Influence of Multiwalled Carbon Nanotubes in Sulfur/Carbon Nanotube Composites Synthesized Using Solution Casting Method †
Abstract
:1. Introduction
2. Materials and Method
2.1. Materials
2.2. Characterization
3. Results and Discussion
3.1. XRD Diffractogram Studies
3.2. Morphological Studies
3.3. FTIR Studies
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Sr. No. | Sample Name | Strain (ϵ × 10−4) | Dislocation Density (δ) (10−4 nm−2) | Crystallite Size tDS (in nm) | Crystallite Size tMS (in nm) | Crystallite Size tWH (in nm) |
---|---|---|---|---|---|---|
1. | S99% MWCNT 1% | 3.74 | 2.96 | 58.92 | 64.75 | 67.64 |
2. | S95% MWCNT 5% | 8.70 | 3.35 | 55.17 | 64.90 | 78.34 |
Sr. No. | Position of Bands (cm−1) | Assignment of Bands |
---|---|---|
1 | 570 | C–H out-of-plane bending, =C–H out-of-plane bending in alkenes |
2 | 797 | C–H out-of-plane bending of aromatic compounds, =C–H out-of-plane bending in alkenes [12] |
3 | 879 | S-OR ester group [12] |
4 | 1045 | C-O stretching band of alcohols, S=O stretching of sulfur compounds [13] |
5 | 1227 | Aliphatic C-O stretching of esters |
6 | 1448 | C=C stretching of carboxylic acid [14] |
7 | 2355 | Combination C-H stretching [15] |
8 | 2972 | C-H stretching of alkane [14] |
9 | 3675 | O-H stretching of alcohol [15] |
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Jain, K.; Jain, S.K.; Malhotra, A.; Dixit, S.; Tripathi, B.; Sahu, R. Influence of Multiwalled Carbon Nanotubes in Sulfur/Carbon Nanotube Composites Synthesized Using Solution Casting Method. Eng. Proc. 2023, 59, 217. https://doi.org/10.3390/engproc2023059217
Jain K, Jain SK, Malhotra A, Dixit S, Tripathi B, Sahu R. Influence of Multiwalled Carbon Nanotubes in Sulfur/Carbon Nanotube Composites Synthesized Using Solution Casting Method. Engineering Proceedings. 2023; 59(1):217. https://doi.org/10.3390/engproc2023059217
Chicago/Turabian StyleJain, Karishma, Sushil Kumar Jain, Anu Malhotra, Shalini Dixit, Balram Tripathi, and Rajesh Sahu. 2023. "Influence of Multiwalled Carbon Nanotubes in Sulfur/Carbon Nanotube Composites Synthesized Using Solution Casting Method" Engineering Proceedings 59, no. 1: 217. https://doi.org/10.3390/engproc2023059217