Search Results (183)

This study investigates the shear strength of lotus-type unidirectional porous copper bonded to alumina substrates using the Direct Bonded Copper (DBC) process. Porous copper specimens with various porosities (38.7–50.9%) and pore sizes (150–800 $\mathsf{\mu }$m) were fabricated and joined to alumina discs. Shear testing revealed that both porosity and pore size significantly affect the interfacial strength. While higher porosity led to reduced shear strength, larger pore sizes enhanced the maximum shear strength owing to increased local contact areas and crack coalescence in the alumina substrate. Fractographic analysis using optical microscopy and SEM-EDS confirmed that failure mainly occurred in the alumina, with local fracture associated with pore distribution and size. To improve strength prediction, a modified model was proposed, reducing the error from 12.3% to 7.5% and increasing the coefficient of determination (R²) from 0.43 to 0.74. These findings highlight the necessity of considering both porosity and pore size when predicting the shear strength of porous copper/alumina DBC joints, and they provide important insights for optimizing metal structures in metal–ceramic bonding for high-performance applications. Full article

This study investigates the effect of hydrogen charging time on the mechanical properties and microstructural evolution of low-carbon ferrite–pearlite steel that has been in service for over 30 years in natural gas transmission. Specimens were subjected to in-situ electrochemical hydrogen charging for varying durations, followed by tensile testing. Detailed microstructural analysis was performed using scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Despite negligible changes in the overall hydrogen content ($C_H$≈ 4.0 wppm), significant alterations in fracture morphology were observed. Fractographic and TEM analyses revealed a clear transition from ductile fracture in uncharged specimens to a predominance of brittle fracture modes (quasi-cleavage, intergranular, and transgranular) in hydrogen-charged samples. The results show time-dependent microstructural changes, including increased dislocation density and the formation of prismatic loop debris, particularly within the ferrite phase. Prolonged charging leads to localized embrittlement, which is explained by enhanced hydrogen trapping at ferrite-cementite boundaries, grain boundaries, and dislocation cores. TEM investigations further indicated a sequential activation of hydrogen embrittlement mechanisms: initially, Hydrogen-Enhanced Localized Plasticity (HELP) dominates within ferrite grains, followed by Hydrogen-Enhanced Decohesion (HEDE), particularly at ferrite-cementite interfaces in pearlite colonies. These findings demonstrate that extended hydrogen charging promotes defect localization, dislocation pinning, and interface decohesion, ultimately accelerating fracture propagation. The study provides valuable insight into the degradation mechanisms of ferrite-pearlite steels exposed to hydrogen, highlighting the importance of charging time. The results are essential for assessing the reliability of legacy pipeline steels and guiding their safe use in future hydrogen transport infrastructure. Full article

This in vitro study aimed to evaluate the fatigue behavior of occlusal veneers (OVs) made of lithium disilicate and composition-gradient multilayered zirconia at different thicknesses, incorporating both experimental and theoretical analyses to predict long-term performance. Seventy-two OVs with ceramic layer thicknesses of 0.5 mm, 1.0 mm, and 1.5 mm were fabricated and adhesively bonded to dentin analog composite abutments. All specimens underwent thermomechanical fatigue testing, involving cyclic loading (49 N, 1.6 Hz, 1.2 million cycles) and thermocycling (5–55 °C), simulating five years of clinical function. Fracture patterns were analyzed using light microscopy and scanning electron microscopy. A fatigue lifetime model based on plate-on-foundation theory and slow crack growth was applied to estimate cycles to radial failure. No complete fractures or debonding occurred. However, 50% of 0.5 mm zirconia OVs developed flexural radial cracks from the intaglio surface, while all lithium disilicate and zirconia veneers ≥1.0 mm remained intact. Theoretical predictions closely matched the experimental outcomes, indicating that 0.5 mm zirconia performance aligned with the lower-bound fatigue estimates for 5Y-PSZ. Results suggest that lithium disilicate offers superior fatigue resistance at minimal thickness, while thin zirconia is prone to subsurface cracking. A minimum thickness of 0.7 mm is recommended for zirconia-based OVs. Full article

To address the brittle matrix failure frequently observed in filament-wound composite layers of onboard pressure vessels operating under cryogenic and high-pressure conditions, we studied a bisphenol-A epoxy resin (DGEBA) system modified with polyetheramine (T5000) and 3,4-Epoxycyclohexylmethyl 3′,4′-epoxycyclohexanecarboxylate (CY179). The curing and rheological behavior of the modified resin were first evaluated, revealing a favorable processing, with viscosity suitable for wet-filament winding. Subsequently, its coefficient of thermal expansion (CTE) and tensile properties were characterized over the 300 K–90 K range, demonstrating a linear increase in elastic modulus and tensile strength with decreasing temperature. Carbon fibre-reinforced polymer composites (CFRP) were then fabricated using this resin system, and both longitudinal and transverse tensile tests, along with microscopic fracture surface analyses, were conducted. The results showed that CFRP-0° specimens exhibited an initial increase followed by a decrease in elastic modulus with decreasing temperature, whereas CFRP-90° specimens demonstrated pronounced cryogenic strengthening, with tensile strength and modulus enhanced by 52.2% and 82.4%, respectively. The findings provide comprehensive properties for the studied resin system and its CFRP under room temperature (RT) to cryogenic conditions, offering a basis for the design and engineering of cryo-compressed hydrogen storage vessels. Full article

This study investigates the effect of polymer film lamination on the tensile performance of wood fiber-reinforced polypropylene (WP) composites. Neat polypropylene (PP) and WP containing 25 wt% wood fiber were injection-molded and laminated with 0.1 mm PP or polyethylene terephthalate (PET) films using a compatible adhesive. Four configurations were examined: unlaminated (0S), single-sided half-length (1S-H), single-sided full-length (1S-F), and double-sided full-length (2S-F). Mechanical properties and fracture morphology were characterized by uniaxial tensile tests and scanning electron microscopy (SEM), alongside measurements of surface roughness. PET lamination produced the greatest strength enhancements, with 2S-F specimens achieving gains of 12% for PP and 21% for WP, whereas PP lamination gave minimal or negative effects, except for a 5% increase in WP. Strength improvements were attributed to surface smoothing and suppression of crack initiation, as confirmed by roughness measurements and SEM observations. PET’s higher stiffness and strength accounted for its superior reinforcement relative to PP. Fractographic analysis revealed flat regions near specimen corners—interpreted as crack initiation sites—indicating that lamination delayed crack propagation. The results demonstrate that PET film lamination is an effective and practical post-processing strategy for enhancing the mechanical performance of wood–plastic composites. Full article

The rising demand for aluminium and environmental concerns highlight the need for a circular economy using recycled alloys. This study examines the effect of shot peening on the high-cycle fatigue life of secondary AlZn10Si8Mg alloys with different iron contents: Alloy A (0.14 wt.% Fe) and Alloy B (0.56 wt.% Fe). Although both alloys showed similar tensile properties, Alloy B had higher porosity and finer β-Al₅FeSi intermetallics. Shot peening was applied at 100% and 1000% coverage to evaluate changes in surface roughness, porosity, residual stresses, and fatigue performance. The treatment significantly reduced surface-connected porosity via plastic deformation, enhancing fatigue life despite increased roughness. Fatigue tests showed a 21% increase in fatigue limit for Alloy A and a 6% gain for Alloy B at higher coverage. Fractographic analysis revealed that 95% of fatigue cracks initiated at surface pores. Residual stress measurements confirmed compressive stresses were limited to the near-surface layer, with minimal influence on subsurface crack propagation. Overall, shot peening proves to be an effective method for improving fatigue resistance in recycled aluminium alloys, even in alloys with elevated iron content, reinforcing their potential for structural applications under cyclic loading. Full article

Laser powder bed fusion (LPBF) can fabricate hydraulic components with significant weight reduction, and in this study, small punch tests (SPTs) evaluated the tensile and fracture properties of four stainless steels (30Cr13, 316L, 15-5PH, 17-4PH), alongside metallographic, scanning electron microscope (SEM), and Electron Backscatter Diffraction (EBSD) analyses which examined their fracture modes, grain orientation, phase distribution, and grain boundary distribution. The tensile property results showed ductility rankings as 316L > 17-4PH > 15-5PH > 30Cr13, with correlations between R_p0.2 and R_m from SPT and uniaxial tensile tests for all four, while high-magnification SEM fractographs revealed ductile dimples on 15-5PH, 17-4PH, and 316L SPT specimens versus distinct cleavage fracture in 30Cr13. EBSD analysis indicated austenite content order as 316L > 17-4PH > 30Cr13 > 15-5PH, grain size order as 316L > 17-4PH > 15-5PH > 30Cr13, and high-angle grain boundaries ranking as 15-5PH > 30Cr13 > 17-4PH > 316L; additionally, notched SPT specimens inspected per EN 10371 for fracture toughness showed J-integral (J_IC) values in the order 316L > 17-4PH > 15-5PH > 30Cr13, consistent with ductility and grain size results. Full article

This study investigated the effect of laser shock peening (LSP) treatment on the fatigue performance of Q355D steel butt-welded joints. The results demonstrate that LSP sig-nificantly enhances joint fatigue resistance through gradient hardening in surface lay-ers, introduction of high-magnitude residual compressive stress fields, and micro-structural refinement. Specifically, microhardness increased across all joint zones with gradient attenuation of strengthening effects within an approximately 700 μm depth. LSP effectively suppressed residual tensile stress concentration in regions beyond 4 mm on both sides of the weld. Fatigue tests confirmed that LSP substantially extended joint fatigue life: by 113–165% in the high-stress region (250–270 MPa) and 46–63% in the medium-low-stress region (230–240 MPa). Fractographic analysis further revealed reduced fatigue striation spacing and lower microcrack density in LSP-treated speci-mens, reflecting the synergistic effect of residual compressive stress fields and micro-structural refinement in retarding crack propagation. This work substantiates LSP as an effective method for enhancing fatigue resistance in Q355D steel welded joints. Full article

This study investigates premature fatigue failures in three EA1N steel axles from permanent magnet direct-drive locomotives during wheel-seat bending tests. Complete fracture occurred in one axle at 3 million cycles, and in the other two axles, cracks appeared and were observed through magnetic particle detection at 3.5 million and 1.6 million cycles, respectively. A comprehensive failure analysis was conducted through metallurgical examination, fractography, mechanical testing, residual stress measurement, and finite element analysis. The fractographic results revealed fractures consistently initiated at the wheel-seat to axle-body transition arc, exhibiting characteristic ratchet marks and beach patterns. The premature fracture mechanism was identified as a high-stress fatigue fracture. The residual stress measurements showed detrimental tensile stresses at the surface. Coupled with the operating stress, the stress on the axle exceeds fatigue strength, which accelerates the initiation and propagation of fatigue cracks. Based on these observations, the failure mechanism was identified, and preventive methods were proposed to reduce the risk of recurrence of the in-service axles. Full article

This study introduces a time-efficient rotating bending fatigue testing system featuring 11 dual-end spindles, enabling simultaneous testing of 22 specimens. Designed for high-throughput fatigue life (S–N curve) assessment, the system theoretically allows over 93% reduction in total test duration, with 87.5% savings demonstrated in validation experiments using AISI 304 stainless steel. The PLC-based architecture provides autonomous operation, real-time failure detection, and automatic cycle logging. ER16 collet holders are easily replaceable within one minute, and all the components are selected from widely available industrial-grade parts to ensure ease of maintenance. The modular design facilitates straightforward adaptation to different station counts. The validation results confirmed an endurance limit of 421 MPa, which is consistent with the established literature and within ±5% deviation. Fractographic analysis revealed distinct crack initiation and propagation zones, supporting the observed fatigue behavior. This high-throughput methodology significantly improves testing efficiency and statistical reliability, offering a practical solution for accelerated fatigue life evaluation in structural, automotive, and aerospace applications. Full article

Discontinuous fibers are commonly added to matrix materials in additive manufacturing to enhance properties, but such benefits may be constrained by print and fiber orientation. The additive processes of forming rasters and layers in powder bed fusion inherently cause anisotropy in printed parts. Many print parameters, such as laser, temperature, and hatch pattern, influence the anisotropy of tensile properties. This study characterizes fiber orientation attributed to recoating non-encapsulated fibers and the resulting anisotropic tensile properties. Tensile and fracture properties of polyamide 12 reinforced with 0%, 2.5%, 5%, and 10% discontinuous carbon fibers by volume were characterized in two primary print/tensile loading orientations: tensile loading parallel to the recoater (“horizontal specimens”) and tensile load along the build axis (“vertical specimens”). Density and fractographic analysis indicate a homogeneous mixture with low porosity and primary fiber orientation along the recoating direction for both print orientations. Neat specimens (zero fiber) loaded in either direction have similar tensile properties. However, fiber-reinforced vertical specimens have significantly reduced consistency and tensile strength as fiber content increased, while the opposite is true for horizontal specimens. These datasets and results provide a mechanism to tune material properties and improve the functionality of selectively laser-sintered fiber-reinforced parts through print orientation selection. These datasets could be used to customize functionally graded parts with multi-material selective laser-sintering manufacturing. Full article

Silica/alumina composite particles were synthesized via the sol–gel method to promote fine dispersion and homogenous mixing. Aluminum chloride hydroxide served as the alumina precursor, while amorphous silica, obtained from rice husk, was directly incorporated into the alumina sol. Following synthesis, the material was calcined at 1000 °C, yielding an α-cristobalite form of silica and corundum-phase alumina. These hybrid particles were introduced into polymer composites at reinforcement levels of 1 wt.%, 3 wt.%, and 5 wt.%. Mechanical behavior was evaluated through three-point bending tests, Shore D hardness measurements, and controlled-energy impact testing. Among the formulations, the 3 wt.% composite exhibited optimal performance, displaying the highest flexural modulus and strength, along with enhanced impact resistance. Hardness increased with rising particle content. Fractographic analysis revealed that the 3 wt.% loading produced a notably rougher fracture surface, correlating with improved energy absorption. In contrast, the 5 wt.% composite, although harder than the matrix and other composites, exhibited diminished toughness due to particle agglomeration. Full article

Nodular Cast Iron (NCI, also known as ductile iron) is widely used in important components such as crankshafts for automotive engines and internal combustion engines, as well as storage and transportation containers for spent fuel in nuclear power plants, due to its good comprehensive mechanical properties such as strength, toughness, and wear resistance. The effect of temperature on the fracture behavior of NCI was investigated using compact tensile (CT) specimens at different temperatures. The results showed that the conditional fracture toughness parameter (K_Q) of the NCI specimens firstly increased and then decreased with decreasing temperature. The crack tip opening displacement δ_m shows a significant ductile–brittle transition behavior with the decreasing of temperature. δ_m remains constant in the upper plateau region but sharply decreases in the ductile–brittle region (−60 °C to −100 °C) and stabilizes at a smaller value in the lower plateau region. Multiscale fractographic analysis indicated that the fracture mechanism changed from ductile fracture (above −60 °C) to ductile–brittle mixed (−60 °C to −100 °C) and then to completely brittle fracture (below −100 °C). As the temperature decreased, the fracture characteristics changed from ductile dimples to dimple and cleavage mixed and then to brittle cleavage. Full article

This study examines the microstructural evolution, mechanical properties, and wear behavior of medium-carbon dual-phase steel (AISI 1040) processed via Multi-Axis Compression (MAC). The DP steel was produced through inter-critical annealing at 745 °C, followed by MAC at 500 °C, resulting in a refined grain microstructure. Optical micrographs confirmed the presence of ferrite and martensite phases after annealing, with significant grain refinement observed following MAC. The average grain size decreased from 66 ± 4 μm to 18 ± 1 μm after nine MAC passes. Mechanical testing revealed substantial improvements in hardness (from 145 ± 9 HV to 298 ± 18 HV) and ultimate tensile strength (from 557 ± 33 MPa to 738 ± 44 MPa), attributed to strain hardening and the Hall–Petch effect. Fractographic analysis revealed a ductile failure mode in the annealed sample, while DP0 and DP9 exhibited a mixed fracture mode. Both DP0 and DP9 samples demonstrated superior wear resistance compared to the annealed sample. However, the DP9 sample exhibited slightly lower wear resistance than DP0, likely due to the fragmentation of martensite induced by high accumulated strain, which could act as crack initiation sites during sliding wear. Furthermore, wear resistance was significantly enhanced due to the combined effects of the DP structure and Severe Plastic Deformation (SPD). These findings highlight the potential of MAC processing for developing high-performance steels suitable for lightweight automotive applications. Full article

Fused Filament Fabrication (FFF) is a widely adopted additive manufacturing technique, yet its mechanical performance is highly dependent on process parameters, particularly nozzle diameter and printing speed. This study evaluates the influence of these parameters on the tensile behavior of Acrylonitrile Butadiene Styrene (ABS) and Polylactic Acid (PLA), aiming to determine optimal conditions for enhanced strength. ASTM D638-Type IV specimens were printed using nozzle diameters ranging from 0.05 to 0.25 mm and speeds from 15 to 80 mm/s. For ABS, tensile strength increased from 56.46 MPa to 60.74 MPa, representing a 7.6% enhancement, as nozzle diameter increased, with the best performance observed at 0.25 mm and 45 mm/s, attributed to improved melt flow and interlayer fusion. PLA exhibited a non-linear response, reaching a maximum strength of 89.59 MPa under the same conditions, marking a 22.3% enhancement over the minimum value. The superior performance of PLA was linked to optimal thermal management that enhanced crystallinity and interlayer bonding. Fractographic analysis revealed reduced porosity and smoother fracture surfaces under optimized conditions. Overall, PLA consistently outperformed ABS across all settings, with an average tensile strength advantage of 47.5%. The results underscore the need for material-specific parameter tuning in FFF and offer practical insights for optimizing mechanical performance in applications demanding high structural integrity, including biomedical, aerospace, and functional prototyping. Full article