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Search Results (756)

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Keywords = drilling temperatures

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19 pages, 6638 KB  
Article
High-Temperature Degradation of Throttling Performance in While-Drilling Jars Induced by Thermal Expansion and Fluid Rheology
by Zhaoyang Zhao, Zhanghua Lian, Hao Yu, Wei Sun, Senyan Liu, Zhiyong Wan and Jiachang Nie
Machines 2025, 13(9), 824; https://doi.org/10.3390/machines13090824 (registering DOI) - 7 Sep 2025
Abstract
During deep and ultra-deep well drilling operations, the throttling performance of the hydraulic-while-drilling jar is significantly affected by the combined influence of temperature-induced differential thermal expansion among components and changes in the rheological properties of hydraulic oil. These effects often lead to unstable [...] Read more.
During deep and ultra-deep well drilling operations, the throttling performance of the hydraulic-while-drilling jar is significantly affected by the combined influence of temperature-induced differential thermal expansion among components and changes in the rheological properties of hydraulic oil. These effects often lead to unstable jarring behavior or even complete failure to trigger jarring during stuck pipe events. Here, we propose a high-temperature degradation evaluation model for the throttling performance of the throttle valve in an HWD jar based on thermal expansion testing of individual components and high-temperature rheological experiments of hydraulic oil. By using the variation characteristics of the throttling passage geometry as a linkage, this model integrates the thermo-mechanical coupling of the valve body with flow field simulation. Numerical results reveal that fluid pressure decreases progressively along the flow path through the throttle valve, while flow velocity increases sharply at the channel entrance and exhibits mild fluctuations within the throttling region. Under fluid compression, the throttling areas of both the upper and lower valves expand to some extent, with their spatial distributions closely following the pressure gradient and decreasing gradually along the flow direction. Compared with ambient conditions, thermal expansion under elevated temperatures causes a more pronounced increase in throttling area. Additionally, as hydraulic oil viscosity decreases with increasing temperature, flow velocities and mass flow rates rise significantly, leading to a marked deterioration in the throttling performance of the drilling jar under high-temperature downhole conditions. Full article
(This article belongs to the Section Machine Design and Theory)
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22 pages, 6816 KB  
Article
Synergistic Effects of Nano-SiO2 on Emulsion Film Stability and Non-Newtonian Rheology of Offshore Oil-Based Drilling Fluids
by Daicheng Peng, Fuhao Bao, Dong Yang, Lei Pu and Peng Xu
J. Mar. Sci. Eng. 2025, 13(9), 1722; https://doi.org/10.3390/jmse13091722 - 5 Sep 2025
Viewed by 563
Abstract
The ocean harbors vast potential for oil and gas resources, positioning offshore drilling as a critical approach for future energy exploration. However, high-temperature and high-pressure offshore reservoirs present formidable challenges, as conventional water-based drilling fluids are prone to thermal degradation and rheological instability, [...] Read more.
The ocean harbors vast potential for oil and gas resources, positioning offshore drilling as a critical approach for future energy exploration. However, high-temperature and high-pressure offshore reservoirs present formidable challenges, as conventional water-based drilling fluids are prone to thermal degradation and rheological instability, leading to wellbore collapse and stuck-pipe incidents. Offshore oil-based drilling fluids (OBDFs), typically water-in-oil emulsions, offer advantages in wellbore stability, lubricity, and contamination resistance, yet their stability under extreme high-temperature conditions remains limited. This study reveals the enhancement of offshore OBDFs performance in harsh conditions by employing nano-SiO2 to synergistically improve emulsion film stability and non-Newtonian rheological behavior while systematically elucidating the underlying mechanisms. Nano-SiO2 forms a composite film with emulsifiers, reducing droplet size, enhancing mechanical strength, and increasing thermal stability. Optimal stability was observed at an oil-to-water ratio of 7:3 with 2.5% nano-SiO2 dispersion and 4.0% emulsifier. Rheological analyses revealed that nano-silica enhances electrostatic repulsion, reduces plastic viscosity, establishes a network structure that increases yield stress, and promotes pronounced shear-thinning behavior. Macroscopic evaluations, including fluid loss, rheological performance, and electrical stability, further confirmed the improved high-temperature stability of offshore OBDFs with nano-SiO2 at reduced emulsifier concentrations. These findings provide a theoretical basis for optimizing offshore OBDFs formulations and their field performance, offering breakthrough technological support for safe and efficient drilling in ultra-high-temperature offshore reservoirs. Full article
(This article belongs to the Special Issue Offshore Oil and Gas Drilling Equipment and Technology)
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25 pages, 5500 KB  
Article
Analysis of CH4 Solubility Characteristics in Drilling Fluids: Molecular Simulation and Solubility Experiment
by Huaqing Liu, Linyan Guo, Dejun Cai, Xiansi Wang, Zhigang Li, Yongsheng Zhang and Chi Peng
Appl. Sci. 2025, 15(17), 9770; https://doi.org/10.3390/app15179770 (registering DOI) - 5 Sep 2025
Viewed by 198
Abstract
Based on molecular simulation methods, this paper constructs a molecular model of the CH4-drilling fluid system to conduct an in-depth analysis of the microscopic dissolution behavior of CH4 in drilling fluids. By utilizing key parameters such as molecular motion trajectories, [...] Read more.
Based on molecular simulation methods, this paper constructs a molecular model of the CH4-drilling fluid system to conduct an in-depth analysis of the microscopic dissolution behavior of CH4 in drilling fluids. By utilizing key parameters such as molecular motion trajectories, interaction energies and solubility free energies, the mechanisms of CH4 dissolution and diffusion are revealed. The factors influencing CH4 solubility and their variation mechanisms are elucidated at the molecular level. Through gas solubility experiments, the variation patterns of CH4 solubility in drilling fluids under different temperature and pressure conditions are investigated, and optimized solubility models for CH4-drilling fluid systems are selected. The results indicate that the dissolution and diffusion behavior of CH4 in drilling fluids can be described using free volume, interaction energy and solubility free energy, with the degree of influence ranked as follows: interaction energy > free volume > solubility free energy. The interaction and free volume of CH4 in oil-based drilling fluids are both greater than those in water-based drilling fluids, suggesting a higher solubility of CH4 in oil-based drilling fluids. Solubility models of CH4 in drilling fluids under conditions of 30~120 °C and 10~60 MPa are obtained by regression. The research findings not only deepen the understanding of the dissolution and diffusion behavior of CH4 in drilling fluids for shale gas horizontal wells, but also provide crucial parameters for establishing wellbore pressure models in managed pressure drilling. Full article
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15 pages, 7971 KB  
Article
Effect of Short Carbon Fiber Volume Fraction on High-Temperature Tensile Properties of SCF/2A12 Composite
by Jinhao Wu, Shiyin Huang, Qingnan Meng, Mu Yuan, Sifan Wang, Xinyue Mao, Yuting Qiu and Linkai He
Materials 2025, 18(17), 4143; https://doi.org/10.3390/ma18174143 - 4 Sep 2025
Viewed by 297
Abstract
To meet the increasing performance requirements of drilling pipes, including a reduced weight and enhanced mechanical and thermal properties, the application of aluminum alloys must be further advanced. Short-carbon-fiber-reinforced 2A12 aluminum alloy composites were fabricated via powder metallurgy. The density, hardness, and tensile [...] Read more.
To meet the increasing performance requirements of drilling pipes, including a reduced weight and enhanced mechanical and thermal properties, the application of aluminum alloys must be further advanced. Short-carbon-fiber-reinforced 2A12 aluminum alloy composites were fabricated via powder metallurgy. The density, hardness, and tensile strength of the composites were measured. The influence of the carbon fiber content on the composite’s mechanical properties was investigated across various temperatures. The composite material exhibited maximum yield strengths of 412 MPa at room temperature, 381 MPa at 180 °C, and 337 MPa at 220 °C. Incorporating carbon fibers increased the service temperature of a 2A12 aluminum alloy by approximately 40 °C. The strength increment of composites with a fiber content below 6 vol.% corresponded to the load transfer mechanism of carbon fiber, while the reason for non-conformity at a more than 6 vol.% fiber content was the continuous fracturing of carbon fibers, leading to the failure of the composites. Full article
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27 pages, 3899 KB  
Article
Experimental Study and Rheological Modeling of Water-Based and Oil-Based Drilling Fluids Under Extreme Temperature–Pressure Condition
by Haishen Lei, Chun Cai, Baolin Zhang, Jing Luo, Ping Chen and Dong Xiao
Energies 2025, 18(17), 4687; https://doi.org/10.3390/en18174687 - 3 Sep 2025
Viewed by 321
Abstract
With the growing demand for energy, oil and gas exploration and development are progressively moving into deep and ultra-deep formations, where extreme temperatures and pressures create complex challenges for drilling operations. While drilling fluids are critical for controlling bottom-hole pressure, cooling drill bits, [...] Read more.
With the growing demand for energy, oil and gas exploration and development are progressively moving into deep and ultra-deep formations, where extreme temperatures and pressures create complex challenges for drilling operations. While drilling fluids are critical for controlling bottom-hole pressure, cooling drill bits, and removing cuttings, accurately characterizing their rheological behavior under high-temperature and high-pressure (HTHP) conditions remains a key focus, as existing research has limitations in model applicability and parameter prediction range under extreme downhole environments. To address this, the study aims to determine the optimal rheological model and establish a reliable mathematical prediction model for drilling fluid rheological parameters under HTHP conditions, enhancing the precision of downhole temperature and pressure calculations. Rheological experiments were conducted on eight field-collected samples (4 water-based and four oil-based drilling fluids) using a Chandler 7600 HTHP rheometer, with test conditions up to 247 °C and 140 MPa; nonlinear fitting via a hybrid Levenberg–Marquardt and Universal Global Optimization algorithm and multivariate regression were employed for model development. Results showed that oil-based and water-based drilling fluids exhibited distinct rheological responses to temperature and pressure, with the Herschel–Bulkley model achieving superior fitting accuracy (coefficient of determination > 0.999). The derived prediction model for Herschel–Bulkley parameters, accounting for temperature-pressure coupling, demonstrated high accuracy (R2 > 0.95) in validation. This research provides an optimized rheological modeling approach and a robust prediction tool for HTHP drilling fluids, supporting safer and more efficient deep and ultra-deep drilling operations. Full article
(This article belongs to the Section B: Energy and Environment)
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28 pages, 13652 KB  
Article
Study of Structure and Phase Formation During Thermal Treatment of Geopolymer Compositions Based on Mineral Waste
by Elena A. Yatsenko, Sergei V. Trofimov, Yuri V. Novikov, Boris M. Goltsman and Vitaliy V. Sergeev
Materials 2025, 18(17), 4132; https://doi.org/10.3390/ma18174132 - 3 Sep 2025
Viewed by 509
Abstract
A comprehensive study was conducted to investigate the influence of mineral waste on the thermal stability of foamed geopolymer materials. The study’s objects were steelmaking slag (SS) from the Taganrog Metallurgical Plant, drilling sludge (DS) from the Sutorminskoye oil field, and an ash [...] Read more.
A comprehensive study was conducted to investigate the influence of mineral waste on the thermal stability of foamed geopolymer materials. The study’s objects were steelmaking slag (SS) from the Taganrog Metallurgical Plant, drilling sludge (DS) from the Sutorminskoye oil field, and an ash and slag mixture (ASM) from the Novocherkasskaya SDPP. The utilisation of drilling sludge as an additive in the production of geopolymers has been proposed for the first time. The study involved the development of alkaline activators based on solutions of sodium and potassium silicates and their hydroxides. The samples were synthesised with varying proportions of steelmaking slag and drilling sludge, and physicochemical, mechanical and high-temperature studies were conducted to ascertain the optimal composition. X-ray phase analysis of the synthesised samples was conducted. An investigation was conducted into alterations in the phase composition of the material as a consequence of heat treatment. Proposals were hereby made for the mechanisms of the formation of new phases. The study identified an alkaline activator based on a solution of silicate and sodium hydroxide, with the introduction of 10% steelmaking slag into the component mixture, as the most effective mixture. The resultant geopolymers exhibited a density of 311 kg/m3 and an ultimate compressive strength of 1.54 MPa. Full article
(This article belongs to the Topic Solid Waste Recycling in Civil Engineering Materials)
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15 pages, 3389 KB  
Article
Preparation, Performance Research and Field Application Practice of Temperature-Sensitive Lost Circulation Material for Shale Oil Wells
by Wenzhe Zhang, Jinsheng Sun, Feng Shen, Wei Li, Xianbin Huang, Kaihe Lv, Meichun Li, Shaofei Xue, Shiyu Wang and Hongmei Li
Polymers 2025, 17(17), 2395; https://doi.org/10.3390/polym17172395 - 2 Sep 2025
Viewed by 353
Abstract
Drilling fluid losses into formation voids are among the major issues that lead to increases in the costs and nonproductive time of operations. Lost circulation materials have been widely used to stop or mitigate losses. In most cases, the size of the loss [...] Read more.
Drilling fluid losses into formation voids are among the major issues that lead to increases in the costs and nonproductive time of operations. Lost circulation materials have been widely used to stop or mitigate losses. In most cases, the size of the loss zone is not known, making conventional lost circulation materials unsuitable for plugging the loss zone. In this study, novel temperature-sensitive LCM (TS-LCM) particles composed of diglycidyl ether of bisphenol A (DGEBA) and 4,4′-diaminodiphenyl methane were prepared. It is a thermal-response shape-memory polymer. The molecular structure was analyzed by Fourier transform infrared spectroscopy. The glass transition temperature (Tg) was tested by Different scanning calorimetry (DSC). The shape-memory properties were evaluated by a bend-recovery test instrument. The expansion and mechanical properties of particles were investigated under high temperature and high pressure. Fracture sealing testing apparatus was used to evaluate sealing performance. The mechanism of sealing fracture was discussed. Research results indicated that the Tg of the TS-LCM was 70.24 °C. The shape fixation ratio was more than 99% at room temperature, and the shape recovery ratio was 100% above the Tg. The particle was flaky before activation. It expanded to a cube shape, and the thickness increased when activated. The rate of particle size increase for D90 was more than 60% under 120 °C and 20 MPa. The activated TS-LCM particles had high crush strength. The expansion of the TS-LCM particles could self-adaptively bridge and seal the fracture without knowing the width. The addition of TS-LCM particles could seal the tapered slot with entrance widths of 2 mm, 3 mm and 4 mm without changing the lost circulation material formulation. The developed TS-LCM has good compatibility with local saltwater-based drilling fluid. In field tests in the Yan’an area of the Ordos Basin, 15 shale oil horizontal wells were plugged with excellent results. The equivalent circulating density of drilling fluid leakage increased by an average of 0.35 g/cm3, and the success rate of plugging malignant leakage increased from 32% to 82.5%. The drilling cycle was shortened by an average of 14.3%, and the effect of enhancing the pressure-bearing capacity of the well wall was significant. The prepared TS-LCM could cure fluid loss in a fractured formation efficiently. It has good prospects for promotion. Full article
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13 pages, 2752 KB  
Article
Development and Mechanistic Evaluation of Polymeric Nanomicrogels Under High-Temperature and High-Salinity Conditions
by Wei Zhang, Yinbo He, Tengfei Dong, Huayan Mu, Guancheng Jiang and Quande Wang
Gels 2025, 11(9), 689; https://doi.org/10.3390/gels11090689 - 30 Aug 2025
Viewed by 308
Abstract
Fracture-induced loss poses severe challenges to drilling operations, particularly under high-temperature and high-salinity conditions encountered in deep wells. Conventional plugging materials, characterized by relatively large particle sizes and poor structural integrity, often exhibit insufficient thermal stability and salt tolerance under extreme drilling conditions, [...] Read more.
Fracture-induced loss poses severe challenges to drilling operations, particularly under high-temperature and high-salinity conditions encountered in deep wells. Conventional plugging materials, characterized by relatively large particle sizes and poor structural integrity, often exhibit insufficient thermal stability and salt tolerance under extreme drilling conditions, making them prone to structural degradation and loss of adhesion, which ultimately leads to drilling fluid deterioration and downhole complications. To address this issue, a core–shell-structured microgel, ANDT-70 (named after the acronyms of 2-acrylamido-2-methylpropane sulfonic acid, N-vinyl-2-pyrrolidinone, N, N-dimethylacrylamide, dimethyl diallyl ammonium chloride, and titanium dioxide nanoparticles), was synthesized and systematically evaluated for its thermal stability, salt resistance, and interfacial adhesion capabilities. The structural evolution, dispersion behavior, and colloidal stability of the microgel were thoroughly characterized using scanning electron microscopy (SEM), transmission electron microscopy (TEM), atomic force microscopy (AFM), Raman spectroscopy, and Zeta potential analysis. Experimental results indicate that ANDT-70 exhibits excellent thermal stability and resistance to salt-induced degradation at 260 °C, maintaining its fundamental structure and performance under harsh high-temperature and high-salinity conditions, with a viscosity retention of 81.10% compared with ambient conditions. Compared to representative materials reported in the literature, ANDT-70 exhibited superior tolerance to ionic erosion in saline conditions. AFM analysis confirmed that ANDT-70 significantly improves bentonite slurry dispersion and reduces salt sensitivity risks. ANDT-70 stably adsorbs onto bentonite lamellae via the synergistic action of electrostatic interactions and hydrogen bonding, thereby forming a dense cementation network that markedly enhances the structural stability and adhesion of the system. This network significantly enhances the cohesion and structural integrity of drilling fluid systems under extreme conditions. In conclusion, ANDT-70 demonstrates strong potential as a high-performance functional microgel for enhancing the stability and effectiveness of advanced drilling fluids under complex geological environments. Full article
(This article belongs to the Special Issue Polymer Gels for Oil Recovery and Industry Applications)
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15 pages, 5326 KB  
Article
Study on the Construction of a Nonlinear Creep Constitutive Model of Salt-Gypsum Rock in the Bayan Deep and the Critical Value of Wellbore Shrinkage Liquid Column Pressure
by Penglin Liu, Aobo Yin, Tairan Liang, Wen Sun, Wei Lian, Bo Zhang, Shanpo Jia and Jinchuan Huang
Processes 2025, 13(9), 2747; https://doi.org/10.3390/pr13092747 - 28 Aug 2025
Viewed by 323
Abstract
Aiming at the problems of borehole shrinkage and pipe sticking caused by creep in salt-gypsum rock formations during deep well drilling, multi-field coupling creep experiments on deep salt-bearing gypsum mudstone were carried out. Furthermore, a nonlinear creep constitutive model was constructed based on [...] Read more.
Aiming at the problems of borehole shrinkage and pipe sticking caused by creep in salt-gypsum rock formations during deep well drilling, multi-field coupling creep experiments on deep salt-bearing gypsum mudstone were carried out. Furthermore, a nonlinear creep constitutive model was constructed based on the Drucker–Prager criterion, and the critical value of liquid column pressure for borehole shrinkage was determined through numerical simulation. Experiments show that at 140 °C, salt-gypsum rock is mainly subjected to brittle failure with single shear fracture, while at 180 °C, multiple sets of cross-cutting shear bands form, shifting to plastic flow-dominated composite failure. The coupling effect of confining pressure and deviatoric stress is temperature-dependent; the critical deviatoric stress is independent of confining pressure at 140 °C, but decreases significantly with increasing confining pressure at 180 °C, revealing that salt-gypsum rock is more prone to plastic flow under high temperatures and confining pressure. The creep constitutive equation was further determined, and fitting parameters show that the stress exponent m = 2–5 and the time exponent n decrease linearly with the increase in deviatoric stress, and the model can accurately describe the characteristics of three-stage creep. The numerical simulation found that there is a nonlinear relationship between the drilling fluid density and borehole shrinkage; the shrinkage rate exceeds 1.47% when the density is ≤2.0 g/cm3, and the expansion amount is >1.0 mm when ≥2.4 g/cm3. The critical safe density range is 2.1–2.3 g/cm3, which is consistent with the field data in the Bayan area. The research results provide an experimental basis and quantitative method for the dynamic regulation of drilling fluid density in deep gypsum rock formations, and have engineering guiding significance for preventing borehole wall instability. Full article
(This article belongs to the Section Energy Systems)
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17 pages, 4876 KB  
Article
Enhancing Rheology and Wettability of Drilling Fluids at Ultra-Low Temperatures Using a Novel Amide Material
by Ning Huang, Jinsheng Sun, Jingping Liu, Kaihe Lv, Xuefei Deng, Taifeng Zhang, Yuanwei Sun, Han Yan and Delin Hou
Gels 2025, 11(9), 687; https://doi.org/10.3390/gels11090687 - 28 Aug 2025
Viewed by 408
Abstract
The ice sheet and subglacial geological environment in Antarctica have become the focus of scientific exploration. The development of Antarctic drilling technology will serve as a crucial safeguard for scientific exploration. However, the extremely ultra-low temperatures and intricate geological conditions present substantial obstacles [...] Read more.
The ice sheet and subglacial geological environment in Antarctica have become the focus of scientific exploration. The development of Antarctic drilling technology will serve as a crucial safeguard for scientific exploration. However, the extremely ultra-low temperatures and intricate geological conditions present substantial obstacles for drilling operations in Antarctica, and the existing drilling fluid technology cannot satisfy the requirements of efficient and safe drilling. To ameliorate the wettability and rheology of ultra-low-temperature drilling fluids, a new amide material (HAS) was prepared using dodecylamine polyoxyethylene ether, azelaic acid, and N-ethylethylenediamine as raw materials. Experiments using infrared spectroscopy, nuclear magnetic hydrogen spectroscopy, and contact angle indicated that the target product was successfully synthesized. Performance evaluation showed that 2% HAS could achieve a yield point of 2.5 Pa for drilling fluid at −55 °C, and it also gave the fluid superior shear-thinning characteristics and a large thixotropic loop area. This indicated that HAS significantly enhanced the rheological properties of the drilling fluid, ensuring that it can carry cuttings and ice debris. In addition, 2% HAS could also increase the colloidal rate from 8% to more than 76% at −55 °C in different base oils. Meanwhile, the colloid rate was maintained above 92.4% when the density was 0.92~0.95 g/cm3. Mechanism studies showed that HAS increased the zeta potential and decreased the particle size of organoclay. At the same time, it changed the organoclay state from a clustered state to a uniformly dispersed state, and the particle size decreased. It was found that HAS formed a weak gel grid structure through interactions between polar groups, such as amide and imino groups with organoclays particles, thus improving the rheology and wettability of drilling fluid. In addition, HAS is an environmentally friendly high-performance material. Full article
(This article belongs to the Section Gel Applications)
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21 pages, 4866 KB  
Article
Research on the Formation-Wellbore Temperature Profile Characteristics Under the Co-Existence of Kick and Leakage Condition
by Yufei Chen, Mu Li, Hao Wang, Weiwei Hao, Kerou Liu, Yafei Li, Hui Zhang and Geng Zhang
Processes 2025, 13(9), 2730; https://doi.org/10.3390/pr13092730 - 26 Aug 2025
Viewed by 1070
Abstract
During drilling, different kick locations significantly impact the formation-wellbore temperature (FWT) profile under the co-existence of kick and leakage condition (CKL). To ensure safety and efficiency during drilling, we study the effect of different kick locations on the FWT under the CKL. In [...] Read more.
During drilling, different kick locations significantly impact the formation-wellbore temperature (FWT) profile under the co-existence of kick and leakage condition (CKL). To ensure safety and efficiency during drilling, we study the effect of different kick locations on the FWT under the CKL. In this paper, a full transient heat transfer model based on the first law of thermodynamics is established to obtain four distinct WFT profiles under CKL conditions, incorporating both convective heat transfer and variable mass flow effects. Compared with the actual temperature measurement data, the reliability of the developed model is verified. The case studies show that the annular temperature (AT) is lower under the single-point leakage (SL), continuous leakage (CL), and CKL conditions than that in the normal drilling condition. Wellhead temperature in CKL differs significantly from that in normal drilling (ND). As the kick location gets closer to the bottom hole, the AT gets higher, and the temperature difference between the formation and annular gets smaller. Compared with the wellbore temperature profile under ND, the kick location can be detected by real-time monitoring of the FWT profile under the CKL. Full article
(This article belongs to the Section Energy Systems)
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11 pages, 8530 KB  
Article
Towards Manufacturing High-Quality Film-Cooling Holes Using Femtosecond Laser Combined with Abrasive Flow
by Lifei Wang, Zhen Wang, Junjie Xu, Wanrong Zhao and Zhen Zhang
Micromachines 2025, 16(9), 973; https://doi.org/10.3390/mi16090973 - 25 Aug 2025
Viewed by 419
Abstract
Film-cooling holes are the key cooling structures of turbine blades, and there are still great challenges in manufacturing high-quality film-cooling holes. Although abrasive flow machining can be used as a post-processing technique to optimize the quality of film-cooling holes, its action process and [...] Read more.
Film-cooling holes are the key cooling structures of turbine blades, and there are still great challenges in manufacturing high-quality film-cooling holes. Although abrasive flow machining can be used as a post-processing technique to optimize the quality of film-cooling holes, its action process and influence mechanism have not been systematically studied. Herein, the drilling method of femtosecond laser combined with abrasive flow is studied in detail. Moreover, for comparison, the drilling methods of single femtosecond laser, single electrical discharge machining, and electrical discharge machining combined with abrasive flow are also discussed. The microstructure and composition distribution of the hole walls before and after abrasive flow machining were systematically characterized, indicating that abrasive flow can effectively remove the recast layer and cause local plastic deformation. Due to the surface hardening and non-uniform residual stress caused by abrasive impact, abrasive flow machining can increase the high-temperature endurance time of film-cooling holes while reducing the elongation. The combination of femtosecond laser and abrasive flow machining demonstrates the best high-temperature mechanical properties, with the endurance time and elongation reaching 136.15 h and 12.1%, respectively. The fracture mechanisms of different drilling methods are further discussed in detail. The research results provide theoretical guidance for the manufacturing of high-quality film-cooling holes through the composite processing of femtosecond laser and abrasive flow. Full article
(This article belongs to the Special Issue Recent Advances in Micro/Nanofabrication, 2nd Edition)
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17 pages, 2566 KB  
Article
Synergistic Epichlorohydrin-Crosslinked Carboxymethyl Xylan for Enhanced Thermal Stability and Filtration Control in Water-Based Drilling Fluids
by Yutong Li, Fan Zhang, Bo Wang, Jiaming Liu, Yu Wang, Zhengli Shi, Leyao Du, Kaiwen Wang, Wangyuan Zhang, Zonglun Wang and Liangbin Dou
Gels 2025, 11(8), 666; https://doi.org/10.3390/gels11080666 - 20 Aug 2025
Viewed by 283
Abstract
Polymers derived from renewable polysaccharides offer promising avenues for the development of high-temperature, environmentally friendly drilling fluids. However, their industrial application remains limited by inadequate thermal stability and poor colloidal compatibility in complex mud systems. In this study, we report the rational design [...] Read more.
Polymers derived from renewable polysaccharides offer promising avenues for the development of high-temperature, environmentally friendly drilling fluids. However, their industrial application remains limited by inadequate thermal stability and poor colloidal compatibility in complex mud systems. In this study, we report the rational design and synthesis of epichlorohydrin-crosslinked carboxymethyl xylan (ECX), developed through a synergistic strategy combining covalent crosslinking with hydrophilic functionalization. When incorporated into water-based drilling fluid base slurries, ECX facilitates the formation of a robust gel suspension. Comprehensive structural analyses (FT-IR, XRD, TGA/DSC) reveal that dual carboxymethylation and ether crosslinking impart a 10 °C increase in glass transition temperature and a 15% boost in crystallinity, forming a rigid–flexible three-dimensional network. ECX-modified drilling fluids demonstrate excellent colloidal stability, as evidenced by an enhancement in zeta potential from −25 mV to −52 mV, which significantly improves dispersion and interparticle electrostatic repulsion. In practical formulation (1.0 wt%), ECX achieves a 620% rise in yield point and a 71.6% reduction in fluid loss at room temperature, maintaining 70% of rheological performance and 57.5% of filtration control following dynamic aging at 150 °C. Tribological tests show friction reduction up to 68.2%, efficiently retained after thermal treatment. SEM analysis further confirms the formation of dense and uniform polymer–clay composite filter cakes, elucidating the mechanism behind its high-temperature resilience and effective sealing performance. Furthermore, ECX demonstrates high biodegradability (BOD5/COD = 21.3%) and low aquatic toxicity (EC50 = 14 mg/L), aligning with sustainable development goals. This work elucidates the correlation between molecular engineering, gel microstructure, and macroscopic function, underscoring the great potential of eco-friendly polysaccharide-based crosslinked polymers for industrial gel-based fluid design in harsh environments. Full article
(This article belongs to the Section Gel Chemistry and Physics)
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22 pages, 6027 KB  
Article
Study on the Process Characteristics of Picosecond Laser Trepan Cutting Hole Manufacturing for Heat-Resistant Steel
by Liang Wang, Long Xu, Changjian Wu, Yefei Rong and Kaibo Xia
Metals 2025, 15(8), 917; https://doi.org/10.3390/met15080917 - 19 Aug 2025
Viewed by 326
Abstract
Picosecond laser drilling offers high precision and quality, and compared to femtosecond lasers, it also balances processing efficiency, making it widely used across various fields. However, existing drilling processes still face issues such as roundness and taper. Therefore, further research into the processing [...] Read more.
Picosecond laser drilling offers high precision and quality, and compared to femtosecond lasers, it also balances processing efficiency, making it widely used across various fields. However, existing drilling processes still face issues such as roundness and taper. Therefore, further research into the processing characteristics of picosecond laser technology is needed to improve processing quality. This paper uses ANSYS software to conduct numerical simulations of picosecond laser ring-cutting drilling, analyzing the temperature field of microholes under ring-cutting scanning paths as parameters change. Experimental studies were conducted using AISI 310S heat-resistant stainless steel as the base material. This material exhibits excellent high-temperature oxidation resistance and strength retention, making it suitable for laser thermal processing. Using a single-factor method, the study investigated the influence of equidistant concentric circular paths and inner-dense-outer-sparse concentric circular paths on microhole morphology characteristics. The results show that the laser energy distribution is different under different paths. The entrance aperture of the equidistant concentric circle path is larger than that of the inner dense and outer sparse concentric circle path, while the exit aperture is smaller than the latter. Moreover, the roundness is also better than that of the inner dense and outer sparse concentric circle path. The taper of the inner dense and outer sparse concentric circle path is better than that of the equidistant concentric circle path. This study can provide a reference for the optimization of different processing paths in the future. Full article
(This article belongs to the Special Issue High-Energy Beam Machining of Metals)
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30 pages, 2129 KB  
Article
Theoretical and Simulation Study of CO2 Laser Pulse Coupled with Composite Mechanical Drill Bit for Rock-Breaking Technology
by Lei Tao, Hailu Li, Liangzhu Yan and Zhiyuan Zhou
Processes 2025, 13(8), 2619; https://doi.org/10.3390/pr13082619 - 19 Aug 2025
Viewed by 529
Abstract
Facing challenges of low efficiency and severe wear in deep hard formations with conventional drilling bits, this study investigates the synergistic rock-breaking technology combining a pulsed CO2 laser with mechanical bits. The background highlights the need for novel methods to enhance drilling [...] Read more.
Facing challenges of low efficiency and severe wear in deep hard formations with conventional drilling bits, this study investigates the synergistic rock-breaking technology combining a pulsed CO2 laser with mechanical bits. The background highlights the need for novel methods to enhance drilling speed in high-strength, abrasive strata where traditional bits struggle. The theoretical analysis explores the thermo-mechanical coupling mechanism, where pulsed laser irradiation rapidly heats the rock surface, inducing thermal stress cracks, micro-spallation, and strength reduction through mechanisms like mineral thermal expansion mismatch and pore fluid vaporization. This pre-damage layer facilitates subsequent mechanical fragmentation. The research employs finite element numerical simulations (using COMSOL Multiphysics with an HJC constitutive model and damage evolution criteria) to model the coupled laser–mechanical–rock interaction, capturing temperature fields, stress distribution, crack propagation, and assessing efficiency. The results demonstrate that laser pre-conditioning significantly achieves 90–120% higher penetration rates compared to mechanical-only drilling. The dominant spallation mechanism proves energy-efficient. Conclusions affirm the feasibility and significant potential of CO2 laser-assisted drilling for deep formations, contingent on optimized laser parameters, composite bit design (incorporating laser transmission, multi-head layout, and environmental protection), and addressing challenges, like high in-situ stress and drilling fluid interference through techniques like gas drilling. Future work should focus on high-power laser downhole transmission, adaptive control, and rigorous field validation. Full article
(This article belongs to the Section Automation Control Systems)
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