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15 pages, 4075 KB  
Review
Potential of Hairless Canary Seed as a Food-Based Remedy for Celiac Disease and Diabetes
by El-Sayed M. Abdel-Aal and Tamer H. Gamel
Foods 2025, 14(17), 3011; https://doi.org/10.3390/foods14173011 - 28 Aug 2025
Abstract
Hairless canary seed (Phalaris canariensis L.) can play significant roles in human health and nutrition due to its unique nutrient profile. It belongs to the Gramineae family similar to common cereal grains like wheat, rice and corn. On the other hand, the [...] Read more.
Hairless canary seed (Phalaris canariensis L.) can play significant roles in human health and nutrition due to its unique nutrient profile. It belongs to the Gramineae family similar to common cereal grains like wheat, rice and corn. On the other hand, the traditional canary seed is characterized by the presence of silicified spicules or hairs on the hulls of the kernel that could pose health hazards to humans. The hairless canary seed was developed in Canada by a conventional breeding program to mitigate the health concerns associated with the silicified hairs. The hairless grain is silica free, i.e., totally glabrous, and is granted regulatory food approvals by Health Canada and US-FDA. The hairless grain holds a great potential as a whole grain functional food ingredient due to its unique nutritional and functional attributes. As a cereal grain, it is rich in protein that is non-gluten and exceptionally high in tryptophan and bioactive peptides. The grain also contains reasonable amounts of carotenoids, polyphenols, and healthy unsaturated oil. Because of these special characteristics, it is considered a promising nutritious and therapeutic food. This review provides insights into the potential of hairless canary seed as a functional ingredient in products designed to mitigate oxidative stress, diabetes and celiac disease and/or to improve vision and cognition. Full article
(This article belongs to the Section Nutraceuticals, Functional Foods, and Novel Foods)
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18 pages, 3415 KB  
Article
Study on the Modification of Dietary Fiber and Degradation of Zearalenone in Corn Germ Meal by Solid-State Fermentation with Bacillus subtilis K6
by Jiahao Li, Kailong Li, Langwen Tang, Chun Hua, Na Chen, Chenxian Yang, Ying Xin and Fusheng Chen
Foods 2025, 14(15), 2680; https://doi.org/10.3390/foods14152680 - 30 Jul 2025
Viewed by 484
Abstract
Although corn germ meal is a rich source of dietary fiber, it contains a relatively low proportion of soluble dietary fiber (SDF) and is frequently contaminated with high levels of zearalenone (ZEN). Solid-state fermentation has the dual effects of modifying dietary fiber (DF) [...] Read more.
Although corn germ meal is a rich source of dietary fiber, it contains a relatively low proportion of soluble dietary fiber (SDF) and is frequently contaminated with high levels of zearalenone (ZEN). Solid-state fermentation has the dual effects of modifying dietary fiber (DF) and degrading mycotoxins. This study optimized the solid-state fermentation process of corn germ meal using Bacillus subtilis K6 through response surface methodology (RSM) to enhance SDF yield while efficiently degrading ZEN. Results indicated that fermentation solid-to-liquid ratio and time had greater impacts on SDF yield and ZEN degradation rate than fermentation temperature. The optimal conditions were determined as temperature 36.5 °C, time 65 h, and solid-to-liquid ratio 1:0.82 (w/v). Under these conditions, the ZEN degradation rate reached 96.27 ± 0.53%, while the SDF yield increased from 9.47 ± 0.68% to 20.11 ± 1.87% (optimizing the SDF/DF ratio from 1:7 to 1:3). Scanning electron microscopy (SEM) and confocal laser scanning microscope (CLSM) revealed the structural transformation of dietary fiber from smooth to loose and porous forms. This structural modification resulted in a significant improvement in the physicochemical properties of dietary fiber, with water-holding capacity (WHC), oil-holding capacity (OHC), and water-swelling capacity (WSC) increasing by 34.8%, 16.4%, and 15.2%, respectively. Additionally, the protein and total phenolic contents increased by 23.0% and 82.61%, respectively. This research has achieved efficient detoxification and dietary fiber modification of corn germ meal, significantly enhancing the resource utilization rate of corn by-products and providing technical and theoretical support for industrial production applications. Full article
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25 pages, 3317 KB  
Article
Biosurfactant Produced by Bacillus subtilis UCP 1533 Isolated from the Brazilian Semiarid Region: Characterization and Antimicrobial Potential
by Antônio P. da C. Albuquerque, Hozana de S. Ferreira, Yali A. da Silva, Renata R. da Silva, Carlos V. A. de Lima, Leonie A. Sarubbo and Juliana M. Luna
Microorganisms 2025, 13(7), 1548; https://doi.org/10.3390/microorganisms13071548 - 1 Jul 2025
Viewed by 593
Abstract
The increasing resistance of pathogenic microorganisms to antimicrobials has driven the search for safe and sustainable alternatives. In this context, microbial biosurfactants have gained prominence due to their antimicrobial activity, low toxicity, and high stability under extreme conditions. This study presents the production [...] Read more.
The increasing resistance of pathogenic microorganisms to antimicrobials has driven the search for safe and sustainable alternatives. In this context, microbial biosurfactants have gained prominence due to their antimicrobial activity, low toxicity, and high stability under extreme conditions. This study presents the production and characterization of a biosurfactant with antimicrobial potential, obtained from Bacillus subtilis isolated from soil, for application in the control of resistant strains. Bacterial identification was performed using mass spectrometry (MALDI-TOF), confirming it as Bacillus subtilis. The strain B. subtilis UCP 1533 was cultivated using different carbon sources (glucose, soybean oil, residual frying oil, and molasses) and nitrogen sources (ammonium chloride, sodium nitrate, urea, and peptone), with evaluations at 72, 96, and 120 h. The best condition involved a mineral medium supplemented with 2% soybean oil and 0.12% corn steep liquor, resulting in the production of 16 g·L−1 of biosurfactant, with a critical micelle concentration (CMC) of 0.3 g·L−1 and a reduction in water surface tension to 25 mN·m−1. The biosurfactant showed an emulsification index of 100% for used motor oil and ranged from 50% to 100% for different vegetable oils, maintaining stability across a wide range of pH, salinity, and temperature. FT-IR and NMR analyses confirmed its lipopeptide nature and anionic charge. Toxicity tests with Tenebrio molitor larvae showed 100% survival at all the tested concentrations. In phytotoxicity assays, seed germination rates above 90% were recorded for Solanum lycopersicum and Lactuca sativa. Antimicrobial tests revealed inhibitory activity against resistant strains of Escherichia coli and Pseudomonas aeruginosa, as well as against species of the genus Candida (C. glabrata, C. lipolytica, C. bombicola, and C. guilliermondii), highlighting the biosurfactant as a promising alternative in combating antimicrobial resistance (AMR). These results indicate the potential application of this biosurfactant in the development of antimicrobial agents for pharmaceutical formulations and sustainable strategies for phytopathogen control in agriculture. Full article
(This article belongs to the Section Antimicrobial Agents and Resistance)
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17 pages, 7582 KB  
Article
Effects of Feeding Calcium Salts from a Mixture of Linseed and Fish Oil on Productive Response, Metabolic Status, and Reproductive Parameters in Early-Lactation Dairy Cows
by Pablo M. Roskopf, Alejandra Cuatrin, Matías Stangaferro, Gino Storani, Emmanuel Angeli, Gustavo J. Hein and Eloy E. Salado
Dairy 2025, 6(4), 34; https://doi.org/10.3390/dairy6040034 - 1 Jul 2025
Viewed by 656
Abstract
This study evaluated the effects of supplementing early-lactation Holstein cows with rumen-protected omega-3 fatty acids (calcium salts) on productive and reproductive performance. Thirty-six multiparous cows were randomly assigned to one of two treatments from 21 ± 2 days before calving to 105 ± [...] Read more.
This study evaluated the effects of supplementing early-lactation Holstein cows with rumen-protected omega-3 fatty acids (calcium salts) on productive and reproductive performance. Thirty-six multiparous cows were randomly assigned to one of two treatments from 21 ± 2 days before calving to 105 ± 5 days in milk (DIM): a Control group (C) or an Omega-3-supplemented group (O-3), receiving a blend of linseed and fish oil (60:40). Both groups were fed isoenergetic diets, with ground corn as the control supplement. Total dry matter and net energy intake did not differ between treatments. A treatment-by-time interaction was observed for milk yield, with cows in the O-3 group producing more milk than controls at specific time points. Additionally, O-3 cows had higher overall protein yield and improved feed efficiency. No differences were found in body weight, BCS, glucose, insulin, IGF-1, or urea concentrations, but a tendency toward higher plasma NEFA and BHBA concentrations and lower energy balance was observed in the O-3 group. Supplementation increased plasma cholesterol and progesterone concentrations and was associated with a higher proportion of cows being pregnant at 130 DIM. These findings suggest that omega-3 supplementation may improve specific aspects of lactational performance and reproductive efficiency without compromising metabolic status. Full article
(This article belongs to the Section Dairy Animal Nutrition and Welfare)
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12 pages, 2285 KB  
Article
Interfacial Engineering-Free Microfluidics: Toward a Mild and Cost-Effective Strategy for Surfactant- and Demulsifier-Free Hydrogel Microsphere Fabrication
by Qing Qin, Yu Zhang, Yubei Wei, Jinnuo Lv, Meiling Tian, Yuanyuan Sun, Wei Fang, Xingjian Huang, Jianglin Li, Yifeng Su, Xiaoliang Xiang, Xing Hu and Zhizhi Zhou
Micromachines 2025, 16(7), 733; https://doi.org/10.3390/mi16070733 - 22 Jun 2025
Viewed by 1040
Abstract
This study proposes a simple yet versatile microfluidic strategy for fabricating monodisperse alginate hydrogel microspheres using a symmetric flow-focusing device. The system integrates three key innovations: (1) Cost-effective mold fabrication: A paper-based positive master replaces conventional SU-8 photoresist, significantly simplifying device prototyping. (2) [...] Read more.
This study proposes a simple yet versatile microfluidic strategy for fabricating monodisperse alginate hydrogel microspheres using a symmetric flow-focusing device. The system integrates three key innovations: (1) Cost-effective mold fabrication: A paper-based positive master replaces conventional SU-8 photoresist, significantly simplifying device prototyping. (2) Surfactant-free droplet generation: Alginate hydrogel droplets are formed at the first flow-focusing junction without requiring interfacial stabilizers. (3) In situ solidification with coalescence suppression: Acetic acid-infused corn oil is introduced at the adjacent junction, simultaneously triggering ionic crosslinking of alginate via pH reduction while preventing droplet aggregation. Notably, the hydrogel microspheres can be efficiently harvested through oscillatory aqueous phase separation, removing post-fabrication washing steps (typically 6–8 cycles for surfactant and oil removal). This integrated approach demonstrates exceptional advantages in fabrication simplicity, process scalability, and operational robustness for high-throughput hydrogel microsphere production. Full article
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17 pages, 312 KB  
Article
Meat Quality and Fatty Acid Profile of Rams Fed Diets Enriched with Vegetable Oils of Varying Unsaturation Levels
by Evyla Layssa Gonçalves Andrade, Kevily Henrique de Oliveira Soares de Lucena, José Morais Pereira Filho, Marcia Makaline Rodrigues Pereira, Ronaldo Lopes Oliveira, Analívia Martins Barbosa, Elzania Sales Pereira, Claudio Vaz Di Mambro, Marcos Jacome de Araújo and Leilson Rocha Bezerra
Foods 2025, 14(13), 2179; https://doi.org/10.3390/foods14132179 - 22 Jun 2025
Viewed by 508
Abstract
Antioxidant feed additives, such as cashew nutshell liquid (CNSL), rich in phenolic compounds, have gained attention for improving animal production and meat quality. The study evaluated the dietary effects of blending CNSL (0.5%) with different vegetable oils (1.5%) varying in unsaturated fatty acid [...] Read more.
Antioxidant feed additives, such as cashew nutshell liquid (CNSL), rich in phenolic compounds, have gained attention for improving animal production and meat quality. The study evaluated the dietary effects of blending CNSL (0.5%) with different vegetable oils (1.5%) varying in unsaturated fatty acid (UFA) profiles on the meat quality and fatty acid composition of muttons. Forty Santa Inês × Dorper crossbred rams (24.44 ± 1.5 kg) were allocated to five treatments for 70 days: CNSL combined with canola (MUFA-rich) compared to corn, soybean, sunflower, or cottonseed oils (PUFA-rich). The CNSL + canola blend improved meat quality, showing higher water-holding capacity and tenderness and lower cooking loss than CNSL + PUFA-rich oils (p < 0.05). Meat yellowness (b*) increased with CNSL + soybean or cottonseed blend. Meat proximate composition was unaffected (p > 0.05). Minor variations in specific fatty acids were observed, including higher C14:0 and C16:1 in canola and cottonseed + CNSL blend groups and greater EPA (C20:5 n–3) with soybean oil + CNSL blend (p < 0.05). The ∑n–6:∑n–3 ratio was highest with cottonseed and lowest with soybean oil (p < 0.05). Overall, combining CNSL with MUFA-rich oils, particularly canola, compared to PUFA oils, enhances meat quality while supporting the sustainable use of CNSL in ram diets. Full article
(This article belongs to the Section Meat)
21 pages, 3123 KB  
Article
The Impact of Starches from Various Botanical Origins on the Functional and Mechanical Properties of Anhydrous Lotion Body Bars
by Agnieszka Kulawik-Pióro, Beata Fryźlewicz-Kozak, Iwona Tworzydło, Joanna Kruk and Anna Ptaszek
Polymers 2025, 17(13), 1731; https://doi.org/10.3390/polym17131731 - 21 Jun 2025
Viewed by 627
Abstract
Starch, as a natural, low-cost, and vegan-friendly raw material, aligns well with the growing demand for sustainable, zero-waste, and waterless cosmetic products. Its biodegradability and natural origin allow for minimal environmental impact during production and disposal. Anhydrous lotion body bars, solid and water-free [...] Read more.
Starch, as a natural, low-cost, and vegan-friendly raw material, aligns well with the growing demand for sustainable, zero-waste, and waterless cosmetic products. Its biodegradability and natural origin allow for minimal environmental impact during production and disposal. Anhydrous lotion body bars, solid and water-free alternatives to traditional moisturizers, offer high concentrations of active ingredients that are more effective and have a longer shelf life. Their solid form enables packaging in paper-based containers, reducing plastic waste. To address formulation challenges such as excessive greasiness, poor absorption, or lack of structural stability, which are often associated with the high oil content of anhydrous body lotion bars, starch may serve as a promising natural additive. The aim of this study was to optimize the formulation of an innovative starch-based anhydrous lotion bar. For this purpose, physicochemical analyses of starches from various botanical sources (corn, rice, tapioca, waxy corn and potato) were performed, along with evaluations of the functional (including commercially acceptable form, hardness sufficient for application, product stability, reduced greasiness and stickiness) and mechanical properties of the resulting bars. Additionally, the rheological behavior was described using the De Kee model. The results indicate that a 2.5% starch addition, regardless of its botanical origin, provides the best balance between viscosity and ease of application. Moreover, starches with a low moisture content and high oil absorption capacity effectively reduce the greasy skin sensation. These findings demonstrate the potential of starch as a natural multifunctional additive in the development of stable, user-friendly anhydrous lotion body bars. Full article
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27 pages, 4462 KB  
Article
Highland Barley Tartary Buckwheat Coarse Grain Biscuits Ameliorated High-Fat Diet-Induced Hyperlipidaemia in Mice Through Gut Microbiota Modulation and Enhanced Short-Chain Fatty Acid Secretion Mice
by Xiuqing Yang, Xiongfei Kang, Linfang Li and Shaoyu Zhang
Foods 2025, 14(12), 2079; https://doi.org/10.3390/foods14122079 - 12 Jun 2025
Viewed by 1398
Abstract
Dietary modification plays a crucial role in managing and preventing hyperlipidemia. This study examined the combination of highland barley, tartary buckwheat, mung beans, Ormosia hosiei, black rice, and corn germ oil in multi-grain biscuit form. This formulation leverages the synergistic interactions among bioactive [...] Read more.
Dietary modification plays a crucial role in managing and preventing hyperlipidemia. This study examined the combination of highland barley, tartary buckwheat, mung beans, Ormosia hosiei, black rice, and corn germ oil in multi-grain biscuit form. This formulation leverages the synergistic interactions among bioactive compounds, which exert preventive and therapeutic effects against lipid disorders. C57BL/6N mice were fed a high-fat diet for 12 weeks to establish a hyperlipidemia model, followed by feeding with highland barley tartary buckwheat coarse-grain biscuits for 4 weeks. The experimental outcomes revealed that the highland barley tartary buckwheat coarse-grain biscuits effectively controlled body weight and reduced fasting blood sugar levels: body weight was restored to approximately 29 g, and the fasting blood sugar level returned to the normal range of 6 mmol/L. We also observed improved organ indices and regulated blood lipids in hyperlipidemic mice. The total cholesterol of high-fat mice was reduced to 5 mmol/L and the triglyceride level to 1 mmol/L. A significant reduction in inflammatory markers and histopathological improvement in hepatic and adipose tissues were also observed. The intervention enhanced leptin and adiponectin secretion while elevating concentrations of acetic, propionic, butyric, valeric, and caproic acids. Microbiome analysis demonstrated favorable shifts in bacterial populations, characterized by increased Bacteroidetes and Verrucomicrobia abundance and a decreased Firmicutes-to-Proteobacteria ratio, promoting beneficial genera while suppressing potentially pathogenic taxa. These findings suggest that the developed highland barley tartary buckwheat coarse-grain biscuits are a promising dietary intervention for hyperlipidemia management. The effects were potentially mediated through gut microbiota modulation and enhanced short-chain fatty acid production. This research provides novel insights into functional food development for hyperlipidemia. Full article
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20 pages, 1227 KB  
Article
A Mixture of Free and Microencapsulated Essential Oils Combined with Turmeric and Tannin in the Diet of Dairy Cows: Effects on Productive Efficiency and Animal Health
by Emeline Pizzolatto de Mello, Miklos Maximiliano Bajay, Tainara Leticia dos Santos, Renato Santos de Jesus, Guilherme Luiz Deolindo, Luisa Nora, Mario Augusto Tortelli, Gilnei Bruno da Silva, Daiane Manica, Margarete Dulce Bagatini, Francisco Machado and Aleksandro S. da Silva
Animals 2025, 15(11), 1588; https://doi.org/10.3390/ani15111588 - 29 May 2025
Viewed by 532
Abstract
This study aimed to evaluate whether the addition of a phytobiotic additive formulated based on cinnamon and oregano essential oils (50% free and 50% microencapsulated) combined with turmeric extract and tannins to the diet of cows has beneficial effects on health, productivity, and [...] Read more.
This study aimed to evaluate whether the addition of a phytobiotic additive formulated based on cinnamon and oregano essential oils (50% free and 50% microencapsulated) combined with turmeric extract and tannins to the diet of cows has beneficial effects on health, productivity, and milk quality. In a completely randomized design, eighteen Jersey cows were used in a compost barn system over 45 days. The cows were divided into two homogeneous groups: one control (without additive; n = 9) and another treatment (with a phytobiotic at a dose of 2 g/cow/day; n = 9). The diet was formulated based on corn silage, hay and concentrate for daily 30 L/cow production. Blood and milk samples were collected at 15-day intervals. There was a treatment × day interaction: cows that consumed the phytobiotic additive produced a more significant amount of milk at days 14, 17, 18, 30, 39 and 45 (p ≤ 0.05). When we corrected milk production for fat percentage, we observed higher milk production in the cows that consumed phytobiotics compared to the control during the experimental period (p = 0.01). The feed intake of cows fed phytobiotics was lower (p = 0.01). Thus, feed efficiency was better in cows that consumed phytogenics. There was a higher percentage of fat in the milk of cows that consumed phytobiotics and a higher amount of polyunsaturated fatty acids compared to the control (p = 0.02). There was an increase in total protein and globulin levels (p = 0.01), which may be associated with the interaction of the antimicrobial, antioxidant, and immunomodulatory properties of the phytobiotic additive. An increase in immunoglobulins (p = 0.01) and a reduction in acute-phase proteins (p ≤ 0.05) were observed in the blood of cows in the phytobiotic group. Lower levels of TNF-α, IL-1β and IL-6 and higher levels of IL-10 in the serum of cows that consumed the phytoactive (p = 0.01) reaffirm the anti-inflammatory effect of the additive. Lower levels of lipid peroxidation (TBARS) and reactive oxygen species (ROS) were observed in the serum of cows in the phytobiotic group. Greater catalase and superoxide dismutase activity was observed in cows that consumed the phytogenic (p < 0.01). Therefore, it can be concluded that the additive in question has antioxidant, immunological, and anti-inflammatory actions and has the potential to improve productive performance when corrected for milk fat. Full article
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14 pages, 258 KB  
Article
Nanoemulsified Corn Oil in Lactating Barki Nutrition: Effect on Intake, Nutrient Digestibility, Rumen Fermentation Characteristics, and Microbial Population
by Min Gao, Rong-Qing Li, Mostafa S. A. Khattab, Ahmed M. Abd El Tawab, Yong-Bin Liu and Mohamed El-Sherbiny
Animals 2025, 15(10), 1424; https://doi.org/10.3390/ani15101424 - 14 May 2025
Viewed by 456
Abstract
Nanoemulsified corn oil was tested on twenty-one multiparous lactating Barki ewes (mean ± SD: 3 ± 0.4 parity, 44.3 ± 1.9 kg body weight, 30 ± 2.7 months of age, and 402 ± 23 g/d of prior milk production) randomly allocated to the [...] Read more.
Nanoemulsified corn oil was tested on twenty-one multiparous lactating Barki ewes (mean ± SD: 3 ± 0.4 parity, 44.3 ± 1.9 kg body weight, 30 ± 2.7 months of age, and 402 ± 23 g/d of prior milk production) randomly allocated to the following treatments (n = 7 ewes/group): Control—a basal diet consisting of 50% concentrate mixtures and 50% berseem clover; CO—the Control diet + 3% of corn oil; NCO—the Control diet + 3% of nanoemulsified corn oil. A completely randomized design of 25 days of adaptation and 5 days of sampling was employed with seven ewes per treatment. Despite feeding oil according to the recommended values, CO decreased the dry matter intake by 8.3% and 6.7% compared to the Control and NCO, respectively. The negative impact of CO extended to reducing the concentrations of ammonia and total volatile fatty acids in the rumen. On the other hand, NCO had less effect on the biohydrogenation intermediates profile compared to CO; noticeably, higher proportions of unsaturated fatty acid (UFA) were associated with NCO; these results were also supported by an increase in the rumen microbial population with NCO compared to CO, especially the biohydrogenation bacteria, which showed higher abundance with NCO despite the low presence of biohydrogenation intermediates. In conclusion, the NCO demonstrated the ability to decrease the transformation of unsaturated fatty acids into saturated fatty acids in the biohydrogenation environment. This effect was not associated with decreased dry matter intake, changes in nutrient digestibility, or alterations in fermentation patterns. Full article
(This article belongs to the Special Issue Nutrients and Feed Additives in Ruminants)
21 pages, 4054 KB  
Article
Comparison of the Nutritional, Physicochemical, Technological–Functional, and Structural Properties and Antioxidant Compounds of Corn Kernel Flours from Native Mexican Maize Cultivated in Jalisco Highlands
by Luis Alfonso Hernández-Villaseñor, Salvador Hernández-Estrada, Víctor Manuel Gómez-Rodríguez, Humberto Ramírez-Vega, Zuamí Villagrán, Araceli Ortega-Martínez, Efigenia Montalvo-González, José Martín Ruvalcaba-Gómez, Napoleón González-Silva and Luis Miguel Anaya-Esparza
Crops 2025, 5(3), 26; https://doi.org/10.3390/crops5030026 - 3 May 2025
Viewed by 937
Abstract
Maize plays a crucial role in global nutrition and food security, with Mexico making a significant contribution through its diverse native corn genotypes. However, research on flours derived from these native maize genotypes remains limited, hindering their potential applications in food manufacturing. This [...] Read more.
Maize plays a crucial role in global nutrition and food security, with Mexico making a significant contribution through its diverse native corn genotypes. However, research on flours derived from these native maize genotypes remains limited, hindering their potential applications in food manufacturing. This study aimed to determine the nutritional, physicochemical, techno-functional, structural, and antioxidant properties of corn kernel flours from nine native Mexican maize accessions cultivated in the highlands of Jalisco. Enough cobs for each maize accession were randomly selected to yield 1000 g of corn kernels. Data analysis was conducted by analysis of variance and Kruskal–Wallis tests (α = 0.05). Moreover, Principal Component Analysis (PCA) and Hierarchical Cluster Analysis (HCA) were performed. Native corn kernel flour (NCKF) demonstrated higher protein and fat content compared to white hybrid corn flour (WHF). While both flours showed similar pH, titratable acidity, and water activity levels, NCKF exhibited higher total soluble solids. Additionally, NCKF showed superior techno-functional properties, including water solubility, water absorption index, swelling power, emulsifying capacity, and foaming capacity, while its oil absorption index was comparable to that of WHF. Moreover, NCKF contained higher levels of bioactive compounds, such as soluble phenols, condensed tannins, flavonoids, anthocyanins, and carotenoids, along with enhanced antioxidant properties, as measured by FRAP, DPPH, and ABTS assays. FTIR analysis revealed that all NCKF samples exhibited patterns similar to those of WHF with differences in transmittance intensities. Notably, spectral differences were identified by PCA, while HCA demonstrated that corn flours exhibited similitudes and differences among them, which can be categorized into four groups based on their nutritional, physicochemical, and technological–functional properties, as well as antioxidant compound contents. Overall, the evaluated corn flours displayed nutritional, physicochemical, techno-functional, and antioxidant properties for the potential development of functional or nutraceutical food and beverage products. Full article
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11 pages, 932 KB  
Article
Piper aduncum Essential Oil: Toxicity to Sitophilus zeamais and Effects on the Quality of Corn Grains
by Weverton Peroni Santos, Lucas Martins Lopes, Gutierres Nelson Silva, Marcela Silva Carvalho and Adalberto Hipólito de Sousa
Processes 2025, 13(5), 1363; https://doi.org/10.3390/pr13051363 - 29 Apr 2025
Viewed by 448
Abstract
Stored product pests are controlled primarily through applying pyrethroid and organophosphate insecticides or through fumigation with phosphine (PH3). However, several populations of weevils are resistant to these insecticides. Essential oils appear to be safe alternatives for both humans and the environment. [...] Read more.
Stored product pests are controlled primarily through applying pyrethroid and organophosphate insecticides or through fumigation with phosphine (PH3). However, several populations of weevils are resistant to these insecticides. Essential oils appear to be safe alternatives for both humans and the environment. The objective was to investigate the toxicity of Piper aduncum essential oil (PAEO) to Sitophilus zeamais and evaluate its effects on corn grain quality during the four-month storage period. This study was conducted in two stages. In the first stage, the toxicity of PAEO at concentrations lethal to 50 and 95% of insects (LC50 and LC95) was estimated. The second step evaluated the degree of infestation, water content, apparent specific mass, loss of mass, electrical conductivity, and percentage of germination of grains at 0, 30, 60, 90, and 120 days after exposure to PAEO, deltamethrin (pyrethroid), and the control treatment. PAEO presents toxicity to S. zeamais. The LC50 and LC95 values are 298.50 µL kg−1 and 585.20 µL kg−1, respectively. The increases in infestation degree, water content, electric conductivity, and mass loss, as well as reductions in apparent specific mass and germination, show the loss of corn quality during the 120-day storage period, being more significant when no product is applied. PAEO delays the loss of quality of the grains, presenting a greater capacity to preserve the grains for a longer period. Full article
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17 pages, 1106 KB  
Article
Dietary Passion Fruit Seed Oil Supplementation for Health and Performance of Laying Hens
by Laís Garcia Cordeiro, Paola Aparecida Damázio Rodrigues, Gabrieli Andressa de Lima, Elis Omar Figueroa Castillo, Joyce Andrade da Silva, Júlia de Lima Lopes, Anna Luísa Lang, Samir Moura Kadri, Antônio Celso Pezzato and José Roberto Sartori
Agriculture 2025, 15(8), 864; https://doi.org/10.3390/agriculture15080864 - 16 Apr 2025
Viewed by 885
Abstract
Passion fruit seed oil (PFSO) is rich in bioactive compounds, which can enhance laying hens’ health and performance. The current study was conducted to investigate the effect of increasing PFSO supplementation in laying hens’ productive performance, egg quality, relative weight and length of [...] Read more.
Passion fruit seed oil (PFSO) is rich in bioactive compounds, which can enhance laying hens’ health and performance. The current study was conducted to investigate the effect of increasing PFSO supplementation in laying hens’ productive performance, egg quality, relative weight and length of organs, plasma lipid oxidation, antioxidant status, and gene expression of SOD, GPx, CAT, and NRF2 in the liver. One hundred ninety-two 25-week-old Lohmann Whites were randomly divided into three treatments (n = 8 replicates/diet, 8 hens/replicate). The groups were fed a corn–soybean basal diet containing 0.00%, 0.45%, and 0.90% PFSO for 16 weeks. The results indicated that increasing supplementation of PFSO decreased plasma lipid oxidation (n = 8; linear, p = 0.012) and increased CAT gene expression (n = 8; linear, p = 0.001). SOD and NRF2 genes tended to increase linearly, and GPx was not affected (n = 4; p > 0.05). The CAT activity tended to decrease linearly and the SOD and GPx were not affected (n = 8; p > 0.05) by diets. Performance and most egg quality, relative weight, and length of organs did not differ among treatments (n = 8; p > 0.05). Therefore, increasing the supplementation of PFSO in the diet may have positive effects on the laying hens’ health by decreasing oxidative stress, stimulating the antioxidant defense system, and sustaining egg production and quality. Full article
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21 pages, 4221 KB  
Article
Study of the Impact of Operating Parameters and the Addition of Fat on the Physicochemical and Texture Properties of Extruded Snacks
by Nicolas Jacquet, Armande Plompteux, Yves Brostaux, Paul Malumba, Sabine Danthine and Christophe Blecker
Foods 2025, 14(8), 1307; https://doi.org/10.3390/foods14081307 - 9 Apr 2025
Viewed by 1105
Abstract
This study investigated the effects of extrusion parameters (barrel temperature, screw speed) and oil content on the physicochemical and textural properties of corn flour-based snacks, using a Box–Behnken response surface design. Significant predictive models (adjusted R2 > 90%) were established for specific [...] Read more.
This study investigated the effects of extrusion parameters (barrel temperature, screw speed) and oil content on the physicochemical and textural properties of corn flour-based snacks, using a Box–Behnken response surface design. Significant predictive models (adjusted R2 > 90%) were established for specific mechanical energy (SME), expansion ratio, bulk density, hardness, compression work, water activity (aw) and dry matter content. The results showed that increasing oil content dramatically reduced SME (from 229.5 Wh/kg at 5% oil and 110 °C to 68.2 Wh/kg at 10% oil and 180 °C) and expansion ratio (maximum 3.73 at 145 °C, 150 rpm, 0% oil), while increasing bulk density (up to 0.271 g/cm3 at 10% oil). High oil content also led to a sharp increase in hardness (from 67.9 N at 0% oil to 466.9 N at 10% oil). Conversely, higher barrel temperature (up to 180 °C) and screw speed (up to 250 rpm) generally improved snack texture by reducing hardness and density and increasing expansion. Water activity ranged from 0.24 to 0.50 and was positively influenced by oil content and negatively by temperature and screw speed. Overall, oil content had the strongest detrimental impact on snack properties, but optimizing temperature and screw speed allowed the production of snacks with acceptable qualities. Full article
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32 pages, 3424 KB  
Article
Volatility Modeling of the Impact of Geopolitical Risk on Commodity Markets
by Letife Özdemir, Necmiye Serap Vurur, Ercan Ozen, Beata Świecka and Simon Grima
Economies 2025, 13(4), 88; https://doi.org/10.3390/economies13040088 - 26 Mar 2025
Cited by 4 | Viewed by 3545
Abstract
This study analyses the impact of the Geopolitical Risk Index (GPR) on the volatility of commodity futures returns from 4 January 2010 to 30 June 2023, using Exponential Generalized Autoregressive Conditional Heteroskedasticity (EGARCH) models. It expands the research scope to include precious metals, [...] Read more.
This study analyses the impact of the Geopolitical Risk Index (GPR) on the volatility of commodity futures returns from 4 January 2010 to 30 June 2023, using Exponential Generalized Autoregressive Conditional Heteroskedasticity (EGARCH) models. It expands the research scope to include precious metals, agricultural products, energy, and industrial metals. The study differentiates between the impacts of geopolitical threat events and actions using GPRACT and GPRTHREAT indicators. Findings reveal that negative geopolitical shocks increase commodity returns’ volatility more than positive shocks. Specifically, gold, silver, and natural gas are negatively affected, while wheat, corn, soybeans, cotton, zinc, nickel, lead, WTI oil, and Brent oil experience positive effects. Platinum, cocoa, coffee, and copper show no significant impact. These insights highlight the importance of geopolitical risks on commodity market volatility and returns, aiding in risk management and portfolio diversification. Policymakers, financial market stakeholders, and investors can leverage these findings to better understand the GPR’s relationship with commodity markets and develop effective strategies. Full article
(This article belongs to the Special Issue Financial Market Volatility under Uncertainty)
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