Preparation of Electrospun Polyvinyl Alcohol/Nanocellulose Composite Film and Evaluation of Its Biomedical Performance
Abstract
:1. Introduction
2. Results and Discussion
2.1. ZETA Potential of the Spinning Solution
2.2. The Structure and Hydrogen Bond Fitting of PVA/NC Nanofiber Membranes
2.3. Crystallization Properties of PVA/NC Nanofiber Membranes
2.4. Morphology and Porosity of PVA/NC Nanofiber Membranes
2.5. Mechanical Properties of PVA/NC Nanofiber Membranes
2.6. Contact Angle of PVA/NC Nanofiber Membranes
2.7. Liquid Absorption Performance of PVA/NC Nanofiber Membranes
2.8. Cytotoxicity of PVA/NC Nanofiber Membranes
3. Conclusions
4. Experiments and Methods
4.1. Materials
4.2. Preparation of PVA/NC Nanofiber Membranes
4.3. ZETA Potential Test of Spinning Solution
4.4. PVA/NC Nanofiber Membranes Structure and Performance Characterization
4.4.1. Chemical Structure of PVA/NC Nanofiber Membranes
4.4.2. Crystallization Performance of PVA/NC Nanofiber Membranes
4.4.3. Microscopic Morphology, Diameter and Porosity of PVA/NC Nanofiber Membranes
4.4.4. Mechanical Test of PVA/NC Nanofiber Membranes
4.4.5. Contact Angle Test of PVA/NC Nanofiber Membranes
4.4.6. Liquid Absorption Test of PVA/NC Nanofiber Membranes
4.4.7. Cytotoxicity Test of PVA/NC Nanofiber Membranes
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
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Sample | Hydrogen Bond Type | Abbreviations | Wave Number/cm−1 | Average Peak Area | Relative Strength/% | Relative Strength/% | |
---|---|---|---|---|---|---|---|
NC2 | Free hydroxyl | Ⅳ | —OH | 3570 | 6.32 | 2.82 | 2.82 |
Intramolecular hydrogen bond | Ⅲ | OH…OH | 3400 | 150.53 | 67.11 | 68.84 | |
Ⅰ | Annular polymer | 3118 | 3.9 | 1.73 | |||
Intermolecular hydrogen bond | Ⅱ | OH…ether O | 3217 | 63.56 | 28.34 | 28.34 | |
NC4 | Free hydroxyl | Ⅳ | —OH | 3570 | 10.91 | 5.23 | 5.23 |
Intramolecular hydrogen bond | Ⅲ | OH…OH | 3400 | 134.23 | 64.33 | 66.18 | |
Ⅰ | Annular polymer | 3118 | 3.87 | 1.85 | |||
Intermolecular hydrogen bond | Ⅱ | OH…ether O | 3217 | 59.65 | 28.59 | 28.59 | |
NC6 | Free hydroxyl | Ⅳ | —OH | 3570 | 18.1 | 9 | 9 |
Intramolecular hydrogen bond | Ⅲ | OH…OH | 3400 | 113.43 | 56.4 | 59.57 | |
Ⅰ | Annular polymer | 3118 | 6.37 | 3.17 | |||
Intermolecular hydrogen bond | Ⅱ | OH…ether O | 3217 | 63.21 | 31.43 | 31.43 | |
NC8 | Free hydroxyl | Ⅳ | —OH | 3570 | 17.07 | 6.35 | 6.35 |
Intramolecular hydrogen bond | Ⅲ | OH…OH | 3400 | 161.11 | 59.91 | 62.44 | |
Ⅰ | Annular polymer | 3118 | 6.8 | 2.53 | |||
Intermolecular hydrogen bond | Ⅱ | OH…ether O | 3217 | 83.94 | 31.21 | 31.21 |
NC0 | NC2 | NC4 | NC6 | NC8 |
---|---|---|---|---|
50.06% | 48.08% | 43.32% | 38.23% | 42.45% |
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Ji, X.; Guo, J.; Guan, F.; Liu, Y.; Yang, Q.; Zhang, X.; Xu, Y. Preparation of Electrospun Polyvinyl Alcohol/Nanocellulose Composite Film and Evaluation of Its Biomedical Performance. Gels 2021, 7, 223. https://doi.org/10.3390/gels7040223
Ji X, Guo J, Guan F, Liu Y, Yang Q, Zhang X, Xu Y. Preparation of Electrospun Polyvinyl Alcohol/Nanocellulose Composite Film and Evaluation of Its Biomedical Performance. Gels. 2021; 7(4):223. https://doi.org/10.3390/gels7040223
Chicago/Turabian StyleJi, Xinbin, Jing Guo, Fucheng Guan, Yuanfa Liu, Qiang Yang, Xin Zhang, and Yi Xu. 2021. "Preparation of Electrospun Polyvinyl Alcohol/Nanocellulose Composite Film and Evaluation of Its Biomedical Performance" Gels 7, no. 4: 223. https://doi.org/10.3390/gels7040223