-coupling and integrations of protons corresponding to each proton in 1H-NMR of HMBA.
- The authors should explain AWS on page 7 in line 235.
- It is hard to see the error bars in Figures 3A and 4G, H.
- It is hard to see the gradient getting blacker toward the outside in Figure 4G, H.
- The compound names should be listed alongside the chemical structures in Figure 1.
- The authors should show 1H-NMR of PRE-0 to compare with PRE-10, 20, and 30 in Figure 2C.
- The authors should show the GPC results of PRE-0. I think that Figure 2E is not necessary to show. It means that it is enough to show the results as Figure 2F.
- The authors should explain WCA and DCA in Figure 3B, D.
- The authors should describe which sample was used in SEM and EDS analyses in Figure 3E.
- As I am color blind, it is difficult for me to recognize the colors of methacryloxypropyl
Author Response
Please see the attachment.
Author Response File: Author Response.pdf
Reviewer 3 Report
The paper show novelty research and the data are all well exhibited.
I have 1 comment: GFE in Figure 3A stands for what? and please put PDMS in the list of Materials (section 2.1).
Author Response
Please see the attachment
Author Response File: Author Response.pdf
Round 2
Reviewer 2 Report
The editor should check that the authors have responded to the reviewer's comments. It shouldn't be the editor's work to forward a reviewer a manuscript.
I cited my previous comments as italic, and strikethrough ones have been revised.
strikethrough
- The authors described on page 2 in lines 46-48,
- The authors should describe the materials, such as liquid LB media and PBS, used for antibacterial assays in the Experimental section. The authors should describe the details of SEM and EDS analysis in the Experimental section.
The authors responed that SEM and EDS details have been added, howevwe, I could not find them in the revied manscirpit. - It was described in the Experimental section that the monomers were mixed with AIBN at 75 degrees, however, the temperature was shown at 70 degrees in Figure 1. Which is correct?
- The authors should show J-coupling and integrations of protons corresponding to each proton in 1H-NMR of HMBA.
It is important point. If the authors would not show the anaysises, I could not trast their synthesitc results. - The authors should explain AWS on page 7 in line 235.
- It is hard to see the error bars in Figures 3A and 4G, H.
- It is hard to see the gradient getting blacker toward the outside in Figure 4G, H.
- The compound names should be listed alongside the chemical structures in Figure 1.
- The authors should show 1H-NMR of PRE-0 to compare with PRE-10, 20, and 30 in Figure 2C.
- The authors should show the GPC results of PRE-0. I think that Figure 2E is not necessary to show. It means that it is enough to show the results as Figure 2F.
It is nessery to show the GPC results of PRE-0. If not, I can not accept the manscript. - The authors should explain WCA and DCA in Figure 3B, D.
- The authors should describe which sample was used in SEM and EDS analyses in Figure 3E.
- As I am color blind, it is difficult for me to recognize the colors of methacryloxypropyl
Author Response
Please see the attachment.
Author Response File: Author Response.pdf