Effect of the Surface States of 1Cr18Ni9Ti Stainless Steel on Mn-Based Brazing Alloy Wetting
Abstract
:1. Introduction
2. Experimental Section
2.1. Wetting Experiment
2.2. Characterization
3. Result and Discussion
3.1. The Characterization of Substrates
3.2. In Situ Observation of the Brazing Alloy Contact Angle
3.3. The Wetting and Spreading Properties
3.4. The Interfacial Microstructure between Brazing Alloy and Substrates
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Element | Fe | Ni | Cr | Mn | Si | Ti | C |
---|---|---|---|---|---|---|---|
1Cr18Ni9Ti | Bal. | 8~11 | 17~19 | ≤2.0 | ≤1.0 | 0.8 | ≤0.12 |
Mn70NiCr | - | 24.0~26.0 | 4.5~5.5 | Bal. | - | - | - |
1Cr18Ni19Ti No. | Surface States | Contact Angle/Brazing Alloy Spreading Area (mm2) | ||
---|---|---|---|---|
1150 °C/15 min | 1170 °C/15 min | 1190 °C/15 min | ||
1 | Acid treatment | 15.4°/26.463 | 19.5°/25.092 | 20.6°/21.264 |
2 | Acid treatment + 4 μm Ni | 6.1°/49.662 | 7.7°/38.031 | 11.8°/37.532 |
3 | Acid treatment + 10 μm Ni | 15.3°/42.318 | 18°/31.408 | 14°/28.142 |
4 | Sandblasting + 4 μm Ni | 10.4°/36.121 | 13.3°/30.121 | 15.3°/26.044 |
5 | Acid treatment | 18.9°/26.248 | 24.7°/18.511 | 22.4°/23.681 |
6 | Acid treatment + 4 μm Ni | 11.6°/39.246 | 6.4°/45.595 | 6.6°/41.073 |
7 | Acid treatment + 10μm Ni | 7.9°/39.581 | 12.0°/39.173 | 11.9°/31.660 |
8 | Sandblasting + 4 μm Ni | 13.0°/31.944 | 11.7°/27.681 | 8.9°/32.523 |
9 | Acid treatment | 20.9°/26.892 | 24.2°/22.125 | 20°/23.647 |
10 | Acid treatment + 4 μm Ni | 10.1°/38.905 | 6.3°/51.458 | 6.6°/43.396 |
11 | Acid treatment + 10 μm Ni | 8.2°/40.169 | 8.6°/45.662 | 6.3°/57.521 |
12 | Sandblasting + 4 μm Ni | 15.1°/32.660 | 9.1°/39.551 | 10.1°/32.533 |
Element (At.%) | Ti | Cr | Mn | Fe | Ni |
---|---|---|---|---|---|
A | - | 17.05 | 2.59 | 24.19 | 56.17 |
B | - | 15.95 | 24.66 | 13.88 | 45.52 |
C | 0.59 | 12.60 | 0.39 | 76.28 | 10.14 |
D | 0.57 | 19.56 | 1.9 | 70.10 | 7.95 |
Element (At.%) | Ti | Cr | Mn | Fe | Ni |
---|---|---|---|---|---|
A | - | 16.06 | 5.50 | 21.92 | 56.53 |
B | - | 14.44 | 22.37 | 15.87 | 47.32 |
C | 1.38 | 8.21 | 0.33 | 49.16 | 40.91 |
D | 0.65 | 19.07 | 1.73 | 70.69 | 7.87 |
Element (At.%) | Ti | Cr | Mn | Fe | Ni |
---|---|---|---|---|---|
A | - | 18.38 | 3.09 | 22.04 | 56.49 |
B | - | 13.77 | 25.23 | 12.69 | 48.32 |
C | 1.13 | 7.73 | 0 | 42.4 | 48.90 |
D | 0.45 | 19.01 | 1.67 | 70.75 | 8.12 |
Element (At.%) | Ti | Cr | Mn | Fe | Ni |
---|---|---|---|---|---|
A | - | 19.06 | 7.66 | 21.04 | 52.25 |
B | - | 10.07 | 34.57 | 7.83 | 47.53 |
C | 6.51 | 19.52 | 8.35 | 52.77 | 12.84 |
D | 0.65 | 19.18 | 1.76 | 70.20 | 8.21 |
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Zhang, C.; Chen, H.; Yang, W.; Zhang, Q.; Yang, B.; Hu, Y.; Li, C.; Gao, D.; Si, X.; Qi, J.; et al. Effect of the Surface States of 1Cr18Ni9Ti Stainless Steel on Mn-Based Brazing Alloy Wetting. Coatings 2022, 12, 1328. https://doi.org/10.3390/coatings12091328
Zhang C, Chen H, Yang W, Zhang Q, Yang B, Hu Y, Li C, Gao D, Si X, Qi J, et al. Effect of the Surface States of 1Cr18Ni9Ti Stainless Steel on Mn-Based Brazing Alloy Wetting. Coatings. 2022; 12(9):1328. https://doi.org/10.3390/coatings12091328
Chicago/Turabian StyleZhang, Chenghao, Huize Chen, Weipeng Yang, Qinlian Zhang, Bo Yang, Yazhen Hu, Chun Li, Dejun Gao, Xiaoqing Si, Junlei Qi, and et al. 2022. "Effect of the Surface States of 1Cr18Ni9Ti Stainless Steel on Mn-Based Brazing Alloy Wetting" Coatings 12, no. 9: 1328. https://doi.org/10.3390/coatings12091328