Physicochemical and In Vitro Starch Residual Digestion Structures of Extruded Maize and Sorghum Starches Added with Sodium Stearoyl Lactylate
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Starch Extrusion
2.3. Starch Granule Morphology
2.4. Starch and Amylose Contents
2.5. Thermal Properties
2.6. X-ray Diffraction
2.7. Starch Digestion Fractions
2.8. In Vitro Starch Digestion Rate and Predicted Glycemic Index
2.9. Transmittance and Wavelength of Maximum Absorption
2.10. Emulsifying Characteristics
2.11. Foaming Characteristics
2.12. Molecular Characteristics of Starch and Amylopectin Chain Length Distribution
2.13. Statistical Analyses
3. Results and Discussion
3.1. Starch Characteristics
3.2. Thermal Characteristics
3.3. In Vitro Starch Digestion Properties
3.4. Functional Properties
3.5. Molecular Characteristics and Chain Length Distribution
3.6. Statistical Analysis
4. Conclusions
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
Appendix A
References
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Treatment | RPM | Moisture (%) | Temp (°C) | SSL (%) |
---|---|---|---|---|
E CT1 | 140 | 30 | 60 | 0 |
E CT 2 | 100 | 30 | 80 | 0 |
E CT 3 | 180 | 30 | 80 | 0 |
E CT 4 | 140 | 20 | 80 | 0 |
E CT 5 | 140 | 40 | 80 | 0 |
E CT 6 | 140 | 30 | 100 | 0 |
E CT 7 | 140 | 20 | 100 | 0.5 |
E CT 8 | 140 | 40 | 100 | 0.5 |
E CT 9 | 100 | 30 | 100 | 0.5 |
E CT 10 | 180 | 30 | 100 | 0.5 |
E CT 11 | 100 | 20 | 80 | 0.5 |
E CT 12 | 180 | 20 | 80 | 0.5 |
E CT 13 | 100 | 40 | 80 | 0.5 |
Treatment | SSL (%) | Temp (°C) | Moisture (%) |
---|---|---|---|
E ST1 | 0.5 | 80 | 40 |
E ST2 | 0.5 | 80 | 20 |
E ST3 | 0.5 | 100 | 20 |
E ST4 | 0.5 | 100 | 40 |
E ST5 | 1 | 80 | 40 |
E ST6 | 1 | 80 | 20 |
E ST7 | 1 | 100 | 20 |
E ST8 | 1 | 100 | 40 |
Treatment | Total Starch (%) | Amylose (%) | Amylopectin (%) |
---|---|---|---|
Maize | 91.23 ± 0.41 b | 27.35 ± 0.15 a | 72.65 ± 0.42 g |
E CT1 | 88.54 ± 0.30 c | 25.65 ± 0.50 b | 74.35 ± 0.29 f |
E CT2 | 89.42 ± 0.52 c | 23.24 ± 0.12 c | 76.76 ± 0.17 d |
E CT3 | 90.07 ± 0.73 b | 24.09 ± 0.77 b | 75.91 ± 0.30 e |
E CT4 | 88.99 ± 0.16 c | 22.21 ± 0.39 d | 77.79 ± 0.81 c |
E CT5 | 89.61 ± 0.40 c | 23.33 ± 0.90 c | 76.67 ± 0.53 d |
E CT6 | 90.22 ± 0.24 b | 23.74 ± 0.03 c | 76.26 ± 0.03 d |
E CT7 | 89.88 ± 0.03 c | 23.30 ± 0.60 c | 76.70 ± 0.58 d |
E CT8 | 90.05 ± 0.52 b | 23.57 ± 0.69 c | 76.44 ± 0.18 d |
E CT9 | 90.13 ± 0.09 b | 23.45 ± 0.12 c | 76.55 ± 0.05 d |
E CT10 | 90.00 ± 0.06 b | 23.82 ± 0.49 c | 76.19 ± 0.63 d |
E CT11 | 88.42 ± 0.85 c | 21.43 ± 0.99 d | 78.57 ± 0.53 c |
E CT12 | 88.59 ± 0.50 c | 22.70 ± 0.09 d | 77.30 ± 0.78 c |
E CT13 | 89.09 ± 0.17 c | 22.41 ± 0.86 d | 77.59 ± 0.54 c |
E CT14 | 88.81 ± 0.65 c | 22.73 ± 0.36 d | 77.27 ± 0.84 c |
Sorghum | 93.23 ± 0.22 a | 21.23 ± 0.22 d | 78.77 ± 0.10 b |
Sorghum SSL | 91.93 ± 0.62 b | 19.92 ± 0.05 e | 80.08 ± 0.20 b |
E ST1 | 91.19 ± 0.40 b | 17.98 ± 0.56 f | 82.02 ± 0.67 a |
E ST2 | 92.00 ± 0.58 b | 19.00 ± 0.51 e | 81.00 ± 0.94 a |
E ST3 | 91.81 ± 0.75 b | 18.60 ± 0.11 e | 81.40 ± 0.20 a |
E ST4 | 90.50 ± 0.31 b | 17.09 ± 0.02 f | 82.91 ± 0.79 a |
E ST5 | 91.82 ± 0.38 b | 18.61 ± 0.99 e | 81.39 ± 0.79 b |
E ST6 | 92.13 ± 0.16 b | 19.12 ± 0.40 e | 80.88 ± 0.03 b |
E ST7 | 90.93 ± 0.54 b | 17.72 ± 0.83 f | 82.28 ± 0.48 a |
E ST8 | 90.54 ± 0.69 b | 17.13 ± 0.43 f | 82.87 ± 0.50 a |
Treatment | To (°C) | Tp (°C) | Tc (°C) | Tf-To (°C) | ΔH (J/g) | %Gel | Crystallinity (%) |
---|---|---|---|---|---|---|---|
Maize | 66.43 ± 1.81 a | 70.31 ± 1.81 b | 73.26 ± 1.81 b | 6.83 ± 1.81 c | 12.43 ± 1.81 b | ND | 27.41 ± 1.81 a |
E CT1 | 64.93 ± 0.51 b | 68.81 ± 0.51 c | 69.13 ± 0.51 c | 4.20 ± 0.51 d | 10.93 ± 0.51 c | 12.07 ± 0.51 d | 25.36 ± 0.51 b |
E CT2 | 55.32 ± 0.94 d | 57.41 ± 0.94 e | 59.36 ± 0.94 e | 4.04 ± 0.94 d | 5.36 ± 0.94 d | 56.88 ± 0.94 c | 11.26 ± 0.94 d |
E CT3 | 54.62 ± 2.46 d | 56.71 ± 2.46 e | 60.24 ± 2.46 e | 5.62 ± 2.46 c | 4.85 ± 2.46 d | 60.97 ± 2.46 b | 10.51 ± 2.46 d |
E CT4 | 53.65 ± 2.42 d | 55.74 ± 2.42 e | 59.87 ± 2.42 e | 6.22 ± 2.42 c | 4.66 ± 2.42 d | 62.52 ± 2.42 b | 11.42 ± 2.42 d |
E CT5 | 52.85 ± 2.23 d | 54.94 ± 2.23 e | 58.69 ± 2.23 e | 5.84 ± 2.23 c | 4.78 ± 2.23 d | 61.55 ± 2.23 b | 12.29 ± 2.23 d |
E CT6 | 51.99 ± 2.28 d | 54.08 ± 2.28 e | 57.98 ± 2.28 e | 5.99 ± 2.28 c | 4.73 ± 2.28 d | 61.94 ± 2.28 b | 12.19 ± 2.28 d |
E CT7 | 51.09 ± 1.53 d | 53.18 ± 1.53 f | 57.15 ± 1.53 e | 6.07 ± 1.53 c | 4.71 ± 1.53 d | 62.13 ± 1.53 b | 11.84 ± 1.53 d |
E CT8 | 50.22 ± 0.29 e | 52.31 ± 0.29 f | 56.21 ± 0.29 f | 5.99 ± 0.29 c | 4.73 ± 0.29 d | 61.95 ± 0.29 b | 12.33 ± 0.29 d |
E CT9 | 49.28 ± 1.76 e | 51.37 ± 1.76 f | 55.43 ± 1.76 f | 6.14 ± 1.76 c | 4.68 ± 1.76 d | 62.34 ± 1.76 b | 8.81 ± 1.76 e |
E CT10 | 48.52 ± 1.94 e | 50.61 ± 1.94 f | 54.28 ± 1.94 f | 5.77 ± 1.94 c | 4.80 ± 1.94 d | 61.36 ± 1.94 b | 12.89 ± 1.94 d |
E CT11 | 47.48 ± 0.32 e | 49.57 ± 0.32 g | 53.85 ± 0.32 f | 6.37 ± 0.32 c | 4.61 ± 0.32 d | 62.92 ± 0.32 b | 12.04 ± 0.32 d |
E CT12 | 46.81 ± 2.19 e | 48.90 ± 2.19 g | 52.36 ± 2.19 f | 5.54 ± 2.19 c | 4.87 ± 2.19 d | 60.78 ± 2.19 b | 13.11 ± 2.19 d |
E CT13 | 45.88 ± 0.85 e | 47.97 ± 0.85 g | 52.02 ± 0.85 f | 6.14 ± 0.85 c | 4.68 ± 0.85 d | 62.34 ± 0.85 b | 8.81 ± 0.85 e |
E CT14 | 45.14 ± 0.31 e | 47.23 ± 0.31 g | 50.84 ± 0.31 g | 5.69 ± 0.31 c | 4.83 ± 0.31 d | 61.17 ± 0.31 b | 7.63 ± 0.31 e |
Sorghum | 69.43 ± 1.87 a | 74.32 ± 1.87 a | 76.26 ± 1.87 a | 6.83 ± 1.87 c | 14.21 ± 1.87 a | ND | 29.34 ± 1.87 a |
Sorghum SSL | 67.93 ± 1.46 a | 72.82 ± 1.46 a | 73.13 ± 1.46 b | 5.20 ± 1.46 c | 12.71 ± 1.46 b | 10.56 ± 1.46 d | 27.15 ± 1.46 a |
E ST1 | 57.25 ± 0.20 c | 62.14 ± 0.20 d | 64.15 ± 0.20 d | 6.90 ± 0.20 c | 5.36 ± 0.20 d | 62.28 ± 0.20 b | 13.17 ± 0.20 d |
E ST2 | 49.72 ± 1.01 e | 54.61 ± 1.01 e | 57.21 ± 1.01 e | 7.49 ± 1.01 b | 4.39 ± 1.01 d | 69.08 ± 1.01 a | 17.41 ± 1.01 c |
E ST3 | 50.52 ± 1.87 d | 55.41 ± 1.87 e | 60.15 ± 1.87 e | 9.63 ± 1.87 a | 4.20 ± 1.87 d | 70.43 ± 1.87 a | 13.17 ± 1.87 d |
E ST4 | 48.85 ± 0.98 e | 53.74 ± 1.98 e | 58.43 ± 1.98 e | 9.58 ± 1.98 a | 4.01 ± 1.98 d | 71.79 ± 1.98 a | 7.31 ± 1.98 e |
E ST5 | 47.24 ± 0.43 e | 52.13 ± 0.43 e | 54.13 ± 0.43 f | 6.89 ± 0.43 c | 4.20 ± 0.43 d | 70.47 ± 0.43 a | 13.03 ± 0.43 d |
E ST6 | 48.08 ± 1.51 e | 52.97 ± 1.51 e | 55.26 ± 1.51 f | 7.18 ± 1.51 b | 4.39 ± 1.51 d | 69.11 ± 1.51 a | 14.16 ± 1.51 d |
E ST7 | 48.87 ± 1.46 e | 53.76 ± 1.46 e | 55.12 ± 1.46 f | 6.25 ± 1.46 c | 4.20 ± 1.46 d | 70.47 ± 1.46 a | 13.03 ± 1.46 d |
E ST8 | 47.20 ± 0.50 e | 52.09 ± 0.50 e | 54.33 ± 0.50 f | 7.13 ± 0.50 b | 4.00 ± 0.50 d | 71.82 ± 0.50 a | 7.16 ± 0.50 e |
Treatment | RDS (%) | SDS (%) | RS (%) | pGI |
---|---|---|---|---|
Maize | 73.43 ± 1.83 b | 22.27 ± 0.18 b | 4.30 ± 0.69 f | 92.18 ± 1.25 a |
E CT1 | 64.91 ± 2.87 c | 24.43 ± 3.57 b | 10.66 ± 0.46 e | 90.41 ± 3.61 a |
E CT2 | 72.24 ± 2.65 b | 20.52 ± 3.88 b | 7.24 ± 4.15 e | 93.18 ± 3.10 a |
E CT3 | 68.90 ± 1.40 c | 20.19 ± 4.22 b | 10.91 ± 4.23 e | 92.80 ± 0.57 a |
E CT4 | 75.26 ± 2.83 b | 19.78 ± 2.66 b | 4.96 ± 4.26 f | 93.66 ± 2.43 a |
E CT5 | 66.91 ± 3.44 c | 18.94 ± 2.79 b | 14.15 ± 0.46 d | 92.71 ± 2.43 a |
E CT6 | 70.25 ± 1.60 b | 19.28 ± 1.69 b | 10.48 ± 3.30 e | 93.09 ± 3.70 a |
E CT7 | 71.92 ± 3.56 b | 19.44 ± 3.40 b | 8.64 ± 3.00 e | 93.28 ± 2.30 a |
E CT8 | 70.33 ± 1.90 b | 19.28 ± 3.89 b | 10.38 ± 2.21 e | 93.10 ± 4.19 a |
E CT9 | 73.67 ± 0.52 b | 19.62 ± 3.68 b | 6.71 ± 0.12 f | 93.48 ± 2.29 a |
E CT10 | 65.32 ± 1.57 d | 18.78 ± 0.51 c | 15.90 ± 1.11 c | 92.53 ± 3.80 a |
E CT11 | 78.68 ± 1.07 a | 20.12 ± 3.77 b | 1.20 ± 3.99 g | 94.05 ± 2.59 a |
E CT12 | 60.31 ± 3.29 e | 18.28 ± 3.15 c | 21.41 ± 3.98 a | 91.95 ± 1.59 a |
E CT13 | 73.67 ± 0.17 b | 19.62 ± 2.08 b | 6.71 ± 1.88 f | 93.48 ± 0.87 a |
E CT14 | 63.65 ± 4.05 d | 18.61 ± 4.12 c | 17.73 ± 0.24 b | 92.34 ± 4.17 a |
Sorghum | 62.71 ± 3.90 d | 27.88 ± 0.15 a | 9.41 ± 3.35 e | 90.37 ± 2.03 a |
Sorghum SSL | 62.76 ± 0.13 d | 27.88 ± 2.03 a | 9.37 ± 1.74 e | 90.15 ± 3.29 a |
E ST1 | 71.73 ± 4.00 b | 27.12 ± 0.64 a | 1.15 ± 0.89 g | 93.00 ± 2.10 a |
E ST2 | 72.11 ± 1.68 b | 27.71 ± 0.60 a | 0.18 ± 2.10 g | 92.94 ± 4.13 a |
E ST3 | 70.63 ± 3.27 b | 26.85 ± 1.95 a | 2.52 ± 0.80 g | 92.89 ± 1.53 a |
E ST4 | 65.53 ± 3.49 d | 25.07 ± 2.10 a | 9.40 ± 1.34 e | 92.51 ± 0.85 a |
E ST5 | 65.73 ± 3.85 d | 25.61 ± 3.82 a | 8.66 ± 1.36 e | 92.43 ± 4.02 a |
E ST6 | 72.15 ± 1.70 b | 27.71 ± 1.31 a | 0.13 ± 0.01 h | 92.94 ± 2.39 a |
E ST7 | 69.44 ± 1.20 c | 26.54 ± 1.53 a | 4.03 ± 1.66 f | 92.78 ± 3.26 a |
E ST8 | 72.27 ± 3.96 b | 26.74 ± 1.71 a | 0.99 ± 0.12 g | 93.15 ± 0.27 a |
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de la Rosa-Millan, J.; Heredia-Olea, E.; Pérez-Carrillo, E.; Peña-Gómez, R.; Serna-Saldívar, S.O. Physicochemical and In Vitro Starch Residual Digestion Structures of Extruded Maize and Sorghum Starches Added with Sodium Stearoyl Lactylate. Foods 2023, 12, 1988. https://doi.org/10.3390/foods12101988
de la Rosa-Millan J, Heredia-Olea E, Pérez-Carrillo E, Peña-Gómez R, Serna-Saldívar SO. Physicochemical and In Vitro Starch Residual Digestion Structures of Extruded Maize and Sorghum Starches Added with Sodium Stearoyl Lactylate. Foods. 2023; 12(10):1988. https://doi.org/10.3390/foods12101988
Chicago/Turabian Stylede la Rosa-Millan, Julian, Erick Heredia-Olea, Esther Pérez-Carrillo, Raquel Peña-Gómez, and Sergio O. Serna-Saldívar. 2023. "Physicochemical and In Vitro Starch Residual Digestion Structures of Extruded Maize and Sorghum Starches Added with Sodium Stearoyl Lactylate" Foods 12, no. 10: 1988. https://doi.org/10.3390/foods12101988