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Keywords = bonding tray

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13 pages, 465 KB  
Systematic Review
Bond Strength of Impression Materials to Conventional and Additively Manufactured Custom Tray Materials: A Systematic Review
by Petra Clarkson, Xiaoyun Liu, Andrew B. Cameron, John M. Aarts and Joanne J. E. Choi
Oral 2025, 5(3), 70; https://doi.org/10.3390/oral5030070 - 8 Sep 2025
Viewed by 671
Abstract
Purpose: We aimed to systematically review the current literature on the bond strength between custom tray materials and impression materials, including the various parameters affecting the strength. Methods: Four electronic databases were used: Ovid, Web of Science, PubMed, and Scopus. Relevant studies were [...] Read more.
Purpose: We aimed to systematically review the current literature on the bond strength between custom tray materials and impression materials, including the various parameters affecting the strength. Methods: Four electronic databases were used: Ovid, Web of Science, PubMed, and Scopus. Relevant studies were chosen based on their eligibility, determined through inclusion and exclusion criteria. This review followed the PRISMA strategy. A risk of bias assessment was produced to evaluate the validity of each study. Results: There were 173 initial relevant studies identified, and after the screening process, this was reduced to seven. Two additional studies were also included from hand searching, resulting in total nine studies to be included in the review. Four of the nine evaluated studies concerned additively manufactured (AM) materials, including acrylonitrile butadiene styrene (ABS), polyethylene terephthalate glycol polyester (PETG), high-impact polystyrene (HIPS), and polylactic acid (PLA). Five studies evaluated an auto-polymerizing resin and one a thermoplastic material. All studies used polyvinyl siloxane impression materials and an adhesive selection following manufacturers’ recommendations. Three studies used scanning electron microscopy (SEM) to analyze their specimens. All studies reported a low risk of bias. Conclusions: Surface roughening was shown to reduce the strength of the bonding interface, whereas combining chemical and mechanical retention was shown to increase the bond strength. Inconsistent results exist in determining if AMed (3D-printed) tray materials are comparable or perform better than the conventional tray materials, highlighting the need for further study. Clinical Significance: The bond strength of the custom tray to the dental impression material is critical as it affects the model produced and therefore the final prosthesis. It is therefore invaluable to use materials with high bond strength for the construction of custom trays. Full article
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14 pages, 1148 KB  
Article
AI-Assisted Design of 3D-Printed Lingual Indirect Bonding Trays: A Comparative Evaluation of Bracket Transfer Accuracy
by Viet Hoang, Thi Quynh Trang Vuong, Phuong Huyen Nguyen, Nhu Hai Pham, Kim Loan Hoang, Thi Thu Trang Hoang, Tuan Khang Nguyen, Thi Hong Thuy Pham and Viet Anh Nguyen
J. Clin. Med. 2025, 14(12), 4303; https://doi.org/10.3390/jcm14124303 - 17 Jun 2025
Cited by 2 | Viewed by 914
Abstract
Objectives: This study investigated the use of artificial intelligence (AI) in the design of lingual bracket indirect bonding trays and its association with bracket transfer accuracy using three-dimensional (3D) printing. Methods: Digital impressions of patient’s dental arches were captured using an intraoral scanner, [...] Read more.
Objectives: This study investigated the use of artificial intelligence (AI) in the design of lingual bracket indirect bonding trays and its association with bracket transfer accuracy using three-dimensional (3D) printing. Methods: Digital impressions of patient’s dental arches were captured using an intraoral scanner, and orthodontic setups were virtually constructed. Brackets were virtually positioned in their ideal locations using the digital setups guided by virtual archwire templates. Indirect bonding trays were automatically generated using the AI-powered Auto Creation function of the Medit Splints application, which analyzes anatomical features to streamline design. Bracket transfer accuracy was evaluated in vivo by comparing planned and actual bracket positions across grouped and individual tray configurations. Linear and angular deviations were measured using conventional 3D inspection software. Results: Most bracket transfer errors were within clinically acceptable thresholds, although torque accuracy remained suboptimal. Grouped trays generally exhibited greater precision than individual trays in several dimensions. Conclusions: These findings support the application of AI-assisted design tools to enhance digital workflows and improve consistency in appliance fabrication. Full article
(This article belongs to the Special Issue Latest Advances in Orthodontics)
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11 pages, 4618 KB  
Article
Accuracy of One-Piece vs. Segmented Three-Dimensional Printed Transfer Trays for Indirect Bracket Placement
by Bayan Alyammahi, Amar Hassan Khamis and Ahmed Ghoneima
Dent. J. 2024, 12(11), 352; https://doi.org/10.3390/dj12110352 - 31 Oct 2024
Viewed by 1963
Abstract
Objective: To assess the accuracy of three-dimensional (3D) printed one-piece vs. multiple segmented transfer trays for indirect bonding techniques in moderate and severe crowding cases. Methods: Eighty digital maxillary dental models were produced by an extraoral scanner. 3D-printed one-piece and segmented trays were [...] Read more.
Objective: To assess the accuracy of three-dimensional (3D) printed one-piece vs. multiple segmented transfer trays for indirect bonding techniques in moderate and severe crowding cases. Methods: Eighty digital maxillary dental models were produced by an extraoral scanner. 3D-printed one-piece and segmented trays were virtually designed utilizing Maestro 3D Ortho Studio® v4 and printed using a NextDent printer. The sample was classified into two groups: Group 1 (moderate crowding) included 40 digital models with a space deficiency of 6–7 mm, and Group 2 (severe crowding) included 40 digital models with a space deficiency of 10 mm. Ortho classic brackets were then placed into the 3D printed models with the aid of the transfer trays, and the models with the final bracket positioning were scanned using iTero scanner. Four measurements were selected on each tooth to perform the analysis. Mann–Whitney and Kruskal–Wallis tests were used for comparisons. A p-value of ≤ 0.05 was considered statistically significant. Results: In the moderate crowding group, statistically significant differences were detected between the one-piece, segmented, and control groups for three measurements (p < 0.001), while the rest of the measurements showed no significant differences (p > 0.05). In the severe crowding group, no significant differences were detected for any of the measurements. Conclusions: One-piece and segmented 3D-printed transfer trays are considered accurate tools for indirect bonding in moderate and severe malocclusion cases. The severity of crowding did not affect the accuracy of bracket transfer in indirect bonding. Full article
(This article belongs to the Special Issue Orthodontics and New Technologies: 2nd Edition)
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10 pages, 1794 KB  
Article
Comparison of Two Chosen 3D Printing Resins Designed for Orthodontic Use: An In Vitro Study
by Anna Paradowska-Stolarz, Joanna Wezgowiec and Marcin Mikulewicz
Materials 2023, 16(6), 2237; https://doi.org/10.3390/ma16062237 - 10 Mar 2023
Cited by 13 | Viewed by 3280
Abstract
(1) Background: In recent years, 3D printing has become a highly popular tool for manufacturing in various fields such as aviation, automobiles, plastics, and even medicine, including dentistry. Three-dimensional printing allows dentists to create high-precision models of teeth and jaw structure, and enables [...] Read more.
(1) Background: In recent years, 3D printing has become a highly popular tool for manufacturing in various fields such as aviation, automobiles, plastics, and even medicine, including dentistry. Three-dimensional printing allows dentists to create high-precision models of teeth and jaw structure, and enables them to develop customized tools for patients’ treatment. The range of resins used in dentistry is quite large, and this branch is developing rapidly; hence, studies comparing different resins are required. The present study aimed to compare the mechanical properties of two chosen resins used in dentistry. (2) Materials and methods: Ten specimens each of two types of 3D-printable resins (BioMed Amber and IBT, developed by Formlabs) were prepared. The samples were printed on a Formlabs Form 2 3D printer according to ISO standards. Samples for the compression test were rectangular in shape (10 ± 0.2 mm × 10 ± 0.2 mm × 4 ± 0.2 mm), while the samples used for the tensile test were dumbbell shaped (75 mm long, with 10 mm end width and 2 mm thickness). Tensile and compression tests of both materials were performed in accordance with the appropriate ISO standards. (3) Results: The BioMed Amber resin was more resistant to compression and tensile forces, thus implying that the resin could withstand higher stress during stretching, pulling, or pushing. The IBT resin was less resistant to such loads, and failure of this material occurred at lower forces than those for Biomed Amber. An ANOVA test confirmed that the observed differences were statistically significant (p < 0.001). (4) Conclusions: Based on the properties of both materials, the IBT resin could be better used as a tray for placing orthodontic brackets through an indirect bonding technique, while the BioMed Amber resin would be more useful as a surgical guide for placing dental implants and mini-implants. Further potential fields of application of the resins should be investigated. Full article
(This article belongs to the Special Issue Modern Materials Used in Dentistry - Review of XXI Century Knowledge)
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23 pages, 5591 KB  
Article
Modeling and Simulation of an Energy Integrated Distillation Column in a Bond Graph Approach
by Juancarlos Mendez-B, Gilberto Gonzalez-Avalos, Noe Barrera Gallegos, Gerardo Ayala-Jaimes and Carlos Rubio-Maya
Entropy 2022, 24(9), 1191; https://doi.org/10.3390/e24091191 - 25 Aug 2022
Cited by 4 | Viewed by 4265
Abstract
The bond graph methodology for modelling an integrated energy distillation column is applied in this paper. The distillation column is built by five trays for a binary mixture. However, due to its modular construction in a bond graph, the number of trays can [...] Read more.
The bond graph methodology for modelling an integrated energy distillation column is applied in this paper. The distillation column is built by five trays for a binary mixture. However, due to its modular construction in a bond graph, the number of trays can be increased. In order to link the analysis tools of systems modeled in the bond graph to the mathematical model given to a distillation column, a junction structure of the proposed bond graph is presented. Hence, this junction structure is a way to obtain the state space representation of the modeled column in bond graphs. Likewise, it is well known that distillation columns determine a class of nonlinear systems, so throughout this paper, these systems in a bond graph approach can be analyzed. In order to learn the behavior of the distillation column in the physical domain, simulation results using 20-Sim software are shown. In addition, with the simulation of two case studies consisting of two mixtures with different relative volatilities, the versatility of the column model in a bond graph is presented. In both cases, the increase in the feed flow, the mole fraction of the light component in the feed or the distillate reflux that enriches the concentration of light in the column determine an increase in the mole fraction of light in the distillate and in the bottom reflow. Further, the control design for a distillation column in the physical domain can be extended. Full article
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16 pages, 1828 KB  
Systematic Review
Bracket Transfer Accuracy with the Indirect Bonding Technique—A Systematic Review and Meta-Analysis
by Hisham Sabbagh, Yeganeh Khazaei, Uwe Baumert, Lea Hoffmann, Andrea Wichelhaus and Mila Janjic Rankovic
J. Clin. Med. 2022, 11(9), 2568; https://doi.org/10.3390/jcm11092568 - 4 May 2022
Cited by 24 | Viewed by 5507
Abstract
Purpose: To investigate the bracket transfer accuracy of the indirect bonding technique (IDB). Methods: Systematic search of the literature was conducted in PubMed MEDLINE, Web of Science, Embase, and Scopus through November 2021. Selection Criteria: In vivo and ex vivo studies investigating bracket [...] Read more.
Purpose: To investigate the bracket transfer accuracy of the indirect bonding technique (IDB). Methods: Systematic search of the literature was conducted in PubMed MEDLINE, Web of Science, Embase, and Scopus through November 2021. Selection Criteria: In vivo and ex vivo studies investigating bracket transfer accuracy by comparing the planned and achieved bracket positions using the IDB technique were considered. Information concerning patients, samples, and applied methodology was collected. Measured mean transfer errors (MTE) for angular and linear directions were extracted. Risk of bias (RoB) in the studies was assessed using a tailored RoB tool. Meta-analysis of ex vivo studies was performed for overall linear and angular bracket transfer accuracy and for subgroup analyses by type of tray, tooth groups, jaw-related, side-related, and by assessment method. Results: A total of 16 studies met the eligibility criteria for this systematic review. The overall linear mean transfer errors (MTE) in mesiodistal, vertical and buccolingual direction were 0.08 mm (95% CI 0.05; 0.10), 0.09 mm (0.06; 0.11), 0.14 mm (0.10; 0.17), respectively. The overall angular mean transfer errors (MTE) regarding angulation, rotation, torque were 1.13° (0.75; 1.52), 0.93° (0.49; 1.37), and 1.11° (0.68; 1.53), respectively. Silicone trays showed the highest accuracy, followed by vacuum-formed trays and 3D printed trays. Subgroup analyses between tooth groups, right and left sides, and upper and lower jaw showed minor differences. Conclusions and implications: The overall accuracy of the indirect bonding technique can be considered clinically acceptable. Future studies should address the validation of the accuracy assessment methods used. Full article
(This article belongs to the Topic State-of-the-Art Dentistry and Oral Health)
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13 pages, 4404 KB  
Article
Comparison of Two 3D-Printed Indirect Bonding (IDB) Tray Design Versions and Their Influence on the Transfer Accuracy
by Julius von Glasenapp, Eva Hofmann, Julia Süpple, Paul-Georg Jost-Brinkmann and Petra Julia Koch
J. Clin. Med. 2022, 11(5), 1295; https://doi.org/10.3390/jcm11051295 - 26 Feb 2022
Cited by 18 | Viewed by 5157
Abstract
Objective: This study aims to investigate the transfer accuracy of two different design versions for 3D-printed indirect bonding (IDB) trays. Materials and Methods: Digital plaster models of 27 patients virtually received vestibular attachments on every tooth using OnyxCeph³™ (Image Instruments, Chemnitz, Germany). Based [...] Read more.
Objective: This study aims to investigate the transfer accuracy of two different design versions for 3D-printed indirect bonding (IDB) trays. Materials and Methods: Digital plaster models of 27 patients virtually received vestibular attachments on every tooth using OnyxCeph³™ (Image Instruments, Chemnitz, Germany). Based on these simulated bracket and tube positions, two versions of transfer trays were designed for each dental arch and patient, which differed in the mechanism of bracket retention: Variant one (V1) had arm-like structures protruding from the tray base and reaching into the horizontal and vertical bracket slots, and variant two (V2) had a pocket-shaped design enclosing the brackets from three sides. Both tray designs were 3D-printed with the same digital light processing (DLP) printer using a flexible resin-based material (IMPRIMO® LC IBT/Asiga MAX™, SCHEU-DENTAL, Iserlohn, Germany). Brackets and tubes (discovery® smart/pearl, Ortho-Cast M-Series, Dentaurum, Ispringen, Germany) were inserted into the respective retention mechanism of the trays and IDB was performed on corresponding plaster models. An intraoral scan (TRIOS® 3W, 3Shape, Copenhagen, Denmark) was performed to capture the actual attachment positions and compared to the virtually planned positions with Geomagic© Control (3D Systems Inc., Rock Hill, SC, USA) using a scripted calculation tool, which superimposed the respective tooth surfaces. The resulting attachment deviations were determined in three linear (mesiodistal, vertical and orovestibular) and three angular (torque, rotation and tip) directions and analyzed with a descriptive statistical analysis. A comparison between the two IDB tray designs was conducted using a mixed model analysis (IBM, SPSS® Statistics 27, Armonk, NY, USA). Results: Both design versions of the 3D-printed IDB trays did not differ significantly in their transfer accuracy (p > 0.05). In total, 98% (V1) and 98.5% (V2) of the linear deviations were within the clinically acceptable range of ±0.2 mm. For the angular deviations, 84.9% (V1) and 86.8% (V2) were within the range of ±1°. With V1, most deviations occurred in the mesiodistal direction (3.3%) and in rotation (18%). With V2, most deviations occurred in the vertical direction (3.8%) and in palatinal and lingual crown torque (16.3%). Conclusions: The transfer accuracies of the investigated design versions for 3D-printed IDB trays show good and comparable results albeit their different retention mechanisms for the attachments and are, therefore, both suitable for clinical practice. Full article
(This article belongs to the Collection Digital Dentistry: Advances and Challenges)
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14 pages, 4592 KB  
Article
Transfer Accuracy of Two 3D Printed Trays for Indirect Bracket Bonding—An In Vitro Pilot Study
by Rebecca Jungbauer, Jonas Breunig, Alois Schmid, Mira Hüfner, Robert Kerberger, Nicole Rauch, Peter Proff, Dieter Drescher and Kathrin Becker
Appl. Sci. 2021, 11(13), 6013; https://doi.org/10.3390/app11136013 - 28 Jun 2021
Cited by 21 | Viewed by 4098
Abstract
The present study aimed to investigate the impact of hardness from 3D printed transfer trays and dental crowding on bracket bonding accuracy. Lower models (no crowding group: Little’s Irregularity Index (LII) < 3, crowding group: LII > 7, n = 10 per group) [...] Read more.
The present study aimed to investigate the impact of hardness from 3D printed transfer trays and dental crowding on bracket bonding accuracy. Lower models (no crowding group: Little’s Irregularity Index (LII) < 3, crowding group: LII > 7, n = 10 per group) were selected at random, digitized, 3D printed, and utilized for semiautomated virtual positioning of brackets and tubes. Hard and soft transfer trays were fabricated with polyjet printing and digital light processing, respectively. Brackets and tubes were transferred to the 3D printed models and altogether digitized using intraoral scanning (IOS) and microcomputed tomography (micro-CT) for assessment of linear and angular deviations. Mean intra- and interrater reliability amounted to 0.67 ± 0.34/0.79 ± 0.16 for IOS, and 0.92 ± 0.05/0.92 ± 0.5 for the micro-CT measurements. Minor linear discrepancies were observed (median: 0.11 mm, Q1–Q3: −0.06–0.28 mm). Deviations in torque (median: 2.49°, Q1–Q3: 1.27–4.03°) were greater than angular ones (median: 1.81°, Q1–Q3: 1.05°–2.90°), higher for hard (median: 2.49°, Q1–Q3: 1.32–3.91°) compared to soft (median: 1.77°, Q1–Q3: 0.94–3.01°) trays (p < 0.001), and torque errors were more pronounced at crowded front teeth (p < 0.05). In conclusion, the clinician should carefully consider the potential impact of hardness and crowding on bracket transfer accuracy, specifically in torque and angular orientation. Full article
(This article belongs to the Special Issue 3D Printed Materials Dentistry)
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5 pages, 210 KB  
Article
Occupational Methacrylate Allergy in Dental Personnel
by Norma Cameli, Maria Mariano, Flavia Pigliacelli, Martina Silvestri and Antonio Cristaudo
Allergies 2021, 1(2), 123-127; https://doi.org/10.3390/allergies1020010 - 7 Jun 2021
Cited by 2 | Viewed by 6216
Abstract
Purpose of the article: Acrylate and methacrylate (MA) use in the dental industry is widespread, being utilized in dental prostheses and composite resins, dentin bonding materials, and glass ionomers. However, occupational methacrylate allergy in dental personnel is a growing phenomenon. The aims of [...] Read more.
Purpose of the article: Acrylate and methacrylate (MA) use in the dental industry is widespread, being utilized in dental prostheses and composite resins, dentin bonding materials, and glass ionomers. However, occupational methacrylate allergy in dental personnel is a growing phenomenon. The aims of this retrospective observational study are to evaluate the risk of occupational contact dermatitis following exposure to methacrylates in dental personnel and to identify possible preventive measures. Materials and Methods: A total of 126 subjects exposed to acrylic and methacrylic resins in their professional context and who reported clinical manifestations were included from our outpatient department database. These were subdivided into two groups: 81 dental technicians and 45 dental hygienists. All the subjects had undergone patch testing with a “methacrylate series” (FIRMA) and readings were taken after 2 days (D2), 4 days (D4), and 7 days (D7). Results: A significantly higher incidence of methacrylate allergy was found in the dental technician group compared to the dental hygienists. Among the dental technicians, 40.7% of the subjects presented skin manifestations. The hands were the most frequently affected sites. Conclusion: Our results confirm the high sensitizing potential of MA in the workplace for dental personnel and in particular an increased professional risk in work where the hands are directly involved (dental technicians). Patch testing as an integrated part of a screening tray is needed for a complete evaluation of occupational skin allergy due to MA in dental personnel. The adoption of proper primary preventive measures, including gloves, protective eyewear, face shields, and disposable gowns, can be useful in preventing new cases of contact dermatitis, which may lead to a change of occupation in dental personnel. Full article
(This article belongs to the Section Dermatology)
13 pages, 7879 KB  
Article
Accurate Bracket Placement with an Indirect Bonding Method Using Digitally Designed Transfer Models Printed in Different Orientations—An In Vitro Study
by Julia Süpple, Julius von Glasenapp, Eva Hofmann, Paul-Georg Jost-Brinkmann and Petra Julia Koch
J. Clin. Med. 2021, 10(9), 2002; https://doi.org/10.3390/jcm10092002 - 7 May 2021
Cited by 23 | Viewed by 5533
Abstract
Objective: A digital workflow opens up new possibilities for the indirect bonding (IDB) of brackets. We tested if the printing orientation for bracket transfer models on the build platform of a 3D printer influences the accuracy of the following IDB method. We also [...] Read more.
Objective: A digital workflow opens up new possibilities for the indirect bonding (IDB) of brackets. We tested if the printing orientation for bracket transfer models on the build platform of a 3D printer influences the accuracy of the following IDB method. We also evaluated the clinical acceptability of the IDB method combining digitally planned and printed transfer models with the conventional fabrication of pressure-molded transfer trays. Materials and Methods: In total, 27 digitally planned bracket transfer models were printed with both 15° and 75° angulation from horizontal plane on the build platform of a digital light processing (DLP) printer. Brackets were temporarily bonded to the transfer models and pressure-molded trays were produced on them. IDB was then performed using the trays on the respective plaster models. The plaster models were scanned with an optical scanner. Digitally planned pre-bonding and scanned post-bonding bracket positions were superimposed with a software and resulted in three linear and three angular deviations per bracket. Results: No statistically significant differences of the transfer accuracy of printed transfer models angulated 15° or 75° on the 3D printer build platform were found. About 97% of the linear and 82% of the angular deviations were within the clinically acceptable range of ±0.2 mm and ±1°, respectively. The highest inaccuracies in the linear dimension occurred in the vertical towards the gingival direction and in the angular dimension in palatal crown torque. Conclusion: For the IDB method used, the printing orientation on the build platform did not have a significant impact on the transfer accuracy. Full article
(This article belongs to the Collection Digital Dentistry: Advances and Challenges)
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14 pages, 1673 KB  
Article
Formulation of a Bio-Packaging Based on Pure Cellulose Coupled with Cellulose Acetate Treated with Active Coating: Evaluation of Shelf Life of Pasta Ready to Eat
by Valeria Bugatti, Gianluca Viscusi and Giuliana Gorrasi
Foods 2020, 9(10), 1414; https://doi.org/10.3390/foods9101414 - 7 Oct 2020
Cited by 11 | Viewed by 4474
Abstract
An active packaging based on pure cellulose coupled with cellulose acetate coated with layered double hydroxide (LDH), hosting 4-hydroxybenzoate (listed in EC-Directive 10/2011) as an antimicrobial agent, was formulated and realized. The release of 4-hydroxybenzoate ionically bonded to the LDH layers was much [...] Read more.
An active packaging based on pure cellulose coupled with cellulose acetate coated with layered double hydroxide (LDH), hosting 4-hydroxybenzoate (listed in EC-Directive 10/2011) as an antimicrobial agent, was formulated and realized. The release of 4-hydroxybenzoate ionically bonded to the LDH layers was much slower than the molecule freely dispersed into the coating. The capability of the active packaging to inhibit Pseudomonas, Escherichia coli, Salmonella and Lactic Bacteria was evaluated, as well as the global migration with three different food simulant (i.e., acetic acid at 3% (v/v), ethanol at 50% (v/v) and vegetable oil) that demonstrated, in compliance with the migration limits of the EU regulation, the suitability of the prepared packaging to be employed as food contact material. Ready to east cooked tomato pasta was packaged into the active trays and in uncoated, as control, up to 30 days at 4 °C. Organoleptic characteristics, mold evolution, total mesophilic aerobic counts (TBC), Enterobacteriaceae, Lactic Bacteria and Pseudomonas, and in colony forming unit per gram (CFU/g), showed a significant activity of 4-hydroxybenzoate in increasing the shelf life of the pasta ready to eat. Full article
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13 pages, 2430 KB  
Article
Study on the Concentration of Acrylic Acid and Acetic Acid by Reverse Osmosis
by Qian Liu, Lixin Xie, Hanxiao Du, Shichang Xu and Yawei Du
Membranes 2020, 10(7), 142; https://doi.org/10.3390/membranes10070142 - 6 Jul 2020
Cited by 10 | Viewed by 4265
Abstract
In the production of acrylic acid, the concentration of acrylic acid solution from the adsorption tower was low, which would lead to significant energy consumption in the distillation process to purify acrylic acid, along with the production of a large amount of wastewater. [...] Read more.
In the production of acrylic acid, the concentration of acrylic acid solution from the adsorption tower was low, which would lead to significant energy consumption in the distillation process to purify acrylic acid, along with the production of a large amount of wastewater. Reverse osmosis (RO) was proposed to concentrate the acrylic acid aqueous solution taken from a specific tray in the absorption tower. The effects of operating conditions on the permeate flux and acid retention were studied with two commercial RO membranes (SWC5 and SWC6). When the operating pressure was 4 MPa and the temperature was 25 °C, the permeate fluxes of two membranes were about 20 L·m−2·h−1. The acrylic acid and acetic acid retentions were about 80% and 78%, respectively. After being immersed in the acid solutions for several months, the characteristics of the two membranes were tested to evaluate their acid resistance. After six months of exposure to the acid solution containing 2.5% acrylic acid and 2.5% acetic acid, the retentions of acrylic acid and acetic acid were decreased by 5.7% and 4.1% for SWC5 and 4.9% and 2.2% for SWC6, respectively. The changes of membrane surface morphology and chemical composition showed the hydrolysis of some amide bonds. Full article
(This article belongs to the Section Membrane Processing and Engineering)
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15 pages, 3470 KB  
Article
Laser-Induced Microgrooves Improve the Mechanical Responses of Cemented Implant Systems
by Morshed Khandaker, Abdellah Ait Moussa, Desmond Nuyebga Sama, Fereshteh Safavinia, Susmita Hazra, Onur Can Kalay, Fatih Karpat, Erik Clary and Amgad Haleem
Micromachines 2020, 11(5), 466; https://doi.org/10.3390/mi11050466 - 29 Apr 2020
Cited by 4 | Viewed by 3252
Abstract
The impact of a laser-induced microgroove (LIM) architecture on mechanical responses of two cemented implant systems was evaluated. One system consisted of two aluminum alloy rods bonded end-to-end by polymethylmethacrylate cement. The second system consisted of a custom-made, aluminum tibial tray (TT) cemented [...] Read more.
The impact of a laser-induced microgroove (LIM) architecture on mechanical responses of two cemented implant systems was evaluated. One system consisted of two aluminum alloy rods bonded end-to-end by polymethylmethacrylate cement. The second system consisted of a custom-made, aluminum tibial tray (TT) cemented in an artificial canine tibia. Control specimens for each system were polished smooth at the cement interface. For LIM samples in the rod system, microgrooves were engraved (100 µm depth, 200 µm width, 500 µm spacing) on the apposing surface of one of the two rods. For TT system testing, LIM engraving (100 µm spacing) was confined to the underside and keel of the tray. Morphological analysis of processed implant surfaces revealed success in laser microgrooving procedures. For cemented rods tested under static tension, load to failure was greater for LIM samples (279.0 ± 14.9 N vs. 126.5 ± 4.5 N). Neither non-grooved nor grooved TT samples failed under cyclic compression testing (100,000 cycles at 1 Hz). Compared with control specimens, LIM TT constructs exhibited higher load to failure under static compression and higher strain at the bone interface under cyclic compression. Laser-induced microgrooving has the potential to improve the performance of cemented orthopedic implants. Full article
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17 pages, 5668 KB  
Article
Compatibility of a Silicone Impression/Adhesive System to FDM-Printed Tray Materials—A Laboratory Peel-off Study
by Yichen Xu, Alexey Unkovskiy, Felix Klaue, Frank Rupp, Juergen Geis-Gerstorfer and Sebastian Spintzyk
Materials 2018, 11(10), 1905; https://doi.org/10.3390/ma11101905 - 7 Oct 2018
Cited by 24 | Viewed by 5033
Abstract
Computer-aided design (CAD) and additive manufacturing (AM) have shown promise in facilitating the fabrication of custom trays. Due to the clinical requirements, custom tray materials should achieve good bonding to the impression/adhesive systems. This study evaluated the retention of three fused deposition modeling [...] Read more.
Computer-aided design (CAD) and additive manufacturing (AM) have shown promise in facilitating the fabrication of custom trays. Due to the clinical requirements, custom tray materials should achieve good bonding to the impression/adhesive systems. This study evaluated the retention of three fused deposition modeling (FDM) custom tray materials to a silicone impression/adhesive system before and after gritblasting (GB) by peel-off test. CAD-designed experimental test blocks were printed by FDM using acrylonitrile butadiene styrene (ABS), polyethylene terephthalate glycol copolyester (PETG), and high impact polystyrene (HIPS), and the reference test blocks were made of a conventional light-curing resin (n = 11). Before and after GB, the surface topography of all tray materials was analysed, and the maximum strength of the test block peeled off from a silicone impression/adhesive system was measured. After GB, the arithmetic mean height (Sa) and the valley fluid retention index (Svi) of the four material groups declined (p < 0.05). The peel-off strength of each of the four material groups significantly decreased by GB (p < 0.05), but no statistical difference could be found among them before or after GB. In all peel-off tests, adhesive failure occurred at the adhesive-impression material interface. The results indicated ABS, HIPS, and PETG could provide sufficient adhesion to the adhesive as the conventional light-curing resin, and GB could reduce the roughness generated by FDM and weaken the bonding between the adhesive and the silicone impression. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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