1. Introduction
Laser Powder Bed Fusion (L-PBF) is one of the most advanced additive manufacturing (AM) technologies for producing metal parts with complex geometries and high mechanical performance [
1,
2]. Among commonly used alloys, AlSi10Mg is particularly valued for its low weight and favorable mechanical properties, making it suitable for aerospace and automotive applications. However, its high thermal diffusivity poses challenges during processing due to rapid temperature changes and complex heat dissipation.
Effective process monitoring is therefore essential to ensure part quality and repeatability. Infrared thermography has emerged as a promising in situ technique for monitoring L-PBF, allowing the capture of thermal signatures related to the melt pool and surrounding powder bed [
1,
2]. Although the melt pool is typically smaller than the resolution of conventional thermal cameras, previous studies have shown that statistical features extracted from thermal images can successfully correlate process parameters with defect formation [
3,
4,
5,
6]. This method eliminates the need for direct melt pool visualization or precise knowledge of emissivity and absolute temperature, which are often difficult to determine during processing [
3].
Recent research has used thermal data to predict mechanical properties and detect common defects such as keyhole porosity and lack of fusion, employing both statistical analysis and machine learning approaches [
1,
2,
3,
4,
5,
6].
This work employs a fixed microbolometer thermal system and varying laser power and speed in the Design of Experiments (DOE) to analyze thermal features, such as cooling rate, and their correlation with process parameters and defects during L-PBF of AlSi10Mg. The results support real-time monitoring for improved process control and quality assurance.
2. Materials and Methods
Experiments were conducted on an EOS M290 L-PBF machine (EOS GmbH Krailling: Monaco, Germany) equipped with an FLIR A700 camera (Teledyne FLIR LLC: Wilsonville, OR, USA). The IR system uses a ZnS window and records at 30 fps with a spatial resolution of ~0.6 mm/pixel.
Figure 1 illustrates the system and build layout. Small cubes and cylindrical tensile specimens (ASTM E8/E8M) were built with varying power, scan speed, and position on the plate (
Table 1) [
7]. In a dedicated job, induced keyhole porosity was achieved by reducing scan speed in selected regions and increasing VED from ~74 to ~147 J/mm
3. For defect areas, a 24° lens was used, improving resolution to ~0.35 mm/pixel.
The bulk material surrounding the defects was processed using a laser power of 370 W, a scanning speed of 1280 mm/s, and a volumetric energy density (VED) of 74.12 J/mm3. In contrast, keyhole porosity was induced in designated defect areas by reducing the scanning speed to 700 mm/s, resulting in an increased VED of 146.83 J/mm3.
3. Procedure for Data Analysis
The data analysis procedure involved reconstructing the thermal signal by identifying the maximum signal value associated with the laser scan during material deposition in each region. A 3D sequence was then reconstructed by aligning all frames relative to the maximum (peak) value. Since the laser operates in successive short scan paths and due to the limited track length and high scan speed, secondary peaks may occur as the laser passes nearby shortly after the first exposure.
To avoid interference from overlapping thermal signals, the analysis was restricted to the 10 frames following the identified peak. By considering this window, slope and R
2 [
8] were assessed pixel by pixel in both linear and double-logarithmic scales in order to obtain feature maps capable of describing the local cooling behavior in relation to process parameter variations.
From defined rectangular regions of interest (~2000 pixels per sample), a range of statistical features—including mean, standard deviation, minimum, maximum, and selected percentiles—were calculated for each thermal sequence. These features were then used in ANOVA and regression analyses to identify correlations with process parameters and build position.
4. Results and Discussion
Figure 2 presents the results obtained for a specific job, where at least one specimen with a label ID (as reported in
Table 1) is present for each combination of process parameters, considering both the maximum temperature (
Figure 2a) and the cooling slope (
Figure 2b). In addition,
Figure 2c shows the slope map extracted in a double logarithmic scale, which highlights thermal features related to the cooling behavior during process monitoring of specimens with intentionally induced defects—specifically simulating keyhole porosity. As expected, in these defective areas, where scan speed is reduced and volumetric energy density (VED) is increased, the apparent temperatures are higher. This confirms the method’s potential for detecting small defects, approximately 1 mm in size.
Qualitatively speaking, significantly high apparent temperatures are observed at low scan speeds (ID 3). Additionally, the cooling slope is steeper (more negative) when the scan speed remains at its lowest level. This effect is even more pronounced for the specimen with ID 3, where the laser power is at its highest level. Among the four tested conditions, this specimen corresponds to the highest VED (Volumetric Energy Density).
The statistical analysis (ANOVA), reported in
Table 2, confirmed that power, scan speed, and position had statistically significant effects (
p < 0.001) on both the maximum temperature and the cooling slope descriptors. In contrast, the replicate factor showed no significant influence (
p > 0.05), supporting the repeatability and robustness of the measurements collected during the printing of different layers.
Based on the results obtained from the ANOVA,
Figure 3 presents the correlations between thermal features and process parameters with regression models, separating the four positions and evaluating the RMSE, SNR, and R
2 values.
The results show consistently lower variability at Position II, which aligns with the physics of the process. In fact, this quadrant represents the most favorable printing area, with the recoater moving from right to left and the gas flow directed from the top to bottom.
In contrast, the other positions exhibit a steeper negative cooling slope across the different parameter combinations, indicating reduced cooling efficiency.
5. Conclusions
The implementation of thermal monitoring via microbolometer sensors enables robust correlation between process parameters and thermal features in L-PBF of AlSi10Mg, despite spatial resolution limitations (~0.6 mm/pixel), without requiring knowledge of the actual emissivity or monitoring melt pool behavior.
The ANOVA results reveal statistically significant effects (p < 0.001) of laser power, scan speed, and build position on thermal features such as maximum apparent temperature and cooling slope, with linear models capable of describing this correlation. Moreover, localized detection of keyhole porosity defects, approximately 1 mm in size, is demonstrated through slope map analysis, confirming the system’s capability for in situ defect identification and process control. Future work will focus on developing advanced real-time algorithms for automated defect prediction, adaptive process parameter adjustment, and mechanical properties estimation.
Author Contributions
Conceptualization, E.D. and U.G.; methodology, E.D., G.S., F.D.C., D.P. and U.G.; formal analysis, E.D.; investigation, E.D., G.S. and F.D.C.; data curation, E.D.; writing—original draft preparation, E.D.; writing—review and editing, G.A., G.S., F.D.C., D.P. and U.G.; supervision, U.G., D.P. and A.G.; project administration, U.G. and A.G.; funding acquisition, U.G. All authors have read and agreed to the published version of the manuscript.
Funding
This research was funded by the project TO ZERO—Towards Zero Waste In Aluminium Body-In-White Manufacturing a valere sulle agevolazioni previste dal Decreto Ministeriale 31 dicembre 2021 (Primo sportello) del MIMIT—Accordi per l’innovazione, CUP: B99J23002030005.
Institutional Review Board Statement
Not applicable.
Informed Consent Statement
Not applicable.
Data Availability Statement
The data that support the findings of this study are available from the corresponding author upon reasonable request.
Conflicts of Interest
Gianluca Acquistapace and Alex Giorgini were employed by the company Valland S.p.a. and declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest.
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