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Abstract

Smart Odour Sensing for Automated Monitoring of Bread Products †

1
Department of Chemistry, Materials and Chemical Engineering “Giulio Natta“, Politecnico di Milano, 20133 Milan, Italy
2
Department of Electronics, Information and Bioengineering, Politecnico di Milano, 20133 Milan, Italy
3
Electrolux Italia s.p.a., 33080 Pordenone, Italy
*
Author to whom correspondence should be addressed.
Presented at the XXXV EUROSENSORS Conference, Lecce, Italy, 10–13 September 2023.
Proceedings 2024, 97(1), 172; https://doi.org/10.3390/proceedings2024097172
Published: 9 April 2024

Abstract

:
This work proposes an electronic nose (e-nose) system based on resistive gas sensors to predict the cooking evolution of different types of bread. The e-nose includes six metal-oxide semiconductor (MOS) gas sensors, a low-noise electronic system for signal conditioning and data acquisition, and a classification algorithm for real-time detection of the cooking stage. Baking tests with five different recipes were carried out, and the system performances were evaluated by a panel of tasters, obtaining a -88% accuracy for the automatic detection of cooking time.

1. Introduction

E-nose application in the food industry represents a low-cost solution for quality assessment, process monitoring, and optimization of energy resources [1]. During bread baking, different groups of volatile organic compounds (VOCs) are released in each stage of the fermentation and cooking process, but few studies in the literature have shown that e-noses can be used to monitor this process [2]. For example, Gancarz et al. and Ponzoni et al. [3,4] demonstrate the applicability of e-noses for the detection of key aromas of different bread cooking stages, but do not show the real-time operation of the system in the harsh environment of in-oven operation. In this context, this work presents a new e-nose system for the real-time detection of the cooking stages of bread, applied to a set of five different recipes.

2. Materials and Methods

The experimental setup included a commercial oven, where six gas sensors of different types (Figaro TGS26-00/10/20) were installed, along with temperature and relative humidity sensors. A low-noise electronic system was used for modulated signal conditioning and acquisition to track the sensor resistance and the environmental sensor signals. A data acquisition board logged the data on a computer where a classification algorithm implemented in Matlab was used to predict the bread cooking status. The bare captured resistance traces were affected by the (i) electronic noise of the system, dominated by 1/f contributions from thin-film resistors (Figure 1a) and amplifiers [5] and (ii) huge oscillations due to the humidity changes inside the oven, where a heating element was periodically activated. The acquired signals were thus filtered to remove the oscillations, while 1-kHz signal modulation mitigated 1/f noise. Five bread recipes, with different ingredients and baking procedures, were considered: bread roll (BR), semola (SE), ciabatta (CB), multigrain (MG), and Val Venosta (VV). To account for the different lengths of different bread analyses, an algorithm based on principal component analysis (PCA) was used to select the best down-sampling frequency to apply to the acquired data. After this frequency was selected, a set of two features was extracted from the down-sampled version of the analysis and used as input for the Support Vector Machine (SVM) classifier, which had been trained considering 84 analyses, whose features (area under the curve and resistance ratio) were extracted at 3 different times, representative of the “Medium”, “Cooked”, and “Burnt” stages.

3. Discussion

The real-time operation of the system was then tested. The classification algorithm uses the features extracted from the real-time acquired signals (Figure 1b) to predict the cooking stage (Figure 2a). After the fifth “Cooked” prediction, the oven was stopped, and the bread was evaluated by a panel of tasters on a scale from 1 to 5. The correct cooking stage of 3–4 was obtained for ~88% of the analyses (Figure 2b). These performances will be further improved by expanding the training dataset, leading to a reliable e-nose system for smart ovens.

Author Contributions

C.B.: project management, e-nose training; B.d.D.: software; A.T.: noise measurements; N.D. and F.C.: project management; G.L.: supervision; L.C.: project coordination, supervision. All authors have read and agreed to the published version of the manuscript.

Funding

This research was carried out within the project SOS-COOKS - Smart Odour Sensors for monitoring COOking Systems, funded by MADE S.C.A. R.L., grant number CUP H42C21000910008 e COR 5768228.

Institutional Review Board Statement

Not applicable.

Informed Consent Statement

Not applicable.

Data Availability Statement

Data are confidential.

Conflicts of Interest

The authors declare no conflicts of interest.

References

  1. Tan, J.; Xu, J. Applications of electronic nose (e-nose) and electronic tongue (e-tongue) in food quality-related properties determination: A review. Artif. Intell. Agric. 2020, 4, 104–115. [Google Scholar] [CrossRef]
  2. Gancarz, M.; Malaga-Toboła, U.; Oniszczuk, A.; Tabor, S.; Oniszczuk, T.; Gawrysiak-Witulska, M.; Rusinek, R. Detection and measurement of aroma compounds with the electronic nose and a novel method for MOS sensor signal analysis during the wheat bread making process. Food Bioprod. Process. 2021, 127, 90–98. [Google Scholar] [CrossRef]
  3. Ponzoni, A.; Depari, A.; Falasconi, M.; Comini, E.; Flammini, A.; Marioli, D.; Taroni, A.; Sberveglieri, G. Bread baking aromas detection by low-cost electronic nose. Sens. Actuators B Chem. 2008, 130, 100–104. [Google Scholar] [CrossRef]
  4. di Diodoro, B.; Bax, C.; Dellarosa, N.; Corazza, F.; Langfelder, G.; Capelli, L. Bread baking monitoring by smart sensory system: A feasibility study. In Proceedings of the 2022 IEEE International Symposium on Olfaction and Electronic Nose (ISOEN), Aveiro, Portugal, 29 May–1 June 2022; pp. 1–4. [Google Scholar]
  5. Macku, R.; Smulko, J.; Koktavy, P.; Trawka, M.; Sedlak, P. Analytical fluctuation enhanced sensing by resistive gas sensors. Sens. Actuators B Chem. 2015, 213, 390–396. [Google Scholar] [CrossRef]
Figure 1. (a) Measured noise density of a TGS2620. (b) Temperature, humidity and resistance values of three of the gas sensors during the bread baking process.
Figure 1. (a) Measured noise density of a TGS2620. (b) Temperature, humidity and resistance values of three of the gas sensors during the bread baking process.
Proceedings 97 00172 g001
Figure 2. (a) PCA score plot of the dataset. (b) Sensorial evaluation of bread samples.
Figure 2. (a) PCA score plot of the dataset. (b) Sensorial evaluation of bread samples.
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Share and Cite

MDPI and ACS Style

Bax, C.; di Diodoro, B.; Ticozzi, A.; Dellarosa, N.; Corazza, F.; Langfelder, G.; Capelli, L. Smart Odour Sensing for Automated Monitoring of Bread Products. Proceedings 2024, 97, 172. https://doi.org/10.3390/proceedings2024097172

AMA Style

Bax C, di Diodoro B, Ticozzi A, Dellarosa N, Corazza F, Langfelder G, Capelli L. Smart Odour Sensing for Automated Monitoring of Bread Products. Proceedings. 2024; 97(1):172. https://doi.org/10.3390/proceedings2024097172

Chicago/Turabian Style

Bax, Carmen, Bianca di Diodoro, Alessandro Ticozzi, Nicolò Dellarosa, Flavio Corazza, Giacomo Langfelder, and Laura Capelli. 2024. "Smart Odour Sensing for Automated Monitoring of Bread Products" Proceedings 97, no. 1: 172. https://doi.org/10.3390/proceedings2024097172

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