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Search Results (1,962)

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Keywords = microwave systems

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18 pages, 3279 KB  
Review
Ablative Techniques for the Management of Osseous Spine Metastases: A Narrative Review
by Zach Pennington, Jonathan M. Morris, Aladine Elsamadicy, Sheng-Fu Larry Lo, Joseph H. Schwab and Daniel M. Sciubba
J. Clin. Med. 2025, 14(18), 6358; https://doi.org/10.3390/jcm14186358 (registering DOI) - 9 Sep 2025
Abstract
With continued improvements in systemic cancer therapies, there has been an increase in the survivorship of patients with spinal metastases. However, many patients with spinal metastases are frail and may not be able to tolerate the morbidity of open surgery. For these patients, [...] Read more.
With continued improvements in systemic cancer therapies, there has been an increase in the survivorship of patients with spinal metastases. However, many patients with spinal metastases are frail and may not be able to tolerate the morbidity of open surgery. For these patients, percutaneous ablation techniques offer a minimally invasive approach that can facilitate local tumor control and pain relief. Here we describe the currently employed modalities—radiofrequency ablation (RFA), microwave ablation (MWA), cryoablation, and laser interstitial thermal therapy (LITT)—summarize the clinical support for their use, and overview the relative risks and benefits for each. All these technologies offer to help improve local tumor control and improve oncologic pain associated with vertebral metastases, and they have become a staple of multidisciplinary spine metastasis care at many centers. As clinical experience with these technologies continues to grow, their use will likely become more widely adopted, and so understanding of their indications, risks, and benefits will become increasingly important to the practicing spine oncologist. Full article
(This article belongs to the Section Orthopedics)
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4689 KB  
Article
A Novel Compact Beamforming Network Based on Quasi-Twisted Branch Line Coupler for 5G Applications
by Fayyadh H. Ahmed and Salam K. Khamas
Electronics 2025, 14(17), 3565; https://doi.org/10.3390/electronics14173565 (registering DOI) - 8 Sep 2025
Abstract
This paper presents a novel compact 4 × 4 Butler matrix (BM) employing a quasi-twisted branch line coupler (QBLC) as the unit cell to achieve enhanced bandwidth performance. The proposed BM integrates four QBLCs, a uniquely designed 0 dB crossover, and a 45° [...] Read more.
This paper presents a novel compact 4 × 4 Butler matrix (BM) employing a quasi-twisted branch line coupler (QBLC) as the unit cell to achieve enhanced bandwidth performance. The proposed BM integrates four QBLCs, a uniquely designed 0 dB crossover, and a 45° phase shifter, all fabricated on a double-layer Rogers RO4003C substrate with a thickness of 0.8 mm, dielectric constant (εr) of 3.3, and a loss tangent of 0.0027. A common ground plane is used to separate the layers. Both simulation and experimental results indicate a reflection coefficient of approximately −6.5 dB at the resonant frequency of 6.5 GHz and isolation levels better than −20 dB at all ports. The system achieves output phase differences of ±13°, ±41°, ±61°, ±89°, and ±120° (±10°) at the designated frequencies. The BM occupies a compact area of 13.8 mm × 38.8 mm, achieving a 92.5% size reduction compared to conventional T-shaped BM structures. The design was modeled and simulated using CST Microwave Studio, with a strong correlation observed between simulated and measured results, validating the design’s reliability and effectiveness. Furthermore, the BM’s beamforming performance is evaluated by integrating it with a 1 × 4 microstrip antenna array. The measured return loss at all ports is below −10 dB at 6.5 GHz, and the system successfully achieves switched beam steering toward four distinct angles: −5°, +6°, +26°, −24°, +43, and −43 with antenna gains ranging from 7 to 10 dBi. Full article
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25 pages, 6231 KB  
Review
1,3-Dipolar Cycloaddition of Nitrile Imines and Nitrile Oxides to Exocyclic C=N Bonds—An Approach to Spiro-N-Heterocycles
by Juliana V. Petrova, Maxim E. Kukushkin and Elena K. Beloglazkina
Int. J. Mol. Sci. 2025, 26(17), 8673; https://doi.org/10.3390/ijms26178673 (registering DOI) - 5 Sep 2025
Viewed by 334
Abstract
Nitrile imines and nitrile oxides are capable of undergoing (3+2)-cycloaddition reactions at double and triple carbon–carbon, carbon-heteroatom, or heteroatom–heteroatom bonds of various dipolarophiles, forming five-membered heterocyclic compounds. When cyclic dipolarophiles bearing an exocyclic carbon–nitrogen double bond (exo-C=N) are introduced into the reaction with [...] Read more.
Nitrile imines and nitrile oxides are capable of undergoing (3+2)-cycloaddition reactions at double and triple carbon–carbon, carbon-heteroatom, or heteroatom–heteroatom bonds of various dipolarophiles, forming five-membered heterocyclic compounds. When cyclic dipolarophiles bearing an exocyclic carbon–nitrogen double bond (exo-C=N) are introduced into the reaction with these dipoles, spiro-fused 1,2,4-triazoline or 1,2,4-oxadiazoline cycles are formed. Such reactions can provide efficient synthetic approaches to spiro-heterocyclic compounds with enhanced biological activity. This review comprehensively summarizes the literature data on the 1,3-dipolar cycloaddition of nitrile imines and nitrile oxides to exo-C=N bonds for spiro compound synthesis. The research area covers reactions of both saturated and unsaturated dipolarophiles, monocyclic and polycyclic molecules, as well as compounds containing one to three heteroatoms, with special emphasis on systems containing biologically significant heterocyclic pharmacophores. Recent advances in reaction techniques, such as microwave and ultrasonic activation, as well as one-pot and diffusion protocols, are also mentioned. Full article
(This article belongs to the Section Biochemistry)
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29 pages, 6366 KB  
Article
Integrated Ultra-Wideband Microwave System to Measure Composition Ratio Between Fat and Muscle in Multi-Species Tissue Types
by Lixiao Zhou, Van Doi Truong and Jonghun Yoon
Sensors 2025, 25(17), 5547; https://doi.org/10.3390/s25175547 - 5 Sep 2025
Viewed by 396
Abstract
Accurate and non-invasive assessment of fat and muscle composition is crucial for biomedical monitoring to track health conditions in humans and pets, as well as for classifying meats in the meat industry. This study introduces a cost-effective, multifunctional ultra-wideband microwave system operating from [...] Read more.
Accurate and non-invasive assessment of fat and muscle composition is crucial for biomedical monitoring to track health conditions in humans and pets, as well as for classifying meats in the meat industry. This study introduces a cost-effective, multifunctional ultra-wideband microwave system operating from 2.4 to 4.4 GHz, designed for rapid and non-destructive quantification of fat thickness, muscle thickness, and fat-to-muscle ratio in diverse ex vivo samples, including pork, beef, and oil–water mixtures. The compact handheld device integrates essential RF components such as a frequency synthesizer, directional coupler, logarithmic power detector, and a dual-polarized Vivaldi antenna. Bluetooth telemetry enables seamless real-time data transmission to mobile- or PC-based platforms, with each measurement completed in a few seconds. To enhance signal quality, a two-stage denoising pipeline combining low-pass filtering and Savitzky–Golay smoothing was applied, effectively suppressing noise while preserving key spectral features. Using a random forest regression model trained on resonance frequency and signal-loss features, the system demonstrates high predictive performance even under limited sample conditions. Correlation coefficients for fat thickness, muscle thickness, and fat-to-muscle ratio consistently exceeded 0.90 across all sample types, while mean absolute errors remained below 3.5 mm. The highest prediction accuracy was achieved in homogeneous oil–water samples, whereas biologically complex tissues like pork and beef introduced greater variability, particularly in muscle-related measurements. The proposed microwave system is highlighted as a highly portable and time-efficient solution, with measurements completed within seconds. Its low cost, ability to analyze multiple tissue types using a single device, and non-invasive nature without the need for sample pre-treatment or anesthesia make it well suited for applications in agri-food quality control, point-of-care diagnostics, and broader biomedical fields. Full article
(This article belongs to the Section Biomedical Sensors)
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13 pages, 2440 KB  
Article
High-Fidelity Long-Haul Microwave Photonic Links with Composite OPLLs and Multi-Core Fiber for Secure Command and Control Systems in Contested Environments
by Yuanshuo Bai, Zhaochen Zhang, Weilin Xie, Yang Li, Teng Tian, Dachuan Yuan and Haokai Shen
Photonics 2025, 12(9), 893; https://doi.org/10.3390/photonics12090893 - 5 Sep 2025
Viewed by 184
Abstract
Secure communication for critical command nodes has emerged as a pivotal challenge in modern warfare, in particular considering the vulnerability of these nodes to electronic reconnaissance. To cope with the severe interference, this paper proposes a robust solution for long-distance secure command and [...] Read more.
Secure communication for critical command nodes has emerged as a pivotal challenge in modern warfare, in particular considering the vulnerability of these nodes to electronic reconnaissance. To cope with the severe interference, this paper proposes a robust solution for long-distance secure command and control system leveraging phase-modulated microwave photonic links. Studies that analyze the impairing nonlinear distortions and phase noise stemming from different sources in optical phase demodulation during long-haul transmission has been carried out, unveiling their impairment in coherent transmission systems. To overcome these limitations, a linearized phase demodulation and noise suppression technique based on composite optical phase-locked loop and multi-core fiber is proposed and experimentally validated. Experimental results demonstrate a long-haul transmission over 100 km with an 81 dB suppression for third-order intermodulation distortion and a 27 dB improvement in noise floor at 5 MHz under closed-loop condition, verifying a significant enhancement in the fidelity in long-distance transmission. This method ensures a highly reliable secure communication for command and control systems in contested electromagnetic environments. Full article
(This article belongs to the Special Issue Photodetectors for Next-Generation Imaging and Sensing Systems)
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18 pages, 4130 KB  
Article
Cu9S5/Gel-Derived TiO2 Composites for Efficient CO2 Adsorption and Conversion
by Shuai Liu, Yang Meng, Zhengfei Chen, Jiefeng Yan, Fuyan Gao, Tao Wu and Guangsuo Yu
Gels 2025, 11(9), 711; https://doi.org/10.3390/gels11090711 - 4 Sep 2025
Viewed by 188
Abstract
Engineering phase-selective gel composites presents a promising route to enhance both CO2 adsorption and conversion efficiency in photocatalytic systems. In this work, Cu9S5/TiO2 gel composites were synthesized via a hydrazine-hydrate-assisted hydrothermal method, using TiO2 derived from [...] Read more.
Engineering phase-selective gel composites presents a promising route to enhance both CO2 adsorption and conversion efficiency in photocatalytic systems. In this work, Cu9S5/TiO2 gel composites were synthesized via a hydrazine-hydrate-assisted hydrothermal method, using TiO2 derived from a microwave-assisted sol–gel process. The resulting materials exhibit a porous gel-derived morphology with highly dispersed Cu9S5 nanocrystals, as confirmed by XRD, TEM, and XPS analyses. These structural features promote abundant surface-active sites and interfacial contact, enabling efficient CO2 adsorption. Among all samples, the optimized 0.36Cu9S5/TiO2 composite achieved a methane production rate of 34 μmol·g−1·h−1, with 64.76% CH4 selectivity and 88.02% electron-based selectivity, significantly outperforming Cu9S8/TiO2 synthesized without hydrazine hydrate. This enhancement is attributed to the dual role of hydrazine: facilitating phase transformation from Cu9S8 to Cu9S5 and modulating the interfacial electronic environment to favor CO2 capture and activation. DFT calculations reveal that Cu9S5/TiO2 effectively lowers the energy barriers of critical intermediates (*COOH, *CO, and *CHO), enhancing both CO2 adsorption strength and subsequent conversion to methane. This work demonstrates a gel-derived composite strategy that couples efficient CO2 adsorption with selective photocatalytic reduction, offering new design principles for adsorption–conversion hybrid materials. Full article
(This article belongs to the Special Issue Gels for Removal and Adsorption (3rd Edition))
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29 pages, 9470 KB  
Review
Millimeter-Wave Antennas for 5G Wireless Communications: Technologies, Challenges, and Future Trends
by Yutao Yang, Minmin Mao, Junran Xu, Huan Liu, Jianhua Wang and Kaixin Song
Sensors 2025, 25(17), 5424; https://doi.org/10.3390/s25175424 - 2 Sep 2025
Viewed by 486
Abstract
With the rapid evolution of 5G wireless communications, millimeter-wave (mmWave) technology has become a crucial enabler for high-speed, low-latency, and large-scale connectivity. As the critical interface for signal transmission, mmWave antennas directly affect system performance, reliability, and application scope. This paper reviews the [...] Read more.
With the rapid evolution of 5G wireless communications, millimeter-wave (mmWave) technology has become a crucial enabler for high-speed, low-latency, and large-scale connectivity. As the critical interface for signal transmission, mmWave antennas directly affect system performance, reliability, and application scope. This paper reviews the current state of mmWave antenna technologies in 5G systems, focusing on antenna types, design considerations, and integration strategies. We discuss how the multiple-input multiple-output (MIMO) architectures and advanced beamforming techniques enhance system capacity and link robustness. State-of-the-art integration methods, such as antenna-in-package (AiP) and chip-level integration, are examined for their importance in achieving compact and high-performance mmWave systems. Material selection and fabrication technologies—including low-loss substrates like polytetrafluoroethylene (PTFE), hydrocarbon-based materials, liquid crystal polymer (LCP), and microwave dielectric ceramics, as well as emerging processes such as low-temperature co-fired ceramics (LTCC), 3D printing, and micro-electro-mechanical systems (MEMS)—are also analyzed. Key challenges include propagation path limitations, power consumption and thermal management in highly integrated systems, cost–performance trade-offs for mass production, and interoperability standardization across vendors. Finally, we outline future research directions, including intelligent beam management, reconfigurable antennas, AI-driven designs, and hybrid mmWave–sub-6 GHz systems, highlighting the vital role of mmWave antennas in shaping next-generation wireless networks. Full article
(This article belongs to the Special Issue Millimeter-Wave Antennas for 5G)
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22 pages, 7574 KB  
Article
Multiscale Evaluation and Error Characterization of HY-2B Fused Sea Surface Temperature Data
by Xiaomin Chang, Lei Ji, Guangyu Zuo, Yuchen Wang, Siyu Ma and Yinke Dou
Remote Sens. 2025, 17(17), 3043; https://doi.org/10.3390/rs17173043 - 1 Sep 2025
Viewed by 452
Abstract
The Haiyang-2B (HY-2B) satellite, launched on 25 October 2018, carries both active and passive microwave sensors, including a scanning microwave Radiometer (SMR), to deliver high-precision, all-weather global observations. Sea surface temperature (SST) is among its key products. We evaluated the HY-2B SMR Level-4A [...] Read more.
The Haiyang-2B (HY-2B) satellite, launched on 25 October 2018, carries both active and passive microwave sensors, including a scanning microwave Radiometer (SMR), to deliver high-precision, all-weather global observations. Sea surface temperature (SST) is among its key products. We evaluated the HY-2B SMR Level-4A (L4A) SST (25 km resolution) over the North Pacific (0–60°N, 120°E–100°W) for the period 1 October 2023 to 31 March 2025 using the extended triple collocation (ETC) and dual-pairing methods. These comparisons were made against the Remote Sensing System (RSS) microwave and infrared (MWIR) fused SST product and the National Oceanic and Atmospheric Administration (NOAA) in situ SST Quality Monitor (iQuam) observations. Relative to iQuam, HY-2B SST has a mean bias of –0.002 °C and a root mean square error (RMSE) of 0.279 °C. Compared to the MWIR product, the mean bias is 0.009 °C with an RMSE of 0.270 °C, indicating high accuracy. ETC yields an equivalent standard deviation (ESD) of 0.163 °C for HY-2B, compared to 0.157 °C for iQuam and 0.196 °C for MWIR. Platform-specific ESDs are lowest for drifters (0.124 °C) and tropical moored buoys (0.088 °C) and highest for ship and coastal moored buoys (both 0.238 °C). Both the HY-2B and MWIR products exhibit increasing ESD and RMSE toward higher latitudes, primarily driven by stronger winds, higher columnar water vapor, and elevated cloud liquid water. Overall, HY-2B SST performs reliably under most conditions, but incurs larger errors under extreme environments. This analysis provides a robust basis for its application and future refinement. Full article
(This article belongs to the Special Issue Satellite Remote Sensing for Ocean and Coastal Environment Monitoring)
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24 pages, 7930 KB  
Article
Impact of FY-3D MWRI and MWHS-2 Radiance Data Assimilation in WRFDA System on Forecasts of Typhoon Muifa
by Feifei Shen, Jiahao Zhang, Si Cheng, Changchun Pei, Dongmei Xu and Xiaolin Yuan
Remote Sens. 2025, 17(17), 3035; https://doi.org/10.3390/rs17173035 - 1 Sep 2025
Viewed by 555
Abstract
This study investigates the impact of assimilating FY-3D Microwave Radiation Imager (MWRI) radiance data into the Weather Research and Forecasting (WRF) model, utilizing a 3D-Var data assimilation system, on the forecast accuracy of Typhoon Muifa (2022). The research focuses on the selection of [...] Read more.
This study investigates the impact of assimilating FY-3D Microwave Radiation Imager (MWRI) radiance data into the Weather Research and Forecasting (WRF) model, utilizing a 3D-Var data assimilation system, on the forecast accuracy of Typhoon Muifa (2022). The research focuses on the selection of data from different channels, land/ocean coverage, and orbits of the MWRI, along with the synergistic assimilation strategy with MWHS-2 data. Ten assimilation experiments were conducted, starting from 0600 UTC on 14 September 2022, covering a 42 h forecast period. The results show that after assimilating the microwave radiometer data, the brightness temperature deviation in the ocean area was significantly reduced compared to the simulation without data assimilation. This led to an improvement in the accuracy of typhoon track and intensity predictions, particularly for predictions beyond 24 h. Furthermore, the assimilation of land data and single-orbit data (particularly from the western orbit) further enhanced forecast accuracy, while the joint assimilation of MWHS-2 and MWRI data yielded additional error reductions. These findings underscore the potential of satellite data assimilation in improving typhoon forecasting and highlight the need for optimal land observation and channel selection techniques. Full article
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11 pages, 2379 KB  
Proceeding Paper
Comparative Analysis of Modern Robotic Demining Complexes and Development of an Automated Mission Planning Algorithm
by Yerkebulan Nurgizat, Aidos Sultan, Nursultan Zhetenbayev, Abu-Alim Ayazbay, Arman Uzbekbayev, Gani Sergazin and Kuanysh Alipbayev
Eng. Proc. 2025, 104(1), 63; https://doi.org/10.3390/engproc2025104063 - 29 Aug 2025
Viewed by 401
Abstract
This paper presents a comparative analysis of ten state-of-the-art robotic de-mining systems, grouped into (i) sensor-centric platforms for high-precision detection and (ii) rapid mechanical-contact vehicles for clearance. Building on these findings, we propose a lightweight tracked platform (~1.9 T) equipped with a four-channel [...] Read more.
This paper presents a comparative analysis of ten state-of-the-art robotic de-mining systems, grouped into (i) sensor-centric platforms for high-precision detection and (ii) rapid mechanical-contact vehicles for clearance. Building on these findings, we propose a lightweight tracked platform (~1.9 T) equipped with a four-channel sensing suite-RGB/IR camera, 32-layer LiDAR, pulsed-induction metal detector, and 2.45 GHz microwave thermography—integrated in an adaptive Bayesian “detect → confirm → neutralize” loop. The modular end-effector permits either pinpoint mechanical intervention or deployment of a linear charge. Modelling indicates an expected detection sensitivity ≥ 95% with a false-positive rate ≤ 5% in humanitarian demining mode and a clearance throughput above 1.5 ha·h−1 in breaching mode. Ongoing work includes CFD analysis of the thermal front, fabrication of a prototype, and performance testing in accordance with IMAS 10.20. Full article
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71 pages, 6657 KB  
Review
Biomass Pyrolysis Pathways for Renewable Energy and Sustainable Resource Recovery: A Critical Review of Processes, Parameters, and Product Valorization
by Nicoleta Ungureanu, Nicolae-Valentin Vlăduț, Sorin-Ștefan Biriș, Neluș-Evelin Gheorghiță and Mariana Ionescu
Sustainability 2025, 17(17), 7806; https://doi.org/10.3390/su17177806 - 29 Aug 2025
Viewed by 535
Abstract
The increasing demand for renewable energy has intensified research on lignocellulosic biomass pyrolysis as a versatile route for sustainable energy and resource recovery. This study provides a comparative overview of main pyrolysis regimes (slow, intermediate, fast, and flash), emphasizing operational parameters, typical product [...] Read more.
The increasing demand for renewable energy has intensified research on lignocellulosic biomass pyrolysis as a versatile route for sustainable energy and resource recovery. This study provides a comparative overview of main pyrolysis regimes (slow, intermediate, fast, and flash), emphasizing operational parameters, typical product yields, and technological readiness levels (TRLs). Reactor configurations, including fixed-bed, fluidized-bed, rotary kiln, auger, and microwave-assisted systems, are analyzed in terms of design, advantages, limitations, and TRL status. Key process parameters, such as temperature, heating rate, vapor residence time, reaction atmosphere, and catalyst type, critically influence the yields and properties of biochar, bio-oil, and syngas. Increased temperatures and fast heating rates favor liquid and gas production, whereas lower temperatures and longer residence times enhance biochar yield and carbon content. CO2 and H2O atmospheres modify product distribution, with CO2 increasing gas formation and biochar surface area and steam enhancing bio-oil yield at the expense of solid carbon. Catalytic pyrolysis improves selectivity toward target products, though trade-offs exist between char and oil yields depending on feedstock and catalyst choice. These insights underscore the interdependent effects of process parameters and reactor design, highlighting opportunities for optimizing pyrolysis pathways for energy recovery, material valorization, and sustainable bioeconomy applications. Full article
(This article belongs to the Special Issue Sustainable Waste Process Engineering and Biomass Valorization)
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28 pages, 7103 KB  
Article
Dynamic Mode I Fracture Toughness and Damage Mechanism of Dry and Saturated Sandstone Subject to Microwave Radiation
by Pin Wang, Yinqi Lin, Duo Chen and Tubing Yin
Appl. Sci. 2025, 15(17), 9500; https://doi.org/10.3390/app15179500 - 29 Aug 2025
Viewed by 249
Abstract
Microwave-assisted rock fragmentation has been considered as one of the most promising technologies in rock excavation, but due to the fact that excavation is usually carried out in water-rich environments, understanding the dynamic fracture properties of rocks with different water contents after microwave [...] Read more.
Microwave-assisted rock fragmentation has been considered as one of the most promising technologies in rock excavation, but due to the fact that excavation is usually carried out in water-rich environments, understanding the dynamic fracture properties of rocks with different water contents after microwave irradiation is thus desirable. This study employed an enhanced split Hopkinson pressure bar (SHPB) system to perform dynamic fracture tests on pre-cracked semi-circular bending (SCB) specimens. It systematically explores the changes in the mechanical properties of sandstone under both dry and saturated conditions after exposure to 700 W of microwave radiation for 10 min. Infrared thermal imaging was utilized to capture the temperature distribution across the specimens, while digital image correlation (DIC) and high-speed photography were used to simultaneously record the crack propagation process. Based on the principle of energy conservation, the analysis of energy dissipation during fracture was performed, and the micro-damage evolution mechanism of the material was revealed through scanning electron microscopy (SEM). The results demonstrated that saturated sandstone exhibited a more rapid heating response and significantly lower dynamic fracture toughness and fracture energy compared to dry samples after microwave irradiation. These findings indicate that water saturation amplifies the weakening effect induced by microwaves, making the rock more susceptible to low-stress fractures. The underlying damage mechanisms of microwave radiation on water-bearing sandstone were interpreted with the theory of pore water pressure and structural thermal stresses. Full article
(This article belongs to the Special Issue Recent Advances in Rock Mass Engineering)
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24 pages, 7836 KB  
Article
Experimental Investigation into the Law of Rock Breaking Through the Combination of Microwave Irradiation and Cutting Tools Under Multiple Conditions
by Xiang-Xin Su, Zheng-Wei Li, Yang-Yi Zhou and Shi-Ping Li
Buildings 2025, 15(17), 3082; https://doi.org/10.3390/buildings15173082 - 28 Aug 2025
Viewed by 400
Abstract
Microwave irradiation of rocks can reduce the strength of rocks and ease their subsequent excavation. Exploring the combination of microwave and cutting tools for rock breaking under different conditions is important to the practical engineering application of microwaves. Based on a true triaxial [...] Read more.
Microwave irradiation of rocks can reduce the strength of rocks and ease their subsequent excavation. Exploring the combination of microwave and cutting tools for rock breaking under different conditions is important to the practical engineering application of microwaves. Based on a true triaxial microwave-assisted dual-mode mechanical rock-breaking test system, high-power microwave irradiation of rocks was investigated under different true triaxial stresses, durations of microwave irradiation, and cutting tool conditions such as mechanical drilling tools and tunnel boring machine (TBM) hobs. This research provides important data support for improving the rock-breaking efficiency of mine mining and tunneling as well as mechanical cutting tools and TBM hobs. In this experiment, Chifeng basalt with a relatively high strength was adopted as the research object. A 15 kW (2.45-GHz) open high-power microwave device was used to irradiate 200 mm × 200 mm × 200 mm cubic Chifeng basalt samples under conditions of different burial depths, and a cone drill bit was used for staged excavation. After microwave irradiation of Chifeng basalt measuring 400 mm × 400 mm × 400 mm, a 4-inch (102 mm) rotary cutter was employed to conduct round-by-circle cutting and rock-breaking tests in the microwave irradiation area. The results show that under true triaxial stress, the law of rock breaking by microwave irradiation combined with cone drill bits is as follows: the cutting force shows a trend of increasing–decreasing–increasing again–decreasing again. After microwave irradiation combined with hob cutting, the effective range of the influence of the hob is within the third cutting circle, with a range of diameters of approximately 200 mm. The results also indicate that the open microwave device can pre-crack rocks under deep stress, and there is obvious crack propagation. This research has good applicability to microwave-combined cantilever road-headers and TBM as well as in the mining field, and has a promising development prospect. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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28 pages, 3865 KB  
Review
Recent Advances and Future Perspectives on Heat and Mass Transfer Mechanisms Enhanced by Preformed Porous Media in Vacuum Freeze-Drying of Agricultural and Food Products
by Xinkang Hu, Bo Zhang, Xintong Du, Huanhuan Zhang, Tianwen Zhu, Shuang Zhang, Xinyi Yang, Zhenpeng Zhang, Tao Yang, Xu Wang and Chundu Wu
Foods 2025, 14(17), 2966; https://doi.org/10.3390/foods14172966 - 25 Aug 2025
Viewed by 744
Abstract
Preformed porous media (PPM) technology has emerged as a transformative approach to enhance heat and mass transfer in vacuum freeze-drying (VFD) of agricultural and food products. This review systematically analyzes recent advances in PPM research, with particular focus on spray freeze-drying (SFD) as [...] Read more.
Preformed porous media (PPM) technology has emerged as a transformative approach to enhance heat and mass transfer in vacuum freeze-drying (VFD) of agricultural and food products. This review systematically analyzes recent advances in PPM research, with particular focus on spray freeze-drying (SFD) as the dominant technique for precision pore architecture control. Empirical studies confirm PPM’s efficacy: drying time reductions of 20–50% versus conventional VFD while improving product quality (e.g., 15% higher ginsenoside retention in ginseng, 90% enzyme activity preservation). Key innovations include gradient porous structures and multi-technology coupling strategies that fundamentally alter transfer mechanisms through: resistance mitigation via interconnected macropores (50–500 μm, 40–90% porosity), pseudo-convection effects enabling 30% faster vapor removal, and radiation enhancement boosting absorption by 40–60% and penetration depth 2–3 times. While inherent VFD limitations (e.g., low thermal conductivity) persist, we identify PPM-specific bottlenecks: precision regulation of pore structures (<5% size deviation), scalable fabrication of gradient architectures, synergy mechanisms in multi-field coupling (e.g., microwave-PPM interactions). The most promising advancements include 3D-printed gradient pores for customized transfer paths, intelligent monitoring-feedback systems, and multiscale modeling bridging pore-scale physics to macroscale kinetics. This review provides both a critical assessment of current progress and a forward-looking perspective to guide future research and industrial adoption of PPM-enhanced VFD. Full article
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12 pages, 3228 KB  
Communication
Green and Efficient Lithium Extraction from Spent NCM Batteries via Electromagnetic Radiation
by Ling Tong, Gui-Rong Zhang, Da-Shuai Li, Xing-Yu Huang, Yuan-Long Liu and Yan-Qing Cheng
Materials 2025, 18(17), 3975; https://doi.org/10.3390/ma18173975 - 25 Aug 2025
Viewed by 558
Abstract
The conventional recycling of spent lithium-ion batteries (LIBs) is hindered by high energy consumption and severe environmental pollution. In this study, a novel method utilizing high-frequency electromagnetic radiation was proposed to process the black mass derived from spent NCM-LIBs, significantly reducing both energy [...] Read more.
The conventional recycling of spent lithium-ion batteries (LIBs) is hindered by high energy consumption and severe environmental pollution. In this study, a novel method utilizing high-frequency electromagnetic radiation was proposed to process the black mass derived from spent NCM-LIBs, significantly reducing both energy consumption and chemical reagent usage. Conductive carbon black was introduced as an electromagnetic-wave-absorbing additive to improve the electromagnetic energy into thermal energy conversion efficiency during electromagnetic radiation. As a result, the decomposition and reduction of NCM materials can be completed within just 10 min at a microwave power of 500 W. Following electromagnetic irradiation, lithium was efficiently extracted via simple water leaching, achieving an extraction efficiency of 88.24%. Furthermore, a microwave heating device based on traveling-wave propagation was developed. Unlike conventional small-scale microwave systems that employ resonant cavities, this design enables improved heating uniformity, higher efficiency, and greater scalability for industrial microwave-assisted chemical processes. Full article
(This article belongs to the Special Issue Recycling and Electrode Materials of Lithium Batteries)
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