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Search Results (895)

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Keywords = piezoelectric composite

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16 pages, 4083 KB  
Article
Magnetic Field Enhancement of an Electromechanical–Magnetic Antenna for ELF Cross-Medium Communication via a Parallel Configuration
by Chung Ming Leung, He Chen and Menglong Liu
Sensors 2025, 25(20), 6303; https://doi.org/10.3390/s25206303 (registering DOI) - 11 Oct 2025
Abstract
Extremely low-frequency (ELF, 3–30 Hz) signals are effective for cross-medium transmission, yet conventional implementations are hindered by their large size and low efficiency. To address these limitations, a compact electromechanical–magnetic antenna (EMA) was developed and experimentally validated for ELF magnetic communication. The basic [...] Read more.
Extremely low-frequency (ELF, 3–30 Hz) signals are effective for cross-medium transmission, yet conventional implementations are hindered by their large size and low efficiency. To address these limitations, a compact electromechanical–magnetic antenna (EMA) was developed and experimentally validated for ELF magnetic communication. The basic unit of the antenna, a single-EMA, consists of a stacked magnetostrictive composite beam, piezoelectric ceramic plates, and tip-mounted permanent magnets. The total envelope volume of a single EMA is only 3.3 cm3 with a maximum length of 12 cm, representing a substantial reduction compared with conventional ELF antennas. Building on this compact architecture, two EMAs were operated in parallel to form a parallel-EMA system, which significantly enhanced magnetic radiation through constructive magnetic coupling. Moreover, the optimal separation distance between the two EMAs was identified, ensuring efficient cooperative radiation. When driven at 50.2 mW, the parallel-EMA configuration generated a magnetic flux density of 114 pT at a transmission distance of 20 m in seawater. This performance demonstrates nearly a twofold improvement over a single-EMA unit, validating the scalability of parallel operation for stronger magnetic radiation. The compact form factor of the single EMA combined with the enhanced radiation performance of the parallel-EMA system enables portable ELF magnetic communication across diverse cross-medium scenarios, including air-to-sea and underground-to-air links. Full article
(This article belongs to the Section Electronic Sensors)
20 pages, 14967 KB  
Article
Discrete-Time Linear Quadratic Optimal Tracking Control of Piezoelectric Actuators Based on Hammerstein Model
by Dongmei Liu, Xiguo Zhao, Xuan Li, Changchun Wang, Li Tan, Xuejun Li and Shuyou Yu
Processes 2025, 13(10), 3212; https://doi.org/10.3390/pr13103212 - 9 Oct 2025
Viewed by 101
Abstract
To address the issue of hysteresis nonlinearity adversely affecting the tracking accuracy of piezoelectric actuators, an improved particle swarm optimization (PSO) algorithm is proposed to improve the accuracy of hysteresis model parameter identification. Additionally, a discrete-time linear quadratic optimal tracking (DLQT) control strategy [...] Read more.
To address the issue of hysteresis nonlinearity adversely affecting the tracking accuracy of piezoelectric actuators, an improved particle swarm optimization (PSO) algorithm is proposed to improve the accuracy of hysteresis model parameter identification. Additionally, a discrete-time linear quadratic optimal tracking (DLQT) control strategy incorporating hysteresis compensation is developed to improve tracking performance. This study employs the Hammerstein model to characterize the nonlinear hysteresis behavior of piezoelectric actuators. Regarding parameter identification, the conventional PSO algorithm tends to suffer from premature convergence and being trapped in local optima. To address this, a cross-variation mechanism is introduced to enhance population diversity and improve global search ability. Furthermore, adaptive and dynamically adjustable inertia weights are designed based on evolutionary factors to balance exploration and exploitation, thereby enhancing convergence and identification accuracy. The inertia weights and learning factors are adaptively adjusted based on the evolutionary factor to balance local and global search capabilities and accelerate convergence. Benchmark function tests and model identification experiments demonstrate the improved algorithm’s superior convergence speed and accuracy. In terms of control strategy, a hysteresis compensator based on an asymmetric hysteresis model is designed to improve system linearity. To address the issues of incomplete hysteresis compensation and low tracking accuracy, a DLQT controller is developed based on hysteresis compensation. Hardware-in-the-loop tracking control experiments using single and composite frequency reference signals show that the relative error is below 3.3% in the no-load case and below 4.5% in the loaded case. Compared with the baseline method, the proposed control strategy achieves lower root-mean-square error and maximum steady-state error, demonstrating its effectiveness. Full article
(This article belongs to the Section Process Control and Monitoring)
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15 pages, 5011 KB  
Article
Research on Ultrasonic Focusing Stacked Transducers for Composite
by Yi Bo, Jie Li, Shunmin Yang, Chenju Zhou and Yutao Tian
Sensors 2025, 25(19), 6179; https://doi.org/10.3390/s25196179 - 6 Oct 2025
Viewed by 295
Abstract
Most existing carbon fiber composite materials are formed by high-temperature molding of multiple layers of fiber cloth. During the manufacturing and usage processes, materials are prone to defects such as voids, delamination, and inclusions, which seriously threaten their service life and safety performance. [...] Read more.
Most existing carbon fiber composite materials are formed by high-temperature molding of multiple layers of fiber cloth. During the manufacturing and usage processes, materials are prone to defects such as voids, delamination, and inclusions, which seriously threaten their service life and safety performance. Ultrasonic testing is currently a widely adopted method for detecting defects in carbon fiber composite materials. However, existing narrow-pulse ultrasonic transducers often have to sacrifice emission energy to achieve narrow-pulse emission, which results in their limited ability to penetrate thicker carbon fiber composite materials. To address this issue, this paper proposes the design of a focused laminated transducer. By stacking and bonding lead titanate piezoelectric wafers and using a concave lens made of organic glass to focus ultrasonic waves, the emission sound intensity of the ultrasonic transducer is enhanced. The simulation results show that the designed focused double-stack transducer has a directivity gain that is 4.49 dB higher than that of the traditional single-piezoelectric-wafer transducer. The transducer fabricated based on this design has successfully achieved effective detection of internal defects in carbon fiber composite materials. Full article
(This article belongs to the Section Fault Diagnosis & Sensors)
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21 pages, 2596 KB  
Article
Self-Energy-Harvesting Pacemakers: An Example of Symbiotic Synthetic Biology
by Kuntal Kumar Das, Ashutosh Kumar Dubey, Bikramjit Basu and Yogendra Narain Srivastava
SynBio 2025, 3(4), 15; https://doi.org/10.3390/synbio3040015 - 4 Oct 2025
Viewed by 172
Abstract
While synthetic biology has traditionally focused on creating biological systems often through genetic engineering, emerging technologies, for example, implantable pacemakers with integrated piezo-electric and tribo-electric materials are beginning to enlarge the classical domain into what we call symbiotic synthetic biology. These devices are [...] Read more.
While synthetic biology has traditionally focused on creating biological systems often through genetic engineering, emerging technologies, for example, implantable pacemakers with integrated piezo-electric and tribo-electric materials are beginning to enlarge the classical domain into what we call symbiotic synthetic biology. These devices are permanently attached to a body, although non-living or genetically unaltered, and closely mimic biological behavior by harvesting biomechanical energy and providing functions, such as autonomous heart pacing. They form active interfaces with human tissues and operate as hybrid systems, similar to synthetic organs. In this context, the present paper first presents a short summary of previous in vivo studies on piezo-electric composites in relation to their deployment as battery-less pacemakers. This is then followed by a summary of a recent theoretical work using a damped harmonic resonance model, which is being extended to mimic the functioning of such devices. We then extend the theoretical study further to include new solutions and obtain a sum rule for the power output per cycle in such systems. In closing, we present our quantitative understanding to explore the modulation of the quantum vacuum energy (Casimir effect) by periodic body movements to power pacemakers. Taken together, the present work provides the scientific foundation of the next generation bio-integrated intelligent implementation. Full article
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29 pages, 1062 KB  
Review
Cost-Effectiveness of Structural Health Monitoring in Aviation: A Literature Review
by Pietro Ballarin, Giuseppe Sala and Alessandro Airoldi
Sensors 2025, 25(19), 6146; https://doi.org/10.3390/s25196146 - 4 Oct 2025
Viewed by 467
Abstract
(1) Background: Structural Health Monitoring Systems (SHMSs) can reduce maintenance costs and aircraft downtime. However, their economic impact remains underexplored, particularly in cost–benefit terms. (2) Methods: This study conducted a targeted literature review on all the existing studies consisting of seventeen economic analyses [...] Read more.
(1) Background: Structural Health Monitoring Systems (SHMSs) can reduce maintenance costs and aircraft downtime. However, their economic impact remains underexplored, particularly in cost–benefit terms. (2) Methods: This study conducted a targeted literature review on all the existing studies consisting of seventeen economic analyses of SHMS applications. Key features—such as SHMS type, structural material, vehicle type, integration stage, and cost elements—were classified to identify prevailing trends and gaps. (3) Results: The analysis revealed a predominance of piezoelectric-based SHMS applied to metallic fixed-wing aircraft, with limited attention to composite structures and e-VTOLs. Most studies focused on maintenance phase impacts, overlooking integration costs during manufacturing. Potential benefits like operational life extension, prognostic capabilities, and safety margin reduction were rarely explored, while critical drawbacks such as detection performance, reliability, and power consumption were underrepresented. Maintenance and fuel costs were the most frequently considered economic drivers; downtime costs were often neglected. (4) Conclusions: Although the majority of reviewed studies suggest a positive economic impact from SHMS implementation, significant gaps remain. Future research should address SHMS reliability, integration during early design stages, and applications to emerging aircraft like e-VTOLs to fully realize SHMS economic advantages. Full article
(This article belongs to the Special Issue Sensors—Integrating Composite Materials in Aerospace Applications)
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20 pages, 2923 KB  
Article
Synthesis and Integration of an Fe(II) Coordination Compound into Green Resin Matrices for Multifunctional Dielectric, Piezoelectric, Energy Harvesting, and Storage Applications
by Anastasios C. Patsidis, Ioanna Th. Papageorgiou and Zoi G. Lada
Polymers 2025, 17(18), 2509; https://doi.org/10.3390/polym17182509 - 17 Sep 2025
Viewed by 419
Abstract
Polymer-based hybrid composites have emerged as promising platforms for multifunctional energy applications, combining structural versatility with tunable dielectric behavior. In this study, synthesized [Fe(bpy)3]SO4; (tris(2,2′-bipyridine)iron(II) sulfate) coordination compound was incorporated into a green epoxy resin matrix to fabricate nanocomposites [...] Read more.
Polymer-based hybrid composites have emerged as promising platforms for multifunctional energy applications, combining structural versatility with tunable dielectric behavior. In this study, synthesized [Fe(bpy)3]SO4; (tris(2,2′-bipyridine)iron(II) sulfate) coordination compound was incorporated into a green epoxy resin matrix to fabricate nanocomposites aimed at enhancing dielectric permittivity (ε′), piezoelectric coefficient (d33, pC/N), energy-storage efficiency (nrel, %), and mechanical strength (σ, MPa). The integration of the Fe(II) complex via Scanning Electron Microscopy (SEM) confirmed a homogeneous dispersion within the matrix. Broadband Dielectric Spectroscopy (BDS) revealed the presence of three relaxation processes in the spectra of the tested systems, demonstrating enhanced dielectric permittivity with increasing Fe(II) content. Under progressively shorter relaxation times (τ, s), key processes such as interfacial polarization, the polymer matrix’s transition from a glassy to a rubbery state, and the dynamic reorganization of polar side groups along the polymer backbone are activated. The ability to store and retrieve electric energy was confirmed by varying filler content under direct current (dc) conditions. The nanocomposite with 10 phr (mass parts/100 mass parts of resin) filler achieved a piezoelectric coefficient of d33 = 5.1 pC/N, an energy-storage efficiency of nrel = 44%, and a tensile strength of σ = 55.5 MPa, all of which surpass values reported for conventional epoxy-based composites. These results confirm the ability of the system to store and retrieve electric energy under direct current (dc) fields, while maintaining mechanical robustness and thermal stability due to synergistic interactions between the epoxy matrix and the Fe(II) complex. The multifunctional behavior of the composites underscores their potential as advanced materials for integrated dielectric, piezoelectric, and energy storage and harvesting applications. Full article
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28 pages, 6245 KB  
Article
Time Response of Delaminated Active Sensory Composite Beams Assuming Non-Linear Interfacial Effects
by Nikolaos A. Chrysochoidis, Christoforos S. Rekatsinas and Dimitris A. Saravanos
J. Compos. Sci. 2025, 9(9), 500; https://doi.org/10.3390/jcs9090500 - 15 Sep 2025
Viewed by 377
Abstract
A layerwise laminate FE model capable of predicting the dynamic response of delaminated composite beams with piezoelectric actuators and sensors encompassing local non-linear contact and sliding at the delamination interfaces was formulated. The kinematic assumptions of the layerwise model enabled the representation of [...] Read more.
A layerwise laminate FE model capable of predicting the dynamic response of delaminated composite beams with piezoelectric actuators and sensors encompassing local non-linear contact and sliding at the delamination interfaces was formulated. The kinematic assumptions of the layerwise model enabled the representation of opening and sliding of delamination interfaces as generalized strains, thereby allowing the introduction of interfacial contact and sliding effects through constitutive relations at the interface. This realistic FE model, assisted by representative experiments, was used to study the time response of delaminated active sensory composite beams with predefined delamination extents. The time response was measured and simulated for narrowband actuation signals at two distinct frequency levels using a surface-bonded piezoceramic actuator, while signal acquisition was performed with a piezopolymer sensor. Four different composite specimens, each containing a different delamination size, were used for this study. Experimental results were directly compared with model predictions to evaluate the performance of the proposed analytical approach. Damage signatures were identified in both the signal amplitude and the time of flight, and the sensitivity to delamination size was examined. Finally, the distributions of axial and interlaminar stresses at various time snapshots of the transient analysis are presented, along with contour plots across the structure’s thickness, which illustrate the delamination location and wave propagation patterns. Full article
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17 pages, 3646 KB  
Article
Piezoelectric Cement Composites Enhanced by Triply Periodic Minimal Surface Architectures
by Hu Xu, Hongliang Li, Xuyang Chen, Zheng Zeng and Annan Jiang
Appl. Sci. 2025, 15(18), 9991; https://doi.org/10.3390/app15189991 - 12 Sep 2025
Viewed by 339
Abstract
This study systematically investigates the piezoelectric performance of cement-based composite materials integrated with triply periodic minimal surface (TPMS) piezoelectric ceramic architectures, including Schwarz P and Neovius structures, in comparison with conventional 0–3 and 1–3 connectivity models. Under mechanical loading conditions, finite element analysis [...] Read more.
This study systematically investigates the piezoelectric performance of cement-based composite materials integrated with triply periodic minimal surface (TPMS) piezoelectric ceramic architectures, including Schwarz P and Neovius structures, in comparison with conventional 0–3 and 1–3 connectivity models. Under mechanical loading conditions, finite element analysis was employed to evaluate the average piezoelectric coefficients, voltage coefficients, and potential outputs of composites with varying piezoelectric ceramic volume fractions. Key findings reveal that the Neovius structure exhibits superior performance: at a 20% ceramic volume fraction, its average piezoelectric coefficient reaches 116 pC/N under 15 kN loading, surpassing the 0–3 type by approximately 12-fold. Both Schwarz P and Neovius structures demonstrate approximately 12× higher average piezoelectric coefficients than the 0–3 model, attributed to their continuous charge transfer pathways and efficient stress distribution enabled by TPMS geometry. Additionally, the piezoelectric voltage coefficients of TPMS-based composites significantly exceed those of traditional 1–3 and 0–3 structures. The potential generation capacity of Neovius composites peaks at 6.7 V under high loading, highlighting their superiority in charge accumulation. The results underscore the critical role of piezoelectric ceramic architecture: the bicontinuous TPMS configurations mitigate phase discontinuity issues, enhancing both mechanical–electrical coupling and energy conversion efficiency. This study provides a novel framework for optimizing cement-based piezoelectric composites toward applications in structural health monitoring, energy harvesting, and smart infrastructure. Full article
(This article belongs to the Section Materials Science and Engineering)
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35 pages, 3619 KB  
Review
Research Progress on the Preparation, Modification, and Applications of g-C3N4 in Photocatalysis and Piezoelectric Photocatalysis
by Mengyang Li, Liuqing Yang, Yizhe Song, Hongru Hou, Yujie Fang, Yucheng Liu, Lihao Xie and Dingze Lu
Inorganics 2025, 13(9), 300; https://doi.org/10.3390/inorganics13090300 - 5 Sep 2025
Viewed by 871
Abstract
The metal-free polymeric semiconductor graphitic carbon nitride (g-C3N4) has emerged as a promising material for photocatalytic applications due to its responsiveness to visible light, adjustable electronic structure, and stability. This review systematically summarizes recent advances in preparation strategies, including [...] Read more.
The metal-free polymeric semiconductor graphitic carbon nitride (g-C3N4) has emerged as a promising material for photocatalytic applications due to its responsiveness to visible light, adjustable electronic structure, and stability. This review systematically summarizes recent advances in preparation strategies, including thermal polycondensation, solvothermal synthesis, and template methods. Additionally, it discusses modification approaches such as heterojunction construction, elemental doping, defect engineering, morphology control, and cocatalyst loading. Furthermore, it explores the diverse applications of g-C3N4-based materials in photocatalysis, including hydrogen (H2) evolution, carbon dioxide (CO2) reduction, pollutant degradation, and the emerging field of piezoelectric photocatalysis. Particular attention is given to g-C3N4 composites that are rationally designed to enhance charge separation and light utilization. Additionally, the synergistic mechanism of photo–piezocatalysis is examined, wherein a mechanically induced piezoelectric field facilitates carrier separation and surface reactions. Despite significant advancements, challenges persist, including limited visible-light absorption, scalability issues, and uncertainties in the multi-field coupling mechanisms. The aim of this review is to provide guidelines for future research that may lead to the development of high-performance and energy-efficient catalytic systems in the context of environmental and energy applications. Full article
(This article belongs to the Special Issue Featured Papers in Inorganic Materials 2025)
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11 pages, 1944 KB  
Article
Dual-Mode Flexible Pressure Sensor Based on Ionic Electronic and Piezoelectric Coupling Mechanism Enables Dynamic and Static Full-Domain Stress Response
by Yue Ouyang, Shunqiang Huang, Zekai Huang, Shengyu Wu, Xin Wang, Sheng Chen, Haiyan Zhang, Zhuoqing Yang, Mengran Liu and Libo Gao
Micromachines 2025, 16(9), 1018; https://doi.org/10.3390/mi16091018 - 3 Sep 2025
Viewed by 848
Abstract
Flexible pressure sensors have shown promise applications in scenarios such as robotic tactile sensing due to their excellent sensitivity and linearity. However, the realization of flexible pressure sensors with both static and dynamic response capabilities still face significant challenges due to the properties [...] Read more.
Flexible pressure sensors have shown promise applications in scenarios such as robotic tactile sensing due to their excellent sensitivity and linearity. However, the realization of flexible pressure sensors with both static and dynamic response capabilities still face significant challenges due to the properties of the sensing materials themselves. In this study, we propose a flexible pressure sensor that integrates piezoelectric and ionic capacitance mechanisms for full-domain response detection of dynamic and static forces: a “sandwich” sensing structure is constructed by printing a mixture of multi-walled carbon nanotubes (MWCNTs) onto the surface of the upper and lower electrodes, and sandwiching a polyvinylidene fluoride (PVDF) thin film between the electrodes. The device exhibits a sensitivity of 0.13 kPa−1 in the pressure range of 0–150 kPa. The sensor has a rapid dynamic response (response time 19 ms/12 ms) with a sensitivity of 0.49 mV kPa−1 based on the piezoelectric mechanism and a linearity of 0.9981 based on the ionic capacitance mechanism. The device maintains good response stability under the ball impact test, further validating its potential application in static/dynamic composite force monitoring scenarios. Full article
(This article belongs to the Special Issue Flexible and Wearable Sensors, 4th Edition)
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20 pages, 1598 KB  
Article
Transient Response of Fine-Grained Piezoelectric Coating Composite Structures with a Griffith-Type Interface Crack Under Thermal Impact Loading
by Shuaishuai Hu and Junlin Li
Coatings 2025, 15(9), 1000; https://doi.org/10.3390/coatings15091000 - 29 Aug 2025
Viewed by 450
Abstract
Transient behavior of a Griffith interface crack in fine-grained piezoelectric coating/substrate under thermal impact loading conditions is investigated. It is assumed that the crack faces are thermally and electrically insulated. By employing Fourie–Laplace integral transforms as well as the additivity of solutions, the [...] Read more.
Transient behavior of a Griffith interface crack in fine-grained piezoelectric coating/substrate under thermal impact loading conditions is investigated. It is assumed that the crack faces are thermally and electrically insulated. By employing Fourie–Laplace integral transforms as well as the additivity of solutions, the theoretical expressions for the temperature field, displacement field, and electric field are constructed, thereby deriving specific expressions for the dynamic intensity factors of thermal stress and electric displacement. The boundary-value problem is reduced to singular integral equations solved numerically. Parametric studies quantify time-dependent effects of the coating elastic modulus, thickness, and crack length on dynamic responses. Numerical analyses demonstrate that variations in the elastic modulus ratio and coating thickness induce varied increases or decreases in peak dynamic stress intensity factor. Optimizing coating thickness and elastic modulus significantly enhances structural safety under thermal impact loading. Full article
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16 pages, 7082 KB  
Article
Ultrasound-Responsive Drug Delivery System Based on Piezoelectric Catalytic Mechanisms
by Kaixi Cui, Tianzheng Li, Yifei Ma, Chuanjin Zhang, Ke Zhang, Chao Qi and Kaiyong Cai
J. Funct. Biomater. 2025, 16(8), 304; https://doi.org/10.3390/jfb16080304 - 21 Aug 2025
Cited by 1 | Viewed by 1138
Abstract
Ultrasound-responsive nanomaterials represent a promising approach for achieving non-invasive and localized drug delivery within tumor microenvironments. In this study, we developed a piezocatalysis-assisted hydrogel system that integrates reactive oxygen species (ROS) generation with stimulus-responsive drug release. The platform combines piezoelectric barium titanate (BTO) [...] Read more.
Ultrasound-responsive nanomaterials represent a promising approach for achieving non-invasive and localized drug delivery within tumor microenvironments. In this study, we developed a piezocatalysis-assisted hydrogel system that integrates reactive oxygen species (ROS) generation with stimulus-responsive drug release. The platform combines piezoelectric barium titanate (BTO) nanoparticles with a ROS-sensitive hydrogel matrix, forming an ultrasound-activated dual-function therapeutic system. Upon ultrasound irradiation, the BTO nanoparticles generate ROS—predominantly hydroxyl radicals (OH) and singlet oxygen (1O2)—through the piezoelectric effect, which triggers hydrogel degradation and facilitates the controlled release of encapsulated therapeutic agents. The composition and kinetics of ROS generation were evaluated using radical scavenging assays and fluorescence probe techniques, while the drug release behavior was validated under simulated oxidative environments and acoustic fields. Structural and compositional characterizations (TEM, XRD, and XPS) confirmed the quality and stability of the nanoparticles, and cytocompatibility was assessed using 3T3 fibroblasts. This synergistic strategy, combining piezocatalytic ROS generation with hydrogel disintegration, demonstrates a feasible approach for designing responsive nanoplatforms in ultrasound-mediated drug delivery systems. Full article
(This article belongs to the Special Issue Biomaterials for Drug Delivery and Cancer Therapy)
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21 pages, 4127 KB  
Article
Riboflavin as a Dual-Function Additive for Enhancing Biodegradation in Piezoelectric PLA/BT Composites
by Natalia Puszczykowska, Piotr Rytlewski, Agnieszka Mirkowska, Paweł Cyprys, Piotr Augustyn and Kacper Fiedurek
Materials 2025, 18(16), 3860; https://doi.org/10.3390/ma18163860 - 18 Aug 2025
Viewed by 569
Abstract
Poly(lactic acid)/barium titanate (PLA/BT) composites exhibit piezoelectric properties desirable for bone tissue engineering, but their low biodegradability limits implant resorption. In this study, riboflavin (RF) is introduced as a dual-function additive that enhances biodegradation in PLA/BT composites. Its addition led to significantly increased [...] Read more.
Poly(lactic acid)/barium titanate (PLA/BT) composites exhibit piezoelectric properties desirable for bone tissue engineering, but their low biodegradability limits implant resorption. In this study, riboflavin (RF) is introduced as a dual-function additive that enhances biodegradation in PLA/BT composites. Its addition led to significantly increased microbial colonization and a five-fold higher mass loss compared to unmodified samples. These observations are consistent with the known polarity of RF and its role as a cofactor in microbial metabolism. The PLA/BT/RF composites are subjected to full characterization, including thermogravimetric analysis (TG), differential scanning calorimetry (DSC), tensile testing, dynamic mechanical analysis (DMA), dielectric permittivity measurements, and determination of piezoelectric coefficient d33. Compared to PLA/BT, RF-containing composites exhibit significantly accelerated biodegradation, with mass loss reaching up to 16% after 28 days, while maintaining functional piezoelectricity (d33 ≈ 3.9 pC/N). Scanning electron microscopy (SEM) performed after biodegradation reveals intensified microbial colonization and surface deterioration in the RF-modified samples. The data confirm that riboflavin serves as an effective modifier, enabling controlled biodegradation without compromising electromechanical performance. These results support the use of PLA-based piezoelectric composites for resorbable biomedical implants. Full article
(This article belongs to the Section Advanced Composites)
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22 pages, 2499 KB  
Article
Low-Power Vibrothermography for Detecting Barely Visible Impact Damage in CFRP Laminates: A Comparative Imaging Study
by Zulham Hidayat, Muhammet Ebubekir Torbali, Nicolas P. Avdelidis and Henrique Fernandes
Appl. Sci. 2025, 15(15), 8514; https://doi.org/10.3390/app15158514 - 31 Jul 2025
Cited by 1 | Viewed by 466
Abstract
This study explores the application of low-power vibrothermography (LVT) for detecting barely visible impact damage (BVID) in carbon fibre-reinforced polymer (CFRP) laminates. Composite specimens with varying impact energies (2.5–20 J) were excited using a single piezoelectric transducer with a nominal centre frequency of [...] Read more.
This study explores the application of low-power vibrothermography (LVT) for detecting barely visible impact damage (BVID) in carbon fibre-reinforced polymer (CFRP) laminates. Composite specimens with varying impact energies (2.5–20 J) were excited using a single piezoelectric transducer with a nominal centre frequency of 28 kHz, operated at a fixed excitation frequency of 28 kHz. Thermal data were captured using an infrared camera. To enhance defect visibility and suppress background noise, the raw thermal sequences were processed using principal component analysis (PCA) and robust principal component analysis (RPCA). In LVT, RPCA and PCA provided comparable signal-to-noise ratios (SNR), with no consistent advantage for either method across all cases. In contrast, for pulsed thermography (PT) data, RPCA consistently resulted in higher SNR values, except for one sample. The LVT results were further validated by comparison with PT and phased array ultrasonic testing (PAUT) data to confirm the location and shape of detected damage. These findings demonstrate that LVT, when combined with PCA or RPCA, offers a reliable method for identifying BVID and can support safer, more efficient structural health monitoring of composite materials. Full article
(This article belongs to the Special Issue Application of Acoustics as a Structural Health Monitoring Technology)
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29 pages, 14906 KB  
Article
Hydrothermal Engineering of Ferroelectric PZT Thin Films Tailoring Electrical and Ferroelectric Properties via TiO2 and SrTiO3 Interlayers for Advanced MEMS
by Chun-Lin Li and Guo-Hua Feng
Micromachines 2025, 16(8), 879; https://doi.org/10.3390/mi16080879 - 29 Jul 2025
Viewed by 727
Abstract
This work presents an innovative hydrothermal approach for fabricating flexible piezoelectric PZT thin films on 20 μm titanium foil substrates using TiO2 and SrTiO3 (STO) interlayers. Three heterostructures (Ti/PZT, Ti/TiO2/PZT, and Ti/TiO2/STO/PZT) were synthesized to enable low-temperature [...] Read more.
This work presents an innovative hydrothermal approach for fabricating flexible piezoelectric PZT thin films on 20 μm titanium foil substrates using TiO2 and SrTiO3 (STO) interlayers. Three heterostructures (Ti/PZT, Ti/TiO2/PZT, and Ti/TiO2/STO/PZT) were synthesized to enable low-temperature growth and improve ferroelectric performance for advanced flexible MEMS. Characterizations including XRD, PFM, and P–E loop analysis evaluated crystallinity, piezoelectric coefficient d33, and polarization behavior. The results demonstrate that the multilayered Ti/TiO2/STO/PZT structure significantly enhances performance. XRD confirmed the STO buffer layer effectively reduces lattice mismatch with PZT to ~0.76%, promoting stable morphotropic phase boundary (MPB) composition formation. This optimized film exhibited superior piezoelectric and ferroelectric properties, with a high d33 of 113.42 pm/V, representing an ~8.65% increase over unbuffered Ti/PZT samples, and displayed more uniform domain behavior in PFM imaging. Impedance spectroscopy showed the lowest minimum impedance of 8.96 Ω at 10.19 MHz, indicating strong electromechanical coupling. Furthermore, I–V measurements demonstrated significantly suppressed leakage currents in the STO-buffered samples, with current levels ranging from 10−12 A to 10−9 A over ±3 V. This structure also showed excellent fatigue endurance through one million electrical cycles, confirming its mechanical and electrical stability. These findings highlight the potential of this hydrothermally engineered flexible heterostructure for high-performance actuators and sensors in advanced MEMS applications. Full article
(This article belongs to the Special Issue Manufacturing and Application of Advanced Thin-Film-Based Device)
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