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16 pages, 755 KB  
Article
Screening of Wood Raw Materials for Low-Odor Fiberboard and Particleboard Production: Analysis and Evaluation Based on Volatile Odor Compounds
by Bo Liu, Fang Yang, Lina Tang, Xianwu Zou, Liming Zhu, Qian Chen, Bin Lv and Yuejin Fu
Polymers 2025, 17(17), 2429; https://doi.org/10.3390/polym17172429 (registering DOI) - 8 Sep 2025
Abstract
Woody raw materials of wood-based panels like fiberboard and particleboard are one of the primary sources of product odor and one of the indicators affecting the comprehensive health risk assessment of wood-based panel products. This study employed Gas Chromatography-Mass Spectrometry-Olfactometry (GC-MS-O) to investigate [...] Read more.
Woody raw materials of wood-based panels like fiberboard and particleboard are one of the primary sources of product odor and one of the indicators affecting the comprehensive health risk assessment of wood-based panel products. This study employed Gas Chromatography-Mass Spectrometry-Olfactometry (GC-MS-O) to investigate the odorant composition and odor characteristics, including Total Odor Concentration (TOC), odor intensity (OI), odor activity value (OAV), and risk value (RV), of 22 wood species commonly used in fiberboard and particleboard production in China. This research identified the major odor-active compounds in wood and provided recommendations for selecting wood raw materials suitable for low-odor fiberboards and particleboards produced by integrating RV and toxicity classification data. The results showed that the main compound types influencing wood odor in 22 wood species were predominantly terpenes, aldehydes, and alcohols. Woods of Cinnamomum, Machilus, and Pinus contained a higher number of dominant odor compounds (OAV > 1 and OI ≥ 3). Wood with stronger odor intensity included Cinnamomum, Pinus, Machilus, Bischofia, and Saurauia. The total RV of Cinnamomum, Pinus, Machilus, Cunninghamia, and Bombax wood exceeded one, necessitating special attention when used as raw materials for wood-based panels. Camphor in Cinnamomum and Machilus wood was the most concentrated odorant, followed by 3-Carene in Pinus wood. Odorants with high OAV included Longifolene, δ-Cadinene, Terpinen-4-ol, 2-Nonenal, γ-Terpinene, d-Limonene, 3-methyl-Butanal, Octanal, α-Pinene, Hexanal, D-Camphor, and trans-Calamenene. Odorants with high RV included terpenes, alcohols, aldehydes, and ketones, such as Camphor, 3-Carene, Eucalyptol, α-Terpineol, β-Pinene, α-Santalene, δ-Cadinene, Safrole, Longifolene, and d-Limonene. Focusing on the reduction and control of these odor-active compounds represents a primary approach to mitigating odors in fiberboard and particleboard products. However, addressing health risks associated with product odors requires additional attention to four specific substances: Safrole, Camphor, Eucalyptol, and α-Terpineol. Although the total RV for the five wood species exceeds one, this does not necessarily mean the final wood-based panel product’s RV exceeds one, as it also depends on the influence of the production process. Therefore, further research should be conducted to investigate the effects of various process parameters in wood-based panel production on the odor compounds present in the final panels. From a comprehensive perspective, considering the overall odor characteristics of wood volatiles, all 18 wood species (Salix, Populus, Rhaphiolepis, Ligustrum, Prunus, Fagus, Pterocarya, Firmiana, Celtis, Cunninghamia, Bombax, Bischofia, Ficus, Saurauia, Eucalyptus, Aleurites, Melia, Bridelia) are suitable for the production of low-odor fiberboards and particleboards. Full article
(This article belongs to the Special Issue Eco-Friendly Supramolecular Polymeric Materials, 2nd Edition)
15 pages, 639 KB  
Article
Arbuscular Mycorrhizal Fungi Inoculation Enhances Nutritional Quality of Prickly Pear (Opuntia ficus-indica) Fruits and Cladodes
by Sonia Labidi, Adrien Servent, Ghofran Bouzoumita, Tina Julien, Guillaume Cazals, Manel Ibrahim, Sofiène B. M. Hammami and Nawel Achir
Agriculture 2025, 15(17), 1902; https://doi.org/10.3390/agriculture15171902 - 8 Sep 2025
Abstract
The effects of arbuscular mycorrhizal fungi (AMF) inoculation on the chemical composition of the fruits and cladodes of two Opuntia ficus-indica cultivars, characterized by their red and yellow fruit color, were investigated under field conditions. AMF treatment was found to significantly influence the [...] Read more.
The effects of arbuscular mycorrhizal fungi (AMF) inoculation on the chemical composition of the fruits and cladodes of two Opuntia ficus-indica cultivars, characterized by their red and yellow fruit color, were investigated under field conditions. AMF treatment was found to significantly influence the concentration of phytonutrients in the fruits. The concentrations of betacyanin and betaxanthin increased by 1.2- and 1.9-fold in red and yellow fruits, respectively. The polyphenol content increased by 50%, with piscidic acid being the most abundant polyphenol in the red fruits. A similar increase in ascorbic acid was observed in the yellow fruits. Regarding the cladodes, AMF treatment was found to significantly affect macronutrient levels, with glucose and fructose contents being 90% and 34% higher, respectively. Additionally, cladodes from plants grown with AMF inoculation showed a 20% increase in ascorbic acid and phosphorus. These results demonstrate cultivar- and part-of-plant-dependent effects of AMF inoculation and confirm the nutritional and sustainable potential of Opuntia ficus-indica, particularly when coupled with mycorrhizal biofertilization practices. Full article
(This article belongs to the Section Agricultural Product Quality and Safety)
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16 pages, 2611 KB  
Article
Identification of Allelochemicals in Ficus carica L. and Their Stimulatory Effects on Isatis indigotica Fort. Growth
by Yaru Zhang, Xinle Li, Meiting Yu, Kaijia Xue, Yujiao Song, Chufan Mo, Chunjian Zhao and Chunying Li
Forests 2025, 16(9), 1380; https://doi.org/10.3390/f16091380 - 28 Aug 2025
Viewed by 361
Abstract
Medicinal agroforestry system contributes to enhancing agricultural productivity. In this process, allelochemicals play a crucial role, and certain allelochemicals can even promote the growth of intercropped plants significantly. Previous studies by our group have shown that fig tree (Ficus carica L.) extract [...] Read more.
Medicinal agroforestry system contributes to enhancing agricultural productivity. In this process, allelochemicals play a crucial role, and certain allelochemicals can even promote the growth of intercropped plants significantly. Previous studies by our group have shown that fig tree (Ficus carica L.) extract promotes woad (Isatis indigotica Fort.) growth significantly. However, the specific mechanism by which fig tree influences the growth of woad remains unclear. In this study, we demonstrated the growth-promoting effects of fig tree extract on woad through sterile seedling cultivation experiments and identified three allelochemicals—psoralen, bergapten, and umbelliferone. To further validate the growth-promoting activity of these compounds, a pot experiment was conducted by exogenously applying the three allelochemicals. The results revealed that all three allelochemicals derived from fig tree exhibited a property of concentration dependence on the growth of woad seedlings. Specifically, it shows an obvious promoting effect at the low concentration, while exhibiting inhibiting effects at high concentrations. Among them, the magnitude of the promoting effect, from strongest to weakest, was as follows: bergapten, psoralen, and umbelliferon. This study primarily aimed to elucidate the growth-promoting effect of woad induced by allelochemicals present in fig tree extracts and to clarify how these allelochemicals regulate woad growth. Full article
(This article belongs to the Section Forest Ecophysiology and Biology)
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20 pages, 2743 KB  
Article
Extraction of Ficus carica Polysaccharide by Ultrasound-Assisted Deep Eutectic Solvent-Based Three-Phase Partitioning System: Process Optimization, Partial Structure Characterization, and Antioxidant Properties
by Qisen Sun, Zhubin Song, Fanghao Li, Xinyu Zhu, Xinyu Zhang and Hao Chen
Molecules 2025, 30(17), 3469; https://doi.org/10.3390/molecules30173469 - 23 Aug 2025
Viewed by 598
Abstract
An innovative ultrasound-assisted deep eutectic solvent-based three-phase partitioning (UA-DES-TPP) system was developed for the sustainable extraction of Ficus carica polysaccharide (FCP). Using a hydrophobic DES composed of dodecanoic acid and octanoic acid (1:1 molar ratio), a phase behavior-driven separation mechanism was established. The [...] Read more.
An innovative ultrasound-assisted deep eutectic solvent-based three-phase partitioning (UA-DES-TPP) system was developed for the sustainable extraction of Ficus carica polysaccharide (FCP). Using a hydrophobic DES composed of dodecanoic acid and octanoic acid (1:1 molar ratio), a phase behavior-driven separation mechanism was established. The system was systematically optimized through single-factor experiments and response surface methodology (RSM), achieving a maximum FCP yield of 9.22 ± 0.20% under optimal conditions (liquid–solid ratio 1:24.2 g/mL, top/bottom phase volume ratio 1:1.05 v/v, ammonium sulfate concentration 25.8%). Structural characterization revealed that FCP was a heteropolysaccharide primarily composed of glucose and mannose with α/β-glycosidic linkages and a loose fibrous network. Remarkably, the DESs demonstrated excellent recyclability over five cycles. Furthermore, FCP exhibited significant concentration-dependent antioxidant activities: 82.3 ± 3.8% DPPH radical scavenging at 8 mg/mL, 76.8 ± 0.8% ABTS+ scavenging, and ferric ion reducing power of 45.53 ± 1.07 μmol TE/g. This study provides a new path for the efficient and sustainable extraction of bioactive macromolecules. Full article
(This article belongs to the Special Issue Natural Antioxidants in Functional Food)
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24 pages, 1972 KB  
Article
Identification, Quantification, and Antioxidant Evaluation of Phenolic Compounds from Colored Opuntia ficus-indica (L.) Roots Using UHPLC-DAD-ESI-MS/MS
by Elias Benramdane, Ahmad Mustafa, Nadia Chougui, Nawal Makhloufi, Abderezak Tamendjari and Cassamo U. Mussagy
Antioxidants 2025, 14(8), 1023; https://doi.org/10.3390/antiox14081023 - 21 Aug 2025
Viewed by 680
Abstract
This study investigates the phenolic composition and antioxidant potential of root extracts from three Opuntia ficus-indica varieties (green, red, and orange) using ultra-high-performance liquid chromatography coupled with diode array detection and electrospray ionization–tandem mass spectrometry (UHPLC-DAD-ESI-MS/MS). Phenolic compounds were extracted with a hydromethanolic [...] Read more.
This study investigates the phenolic composition and antioxidant potential of root extracts from three Opuntia ficus-indica varieties (green, red, and orange) using ultra-high-performance liquid chromatography coupled with diode array detection and electrospray ionization–tandem mass spectrometry (UHPLC-DAD-ESI-MS/MS). Phenolic compounds were extracted with a hydromethanolic solvent and quantified by spectrophotometric assays, while antioxidant activity was assessed through DPPH, ABTS, iron III reduction, hydroxyl radical, and nitric oxide scavenging methods. A total of 26 compounds were identified, including piscidic acid, epicatechin-3-O-gallate, and isovitexin, with several phenolics newly reported for O. ficus-indica roots. The green and red varieties showed the highest phenolic contents (up to 147.82 mg/g extract) and strong antioxidant capacity, particularly in ABTS (IC50 = 29.38 μg/mL) and hydroxyl radical inhibition (>90%). Relative Antioxidant Capacity Index (RACI) analysis confirmed a consistent correlation between phenolic/flavonoid content and antioxidant efficacy. These findings highlight the analytical relevance of UHPLC-DAD-ESI-MS/MS for profiling underutilized plant matrices and support the potential use of O. ficus-indica root extracts as natural sources of bioactive compounds for pharmaceutical and biomedical applications. Full article
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17 pages, 1768 KB  
Article
Oral Administration of an Opuntia ficus-indica Fruit Extract Induces Changes in Gut Microbiota Composition: Relationship with Its Anti-Obesity and Anti-Steatotic Effects in Rats Fed a High-Fat High-Fructose Diet
by Iker Gómez-García, Irene Besné-Eseverri, Maria P. Portillo, Alfredo Fernández-Quintela, Ligia Esperanza Díaz, Jose I. Riezu-Boj, Fermín I. Milagro and Jenifer Trepiana
Foods 2025, 14(16), 2891; https://doi.org/10.3390/foods14162891 - 20 Aug 2025
Viewed by 508
Abstract
Diseases such as obesity and metabolic-dysfunction-associated fatty liver disease (MAFLD) are often associated with changes in gut microbiota composition. The present study aims to investigate the relationship between the potential preventive effects of an Opuntia ficus-indica var. colorada cactus pulp extract on obesity [...] Read more.
Diseases such as obesity and metabolic-dysfunction-associated fatty liver disease (MAFLD) are often associated with changes in gut microbiota composition. The present study aims to investigate the relationship between the potential preventive effects of an Opuntia ficus-indica var. colorada cactus pulp extract on obesity and hepatic steatosis, and changes in gut microbiota composition, in a murine model fed a high-fat high-fructose diet. The low-dose extract was the most effective in reducing hepatic TG (−12.5%) and the weight of subcutaneous and visceral adipose tissue (−18.4% and 11.4%, respectively), while the high dose led to improved serum lipid profile (−74.2% in TG, −37.2% in total cholesterol, −50.5% in non-HDL cholesterol and +71.7% in HDL cholesterol). Opuntia extract supplementation did not prevent the dysbiosis in gut microbiota produced by the high-fat high-fructose diet. However, modifications in its composition, consistent with an increment in both Adlercreutzia muris and Cutibacterium acnes, and a reduction in Massiliimalia timonensis, were observed. It can be proposed that these changes may contribute to the extract effects against obesity and liver steatosis. Nevertheless, further research is required to establish a direct link between the anti-obesity and anti-steatotic effects and the functionality of the bacteria modified by the treatment. Full article
(This article belongs to the Special Issue Functional Foods, Gut Microbiota, and Health Benefits)
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23 pages, 10475 KB  
Article
Flavonoids from Ficus pandurate var. angustifolia W.C. Cheng Restore Cognitive Impairment and Regulate the Gut Microbiota in Sleep-Deprived Mice
by Haochen Dai, Songmei Luo and Xin Zhang
Foods 2025, 14(16), 2888; https://doi.org/10.3390/foods14162888 - 20 Aug 2025
Viewed by 394
Abstract
Sleep deprivation (SD) induces cognitive impairment associated with gut microbiota dysbiosis, making it crucial to explore natural remedies targeting the microbiota–gut–brain axis. This study aims to investigate whether Ficus pandurata var. angustifolia W.C. Cheng (a traditional medicine–food plant rich in flavonoids) can mitigate [...] Read more.
Sleep deprivation (SD) induces cognitive impairment associated with gut microbiota dysbiosis, making it crucial to explore natural remedies targeting the microbiota–gut–brain axis. This study aims to investigate whether Ficus pandurata var. angustifolia W.C. Cheng (a traditional medicine–food plant rich in flavonoids) can mitigate cognitive impairment caused by SD by modulating the gut microbiota. The sleep-deprived mouse model was established using the multiple platform water environment method. This study investigated the effects of F. pandurata var. angustifolia flavonoids (FCFs) via behavioral tests, 16S rRNA sequencing, and biochemical analyses to assess cognitive function, gut microbiota, and related pathways. FCF alleviated SD-induced cognitive deficits, reversed gut microbiota dysbiosis (increased beneficial bacteria like Lactobacillus, reduced harmful ones like Desulfovibrio), promoted short-chain fatty acids production, improved colonic histopathology and intestinal barrier function, reduced serum lipopolysaccharide, inhibited glial cell activation and TLR4/NF-κB signaling, and regulated neurotransmitters. In conclusion, FCF ameliorates SD-induced cognitive impairment through regulating gut microbiota, enhancing intestinal barrier, and suppressing neuroinflammation via the microbiota–gut–brain axis, providing a theoretical basis for its application. Full article
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22 pages, 2722 KB  
Article
Optically Active, Chlorophyll-Based Fluorescent Dye from Calabrian Opuntia ficus-indica Cladodes for Sustainable Applications
by Antonio Ferraro, Rita Guzzi, Sephora Kamwe Sighano, Giuseppe Nicoletta, Roberto Caputo, Franco Cofone, Giovanni Desiderio and Oriella Gennari
Sustainability 2025, 17(16), 7504; https://doi.org/10.3390/su17167504 - 20 Aug 2025
Viewed by 410
Abstract
Using ultrasound-assisted extraction, we obtained a chlorophyll-rich extract from Opuntia ficus-indica cladodes (OFI) characterized through thin-layer chromatography (TLC), Fourier-transform infrared spectroscopy (FTIR), and spectrophotometric absorption analysis. The dye exhibited a strong fluorescence response in the visible range (400–800 nm) with a [...] Read more.
Using ultrasound-assisted extraction, we obtained a chlorophyll-rich extract from Opuntia ficus-indica cladodes (OFI) characterized through thin-layer chromatography (TLC), Fourier-transform infrared spectroscopy (FTIR), and spectrophotometric absorption analysis. The dye exhibited a strong fluorescence response in the visible range (400–800 nm) with a pronounced red emission when excited with a UV source. Antioxidant ability was evaluated via DPPH assay, showing an IC50 of 185 µg/mL, highlighting its potential for reactive oxygen species scavenging. The extract was incorporated into polymethyl methacrylate (PMMA), polyvinylpyrrolidone (PVP), and polyvinyl alcohol (PVA), leading to fluorescence intensity enhancements of up to 40 times compared to the dye alone depending on matrix polarity, consistent with aggregation and polarity effects. Stability tests confirmed the dye’s resistance to CO2 exposure, pH variations, and prolonged storage, positioning it as a viable alternative to synthetic fluorophores. These findings suggest that the OFI extract provides a functionally relevant, bio-derived dye platform promoting the valorization of agricultural by-products in high-value technological applications, highlighting a circular and scalable approach to developing ecofriendly fluorescent materials, aligning with sustainability and green technology goals. Full article
(This article belongs to the Special Issue Resource Sustainability: Sustainable Materials and Green Engineering)
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14 pages, 1252 KB  
Article
Rubber-Ficus hirta Vahl. Agroforestry System Enhances Productivity and Resource Utilization Efficiency and Reduces Carbon Footprint
by Jian Pan, Xiu Zeng, Zhengfan Tian, Yan Zhang, Yuanran Xian, Hanqi Tu, Jianxiong Huang and Xiuquan Wang
Agriculture 2025, 15(16), 1750; https://doi.org/10.3390/agriculture15161750 - 15 Aug 2025
Viewed by 389
Abstract
Developing a more productive, resource-efficient, and climate-smart rubber agroforestry model is essential for the sustainable growth of natural rubber cultivation. In this study, we evaluated whether a double-row rubber plantation intercropped with the medicinal crop Ficus hirta Vahl. (DR-F) could achieve this goal, [...] Read more.
Developing a more productive, resource-efficient, and climate-smart rubber agroforestry model is essential for the sustainable growth of natural rubber cultivation. In this study, we evaluated whether a double-row rubber plantation intercropped with the medicinal crop Ficus hirta Vahl. (DR-F) could achieve this goal, using a single-row rubber plantation (SR) as the control. We assessed the feasibility of the DR-F system based on productivity, solar utilization efficiency (SUE), partial factor productivity of applied nitrogen (PFPN), carbon efficiency (CE), net ecosystem carbon balance (NECB), and carbon footprint (CF). No significant difference was observed in rubber tree biomass between the DR-F (10.49 t·ha−1) and SR (8.49 t·ha−1) systems. However, the DR-F system exhibited significantly higher total biomass productivity (23.34 t·ha−1) than the SR systems due to the substantial contribution from intercropped Ficus hirta Vahl., which yielded 12.84 t·ha−1(p < 0.05). The root fresh weight yield of Ficus hirta Vahl. reached 17.55 t·ha−1, generating an additional profit of 20,417 CNY ha−1. The DR-F system also exhibited higher solar radiation interception and greater availability of soil nutrients. Notably, the roots of rubber trees and Ficus hirta Vahl. did not overlap at a 4 m distance from the rubber trees. The DR-F system achieved higher SUE (0.64%), PFPN (51.40 kg·kg−1 N), and CE (6.93 kg·kg−1 C) than the SR system, with the SUE and PFPN differences being statistically significant (p < 0.05). Although the NECB remained unaffected, the DR-F system demonstrated significantly higher productivity and a substantially lower CF (0.33 kg CO2·kg−1, a 56% reduction; p < 0.05). In conclusion, the DR-F system represents a more sustainable and beneficial agroforestry approach, offering improved productivity, greater resource use efficiency, and reduced environmental impact. Full article
(This article belongs to the Special Issue Detection and Management of Agricultural Non-Point Source Pollution)
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17 pages, 2994 KB  
Article
Dyeing and Functional Finishing of Cotton Fabric Using Ficus carica and Eucalyptus Leaf Extracts with Aloe barbadensis Miller as a Bio-Mordant
by Imran Ahmad Khan, Hafsa Khalid, Kashif Javed, Ahmad Fraz, Khalid Pasha and Asfandyar Khan
Resources 2025, 14(8), 127; https://doi.org/10.3390/resources14080127 - 11 Aug 2025
Viewed by 535
Abstract
This study explores the sustainable extraction and application of natural dyes from figs (Ficus carica) and Eucalyptus leaves using an aqueous alkaline medium. The dyeing process was optimized for cotton fabric using the exhaust-dyeing method. Fabrics dyed with Ficus carica extract [...] Read more.
This study explores the sustainable extraction and application of natural dyes from figs (Ficus carica) and Eucalyptus leaves using an aqueous alkaline medium. The dyeing process was optimized for cotton fabric using the exhaust-dyeing method. Fabrics dyed with Ficus carica extract and its blend with Eucalyptus exhibited enhanced color strength, excellent crocking fastness (rated 4–5), and good washing fastness (rated 3–4 on the gray scale). The use of Aloe barbadensis Miller as a bio-mordant significantly improved dye fixation, resulting in deeper, earthy shades, such as green, yellow–green, and yellowish brown. The highest K/S value (5.85) was recorded in samples treated with a mordant, sodium chloride (NaCl), and the combined dye extracts, indicating a synergistic effect among the components. Mosquito repellency tests revealed that treated fabrics exhibited up to 70% repellency, compared to just 20% in undyed samples. Antibacterial testing against E. coli showed that dyed fabrics achieved over 80% bacterial reduction after 24 h, indicating promising antimicrobial functionality. Air permeability slightly decreased post-dyeing due to the potential shrinkage in cotton fabrics. Furthermore, adsorption studies showed a removal efficiency of 57% for Ficus carica dye on graphene oxide (GO) under ultrasonication. These findings confirm the potential of GO as an effective adsorbent material for treating wastewater from natural textile dyes. Overall, the study highlights the environmental safety, functional performance, and multifunctional advantages of plant-based dyeing systems in sustainable textile applications. Full article
(This article belongs to the Special Issue Alternative Use of Biological Resources)
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20 pages, 2063 KB  
Article
Chemometric Evaluation of 16 Priority PAHs in Soil and Roots of Syringa vulgaris and Ficus carica from the Bor Region (Serbia): An Insight into the Natural Plant Potential for Soil Phytomonitoring and Phytoremediation
by Aleksandra D. Papludis, Slađana Č. Alagić, Snežana M. Milić, Jelena S. Nikolić, Snežana Č. Jevtović, Vesna P. Stankov Jovanović and Gordana S. Stojanović
Environments 2025, 12(8), 256; https://doi.org/10.3390/environments12080256 - 28 Jul 2025
Viewed by 474
Abstract
The soil phytomonitoring and phytostabilization potential of Syringa vulgaris and Ficus carica was evaluated regarding 16 priority polycyclic aromatic hydrocarbons (PAHs) using a chemometric approach and the calculation of bioconcentration factors (BCFs) for each individual PAH in plants’ roots from each selected location [...] Read more.
The soil phytomonitoring and phytostabilization potential of Syringa vulgaris and Ficus carica was evaluated regarding 16 priority polycyclic aromatic hydrocarbons (PAHs) using a chemometric approach and the calculation of bioconcentration factors (BCFs) for each individual PAH in plants’ roots from each selected location in the Bor region. PAHs in roots and the corresponding soils were analyzed using the QuEChERS (Quick, Effective, Cheap, Easy, Rugged, Safe) method with some new modifications, gas chromatography/mass spectrometry, Pearson’s correlation study, hierarchical cluster analysis, and BCFs. Several central conclusions are as follows: Each plant species developed its own specific capability for PAH management, and root concentrations ranged from not detected (for several compounds) to 5592 μg/kg (for fluorene in S. vulgaris). In some cases, especially regarding benzo(a)pyrene and chrysene, both plants had a similar tactic—the total avoidance of assimilation (probably due to their high toxicity). Both plants retained significant quantities of different PAHs in their roots (many calculated BCFs were higher than 1 or were even extremely high), which recommends them for PAH phytostabilization (especially fluorene, benzo(b)fluoranthene, and benzo(k)fluoranthene). In soil monitoring, neither of the plants are helpful because their roots do not reflect the actual situation found in soil. Finally, the analysis of the corresponding soils provided useful monitoring information. Full article
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22 pages, 2408 KB  
Article
Postharvest Quality of Parthenocarpic and Pollinated Cactus Pear [Opuntia ficus-indica L. (Mill)] Fruits
by Berenice Karina Flores-Hernández, Ma. de Lourdes Arévalo-Galarza, Manuel Livera-Muñoz, Cecilia Peña-Valdivia, Aída Martínez-Hernández, Guillermo Calderón-Zavala and Guadalupe Valdovinos-Ponce
Foods 2025, 14(14), 2546; https://doi.org/10.3390/foods14142546 - 21 Jul 2025
Viewed by 545
Abstract
Opuntia ficus-indica L. (Mill) belongs to the Cactaceae family. The plant produces edible and juicy fruits called cactus pear, recognized for their pleasant flavor and functional properties. However, the fruits have a short shelf life, hard seeds, and the presence of glochidia in [...] Read more.
Opuntia ficus-indica L. (Mill) belongs to the Cactaceae family. The plant produces edible and juicy fruits called cactus pear, recognized for their pleasant flavor and functional properties. However, the fruits have a short shelf life, hard seeds, and the presence of glochidia in the pericarpel. Recently, by inducing parthenocarpy, seedless fruits of cactus pear have been obtained. They have attractive colors, soft and small seminal residues, with a similar flavor to their original seeded counterparts. Nevertheless, their postharvest physiological behavior has not yet been documented. The aim of this study was to compare the biochemical, anatomical, and physiological characteristics of pollinated fruits, CP30 red and CP40 yellow varieties, with their parthenocarpic counterparts (CP30-P and CP40-P), obtained by the application of growth regulators in preanthesis. Fruits of each type were harvested at horticultural maturity, and analyses were carried out on both pulp and pericarpel (peel), using a completely randomized design. Results showed that red fruits CP30 and CP30-P showed higher concentrations of betacyanins in pulp (13.4 and 18.4 mg 100 g−1 FW) and in pericarpel (25.9 and 24.1 mg 100 g−1 FW), respectively; flavonoid content was significantly higher in partenocarpic fruits compared with the pollinated ones. Parthenocarpy mainly affected the shelf life, in pollinated fruits, CP30 was 14 days but 32 days in CP30-P; for CP40, it was 16 days, and 30 days in CP40-P. Also, the partenocarpic fruits were smaller but with a thicker pericarpel, and lower stomatal frequency. Overall, parthenocarpic fruits represent a viable alternative for commercial production due to their extended shelf life, lower weight loss, and soft but edible pericarpel. Full article
(This article belongs to the Section Food Quality and Safety)
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15 pages, 5557 KB  
Article
Rheological and Physical Properties of Mucilage Hydrogels from Cladodes of Opuntia ficus-indica: Comparative Study with Pectin
by Federica Torregrossa, Matteo Pollon, Giorgia Liguori, Francesco Gargano, Donatella Albanese, Francesca Malvano and Luciano Cinquanta
Gels 2025, 11(7), 556; https://doi.org/10.3390/gels11070556 - 19 Jul 2025
Viewed by 507
Abstract
The physical and rheological properties of mucilage hydrogels derived from the cladodes of Opuntia ficus-indica (L. Mill) were compared with those of commercial pectin for potential applications in the food industry. All hydrogels—formulated by incorporating sucrose and either calcium chloride or calcium carbonate [...] Read more.
The physical and rheological properties of mucilage hydrogels derived from the cladodes of Opuntia ficus-indica (L. Mill) were compared with those of commercial pectin for potential applications in the food industry. All hydrogels—formulated by incorporating sucrose and either calcium chloride or calcium carbonate to promote favorable gel network formation—exhibited pseudoplastic (shear-thinning) behavior. The flow characteristics of the hydrogels prepared with mucilage or pectin conformed to the Casson fluid model. Moreover, all samples consistently displayed loss modulus (G″) values exceeding their corresponding storage modulus (G′) values, indicating a dominant viscous behavior over elastic properties. The ζ-potential of all samples was negative across the pH range studied. Mucilage-based samples exhibited lower ionizability per unit mass and reduced phase stability compared to those containing pectin. Principal component analysis (PCA) revealed that mucilage hydrogels exhibited multivariate profiles similar to pectin hydrogels containing calcium carbonate, though the latter demonstrated greater polydispersity than standard pectic gels. Infrared spectroscopy further highlighted distinct spectral differences between pectins and mucilages, offering valuable insights into their respective functional characteristics. Collectively, these findings underscore the potential of Opuntia ficus-indica mucilages as viable additives in food formulations. Full article
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15 pages, 1498 KB  
Article
Host-Affected Body Coloration Dynamics in Perina nuda Larvae: A Quantitative Analysis of Color Variations and Endogenous Plant Influences
by Songkai Liao, Xinjie Mao, Yuan Liu, Guihua Luo, Jiajin Wang, Haoyu Lin, Ming Tang and Hui Chen
Insects 2025, 16(7), 728; https://doi.org/10.3390/insects16070728 - 17 Jul 2025
Viewed by 508
Abstract
Insects’ body coloration may be indirectly influenced by their host plants. Perina nuda (Lepidoptera: Lymantriidae), commonly known as the Banyan Tussock Moth and a serious pest of banyan trees (Ficus spp.) in southern China, exhibits light body coloration during its first- to [...] Read more.
Insects’ body coloration may be indirectly influenced by their host plants. Perina nuda (Lepidoptera: Lymantriidae), commonly known as the Banyan Tussock Moth and a serious pest of banyan trees (Ficus spp.) in southern China, exhibits light body coloration during its first- to third-instar stages, with its coloration progressively darkening as it matures, but little is known of the relationship between larval body coloration and host plants. To address this gap, we examined the R (red), G (green), B (blue), and L (lightness) values of the head, dorsal thorax and abdomen, stripe, dorsal mid-line, and tail of larvae fed on different hosts and host endogenous substance by using quantitative image analysis and chemical determination. Our results revealed that larval body coloration exhibited conserved ontogenetic patterns but varied significantly with host species, developmental age, and anatomical region. Redundancy analysis identified chlorophyll-b as the dominant driver, strongly associating with dorsal thorax–abdomen pigmentation. Flavonoids exhibited subthreshold significance, correlating with darker dorsal mid-line coloration, while nutrients (sugars, proteins) showed negligible effects. Linear regression revealed weak but significant links between leaf and larval body coloration in specific body regions. These findings demonstrate that host plant endogenous substances play a critical role in shaping larval body coloration. This study provides a foundation for understanding the ecological and biochemical mechanisms underlying insect pigmentation, with implications for adaptive evolution and pest management strategies. Full article
(This article belongs to the Special Issue Ecological Adaptation of Insect Pests)
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22 pages, 1279 KB  
Review
State of the Art of Biomethane Production in the Mediterranean Region
by Antonio Comparetti, Salvatore Ciulla, Carlo Greco, Francesco Santoro and Santo Orlando
Agronomy 2025, 15(7), 1702; https://doi.org/10.3390/agronomy15071702 - 15 Jul 2025
Viewed by 659
Abstract
The Mediterranean region is increasingly confronted with intersecting environmental, agricultural, and socio-economic challenges, including biowaste accumulation, soil degradation, and high dependency on imported fossil fuels. Biomethane, a renewable substitute for natural gas, offers a strategic solution that aligns with the region’s need for [...] Read more.
The Mediterranean region is increasingly confronted with intersecting environmental, agricultural, and socio-economic challenges, including biowaste accumulation, soil degradation, and high dependency on imported fossil fuels. Biomethane, a renewable substitute for natural gas, offers a strategic solution that aligns with the region’s need for sustainable energy transition and circular resource management. This review examines the current state of biomethane production in the Mediterranean area, with a focus on anaerobic digestion (AD) technologies, feedstock availability, policy drivers, and integration into the circular bioeconomy (CBE) framework. Emphasis is placed on the valorisation of regionally abundant feedstocks such as olive pomace, citrus peel, grape marc, cactus pear (Opuntia ficus-indica) residues, livestock manure, and the Organic Fraction of Municipal Solid Waste (OFMSW). The multifunctionality of AD—producing renewable energy and nutrient-rich digestate—is highlighted for its dual role in reducing greenhouse gas (GHG) emissions and restoring soil health, especially in areas threatened by desertification such as Sicily (Italy), Spain, Malta, and Greece. The review also explores emerging innovations in biogas upgrading, nutrient recovery, and digital monitoring, along with the role of Renewable Energy Directive III (RED III) and national biomethane strategies in scaling up deployment. Case studies and decentralised implementation models underscore the socio-technical feasibility of biomethane systems across rural and insular territories. Despite significant potential, barriers such as feedstock variability, infrastructural gaps, and policy fragmentation remain. The paper concludes with a roadmap for research and policy to advance biomethane as a pillar of Mediterranean climate resilience, energy autonomy and sustainable agriculture within a circular bioeconomy paradigm. Full article
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