Search Results (148)

To increase wear resistance, (Zr,Nb)N, ZrN and (Zr,Hf)N coatings with columnar structures and (Zr,Ti)N and (Zr,Nb,Hf)N coatings with nanolayer structures were deposited on an AISI 321 stainless steel substrate. The samples with (Zr,Nb)N and ZrN coatings exhibited the best resistance to failure in the scratch test. The sample with the (Zr,Nb)N coating had the best wear resistance for the first 16,000 s. However, eventually the wear of this sample became notable, and after 20,000 s of testing, the lowest degree of wear was observed in the sample with the (Zr,Nb,Hf)N coating. The wear rate of the uncoated sample was 1.5 times greater than that of the sample with the (Zr,Nb,Hf)N coating. The (Zr,Nb,Hf)N coating also exhibited a low degree of indenter mass loss. The (Zr,Nb,Hf)N and ZrN coatings reduced the coefficient of friction (COF) most (COF of approximately 0.20–0.21, compared to COF = 0.28 for the uncoated sample). Defects (nanocavities) were detected in the interface area between the coatings and the substrate, which in some cases can have a negative effect on the wear resistance of the coating. The (Zr,Nb,Hf)N coating (72.07 at.% Zr, 24.87 at.% Nb and 3.05 at.% Hf) had the best wear resistance and a low friction coefficient. Full article

This study investigates the effect of boron carbide (B₄C) ceramic reinforcement on the microstructural, mechanical, electrical, and electrochemical properties of CoCrMo, Ti, and 17-4 PH alloys produced via powder metallurgy for potential biomedical applications. A systematic experimental design was employed, incorporating varying B₄C contents into each matrix through mechanical alloying, cold pressing, and vacuum sintering. The microstructural integrity and dispersion of B₄C were examined using scanning electron microscopy. The performance of the materials was evaluated using several methods, including Vickers hardness, pin-on-disk wear testing, ultrasonic elastic modulus measurements, electrical conductivity, and electrochemical assessments (potentiodynamic polarization and EIS). This study’s findings demonstrated that B₄C significantly enhanced the hardness and wear resistance of all alloys, especially Ti- and CoCrMo-based systems. However, an inverse correlation was observed between B₄C content and corrosion resistance, especially in 17-4 PH matrices. Ti-5B₄C was identified as the most balanced composition, exhibiting high wear resistance, low corrosion rate and elastic modulus values approaching those of human bone. Weibull analysis validated the consistency and reliability of key performance metrics. The results show that adding B₄C can change the properties of biomedical alloys, offering engineering advantages for B₄C-reinforced biomedical implants. Ti-B₄C composites exhibit considerable potential for application in advanced implant technologies. Full article

High-density polyethylene (HDPE) is a widely used thermoplastic known for its chemical resistance and ease of processing, but it has limited wear performance and moderate mechanical properties. In this study, recycled polyvinyl butyral (rPVB) was incorporated into HDPE at 5, 10, 15, and 20 wt.% to evaluate its effect on tribological performance. Pin-on-disk wear tests were conducted at 12, 15, and 18 N to assess the coefficient of friction (CoF) and wear resistance. Mean CoF values decreased by up to 40% with rPVB addition, with the best performance observed at 15 wt.% rPVB, although some variation was observed across replicates. SEM analysis revealed that rPVB promotes finer debris and transfer film formation, explaining the CoF reduction. However, wear resistance exhibited a complex trend: while rPVB improved adhesion and reduced material loss at lower loads, volume loss increased at higher loads, likely due to rPVB’s lower hardness. Mechanical testing showed an increase in elastic modulus at low rPVB contents due to higher crystallinity, confirmed by DSC; however, tensile strength and impact resistance decreased with rPVB. The results suggest that incorporating 10–15 wt.% of rPVB into HDPE can enhance frictional performance without severely compromising mechanical integrity, offering a sustainable way to valorize rPVB. Full article

This study evaluates the tribological behavior of two elastomeric sealing materials—EPDM and TPV—sliding against 30 wt.% glass fiber-reinforced polyamide 66 (PA66GF30), a composite widely used in structural and guiding components. The application context is low-leakage valve systems in polymer electrolyte membrane fuel cells (PEMFCs), particularly on the cathodic (air) side, where dry contact and low-friction sealing are critical. Pin-on-disk tests were conducted under three normal loads (1, 3, and 6 N) and sliding speeds of approximately 0.05, 0.10, and 0.15 m/s (92, 183, and 286 RPM). The coefficient of friction (CoF), mass loss, and wear morphology were analyzed. TPV generally exhibited lower and more stable friction than EPDM, with CoF values exceeding 1.0 at 1 N but falling within 0.32–0.52 under typical operating conditions (≥3 N). EPDM reached a maximum mass loss of 0.060%, while TPV remained below 0.022%. Microscopy revealed more severe wear features in EPDM, including tearing and abrasive deformation, whereas TPV surfaces displayed smoother, more uniform wear consistent with its dual-phase morphology. These findings support the selection of TPV over EPDM in dry-contact sealing interfaces involving composite counterfaces in PEMFC systems. Full article

This study investigates the current-carrying tribological properties and wear mechanisms of copper–graphite composites under varying contact loads. Two copper–graphite composites with different graphite content were prepared using the pressure sintering method. Current-carrying tribological tests were conducted at three distinct contact loads. Scanning electron microscopy, X-ray diffraction, laser confocal microscopy, and pin-on-disk tribological testing were utilized to examine the current-carrying tribological properties and the worn morphologies of the materials. The results indicate that, under the three contact loads, the friction coefficient of the copper–graphite materials ranged from 0.3 to 0.5, the wear rate was on the order of 10⁻¹³ m³/(N·m), the average voltage drop varied between 0.7 and 1.6 V, and the average electrical noise ranged from 0.2 to 0.9 mV. The wear mechanism included delamination wear and a minor amount of abrasive wear, and the lubricating film formed on the surface was mainly composed of C, PbO, and CuO. Notably, copper–graphite composites with lower graphite content exhibited superior hardness, electrical conductivity, and relative density compared to those with higher graphite content. At a contact load of 0.31 N, the copper–graphite composite containing 30wt% graphite demonstrated the most favorable current-carrying tribological performance, characterized by the lowest wear rate (1.09 × 10⁻¹³ m³/(N·m)), voltage drop (0.943 V), and electrical noise (0.234 mV). Full article

Surface texture and titanium nitride (TiN) coating have been established as effective methods for enhancing the tribological properties of mechanical friction pairs. This work aims to investigate the lubrication performance of rhombic-textured TiN-coated surfaces under oil-lubricated conditions using a pin-on-disk test mode. A total of 17 sets of samples were designed, including a control sample (with no rhombic texture and no TiN coating), a TiN-coated sample and rhombic-textured TiN-coated samples. The rhombic surface texture was fabricated using the end surface of a brass bar. TiN coating deposited TiN on the textured surface. This study focuses on measuring and comparatively analyzing the lubrication load capacity, friction coefficient (COF) and binding force of TiN coatings/substrates in the pin-on-disk friction test mode. Compared with the bare control sample, a rhombic texture can enhance lubrication load-carrying capacity by generating hydrodynamic lubrication effects, thereby reducing friction. Additionally, a rhombic texture enables the mitigation of third-body wear due to wear debris. This research provides valuable insights into the design and fabrication of mechanical friction pairs with high wear resistance under oil-lubricated conditions. For lubrication property enhancement, the influence of groove depth was larger than that of the length of the rhombic side. Full article

The investment casting process, also known as lost-wax casting, is widely used for producing ferrous and non-ferrous metal parts due to its excellent surface finish and dimensional accuracy. In recent years, the use of Co-Cr-Mo alloy has increased due to its high corrosion resistance, good biocompatibility, and relatively high wear resistance. Laser melting of materials has been demonstrated to refine the surface grain structure, reduce surface roughness, and improve both wear and corrosion resistance. The ability to fine-tune parameters such as laser power density and scanning speed facilitates the optimization of the treated layers’ thickness and homogeneity, thereby addressing many of the shortcomings inherent in conventional methods. This study investigates the microstructural, mechanical wear and bioactive behavior of investment-cast Co-Cr-Mo parts subjected to a Nd:YAG laser surface treatment. The effects of different processing parameters were analyzed quantitatively and comprehensively. The specimens were characterized using metallographic techniques, bioactivity evaluation, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), wear testing (Pin-on-Disk), and hardness testing. Our results demonstrate that Nd:YAG laser melting significantly enhances the surface properties and maintains the dimensional accuracy of complex Co-Cr-Mo biomedical components, through microstructural refinement, increased hardness, improved wear resistance, and preserved biocompatibility. The specific combination of investment casting with precisely controlled laser surface modification represents a significant advancement for improving the longevity and performance of biomedical implants. Full article

In this study, the effect of martensite volume fraction on the mechanical, tribological, and corrosion properties of API 5CT dual-phase steel is studied based on intercritical heat treatment routes at different temperatures (730, 760, and 790 °C). Hardness of the specimens increased by increasing the martensite volume fraction up to 50%. Further increase in martensite volume fraction led to an increase in wear resistance. Sliding wear pin-on-disk tests were analyzed following the ASTM G99 standard, obtaining the wear rate, the volume of lost mass, and the Archard coefficient as a function of time and temperature of the heat treatment. A comparison was made between the wear rate and the hardness data, and its proportionality was established. The corrosion behavior of DP steels in 3.5% NaCl solution was studied by the potentiodynamic polarization technique. The result showed that with increasing the martensite amount in the specimen and decreasing the ferrite amount, the corrosion rate decreased. Finally, the corrosion mechanism in DP steel depends on the self-corrosion resistance behavior of both phases (martensite-ferrite) as well as the presence of galvanic corrosion between them. Full article

Worm drive belongs to the inclined plane transmission principle, and there is severe wear on the conjugate tooth surface. To reveal the wear mechanism and realize steel–steel meshing in the spiroid worm drive, the meshing performance model of conjugate tooth surface is established based on differential geometry theory and gear meshing principle, and the wear performance model is inferred by the Archard model and microscopic meshing performance. The wear performance of conjugate tooth surface is analyzed through the digital calculation, the pin-disk friction, and wear testing, as well as the spiroid worm drive prototype performance testing. The results show that there are good lubrication and anti-wear characteristics between the conjugate tooth surfaces, the wear amount on the right flank is twice that of the left flank, the wear depth at the loaded flank of the spiroid gear surface is smaller than that at the unloaded flank, as well as the feasibility of steel–steel meshing in worm drive has been confirmed. Full article

In this work, the microstructure, hardness, tensile and yield strength, and wear resistance of X210CrW12 steel are examined in relation to the impacts of deep cryogenic treatment. In order to achieve this, deep cryogenic treatment at −180 °C was applied to X210CrW12 steel samples for 12, 18, 24, and 36 h following quenching. Following the cryogenic treatments, a tempering heat treatment was applied to the samples at 300 °C for two hours. Experimental results showed that deep cryogenic treatment significantly improved the mechanical properties of X210CrW12 steel. The best mechanical properties were obtained after applying deep cryogenic treatment for 24 and 36 h. The cryogenic treatment showed the most dominant effect on wear resistance. As a result of the wear tests performed with the pin-on-disk method, it was determined that the wear rate of the sample subjected to cryogenic treatment for 36 h was 59.37% less than that of the conventionally hardened sample. The deep cryogenic treatment applied for 36 h provided the highest hardness increase of 12.06%. Compared to the conventionally hardened sample, the tensile and yield strength in the steel subjected to deep cryogenic treatment for 24 h is up to 11.02% and 11.35% higher. As a result of microstructural analysis, it was determined that it provides cryogenic new carbide precipitation, increases carbide density, and provides a more homogeneous carbide distribution. Full article

The article presents the results of a comparison of the wear resistance of coatings with a two-layer architecture (adhesion layer–wear-resistant layer) of Zr-ZrN, Zr-(Zr,Ti)N, Zr,Hf-(Zr,Hf)N, Zr,Nb-(Zr,Nb)N, Zr,Hf-(Ti,Zr,Hf)N, and Zr,Nb-(Ti,Zr,Nb)N coatings, deposited on a titanium alloy substrate. The wear resistance was studied using two different counterbodies: Al₂O₃ and steel. When in contact with the Al₂O₃ counterbodies, the best wear resistance was demonstrated by samples with Zr,Hf-(Zr,Hf)N and Zr,Nb-(Zr,Nb,Ti)N coatings. In tests conducted in contact with the steel counterbody, the best resistance was demonstrated by samples with Zr-ZrN and Zr,Hf-(Ti,Zr,Hf)N coatings. The wear resistance of samples with (Zr,Hf)N and (Zr,Nb,Ti)N coatings was 2.5–3.3 times higher than that of the uncoated sample. The Zr,Nb adhesion layer ensures better adhesion of the coating to the substrate. It was found that not only the adhesion strength of the adhesion layer to the substrate and coating is of significant importance but also the strength of the adhesion layer itself. The surface film of titanium oxide must be completely etched off to ensure maximum strength of the adhesive bond between the coating and the substrate. It has been established that the adhesion of the coating and the titanium substrate is also affected by the characteristics of the outer (wear-resistant) coating layer, which is the composition and structure of the wear-resistant coating layer. Delamination can occur both at the boundary of the adhesive layer with the substrate and at the boundary of the wear-resistant and adhesive layers of the coating depending on the strength of the adhesive bonds in the corresponding pair. It is necessary to ensure a good combination of properties both in the substrate–adhesion layer system and in the adhesion layer–wear-resistant layer system. Full article

This study investigates the influence of graphene nanoplatelets (GNPs) and the formation of nanosized Al₄C₃ on the tribological performance of hot extruded aluminum-based nanocomposites. Al/GNP nanocomposites with varying GNP contents (0, 0.1, 0.5, and 1.1 wt.%) were fabricated through powder metallurgy, including ball milling, compaction, and hot extrusion at 500 °C, which was designed to facilitate the formation of nanosized carbides during the extrusion process. The effect of GNPs and nanosized carbides on the tribological properties of the composites was evaluated using dry friction pin-on-disk tests to assess wear resistance and the coefficient of friction (COF). Microstructural analyses using scanning electron microscopy and energy-dispersive X-ray spectroscopy confirmed the uniform distribution of GNPs and the formation of nanosized Al₄C₃ in the samples. Incorporating 0.1 wt.% GNPs resulted in the lowest wear mass loss (1.40 mg) while maintaining a stable COF (0.52), attributed to enhanced lubrication and load transfer. Although a higher GNP content (1.1 wt.%) resulted in increased wear due to agglomeration, the nanocomposite still demonstrated superior wear resistance compared to the unreinforced aluminum matrix. These findings underscore the potential of combining nanotechnology with precise processing techniques to enhance the wear and friction properties of aluminum-based composites. Full article

Stainless steel 17-4PH is valued for its high strength and corrosion resistance but poses machining challenges due to rapid tool wear. This research investigates the use of pulsed electron beam surface treatment to enhance the surface properties of components fabricated by binder jetting additive manufacturing. The aim is to improve the tribological performance compared to the as-sintered condition and the H900 aging process, which optimizes hardness and wear resistance. Printed samples were sintered in a reducing atmosphere and superficially treated with an electron beam by varying the voltage and the pulse count. Results showed that the voltage affects the roughness and thickness of the treated layer, while the number of pulses influences the hardening of the microstructure and, consequently, the wear resistance. A reciprocating linear pin-on-disk wear test was conducted at 2 N and 10 Hz. Surface-treated samples exhibited lower coefficients of friction, though the values approached those of aged samples after the abrasion of the melted layer, indicating a deeper heat-affected zone formation. Still, the friction remained lower than that of as-printed specimens. This study demonstrates that optimizing electron beam parameters is vital for achieving surface performance comparable to bulk aging treatments, with significant implications for long-term wear resistance. Full article

The increasing demand for high-performance materials in industrial applications highlights the need for composites with enhanced mechanical and tribological properties. Basalt fiber-reinforced polymers (BFRP) are promising materials due to their superior strength-to-weight ratio and environmental benefits, yet their wear resistance and tensile performance often require further optimization. This study examines how adding copper (Cu) powder to epoxy resin influences the mechanical and tribological properties of BFRP composites. Epoxy matrices, modified with 5%, 10%, and 15% weight fractions (wf.%) of copper powder, were reinforced with BFRP-type fabric, using a vacuum bag manufacturing method. Mechanical tests, including bending and tensile tests, showed notable improvements in tensile strength and flexural modulus due to copper addition, with higher copper (Cu) content enhancing ductility. Tribological tests using a pin-on-disk tribometer revealed reduced wear rates and an optimized coefficient of friction. Statistical analysis and 3D microscopy identified wear mechanisms such as delamination and protective copper film formation. The results highlight the significant potential of copper-modified BFRP composites for applications demanding superior mechanical and tribological performance. Full article

This study investigates the optimization of boron coating parameters for medium-carbon steels, specifically AISI 1137, and their subsequent effects on mechanical properties, which are crucial for industrial applications. Despite extensive research on boronizing processes, an understanding of the optimal conditions that enhance wear resistance and hardness while maintaining structural integrity is still lacking. To address this gap, we systematically examined the impact of boronizing temperatures (850 °C and 950 °C) and durations (2, 4, and 8 h) on the structural and mechanical properties of AISI 1137 steel. Our findings indicate the need for improved surface properties in medium-carbon steels used in demanding environments, such as automotive and machinery components. The boronizing process was carried out using Ekabor 1 powder, with characterization performed through optical microscopy, pin-on-disk wear tests, and Vickers hardness analysis. Results showed that the thickness of the boronized layer ranged from 50.6 μm to 64.8 μm, with wear resistance increasing by 1.8 to 3.9 times at 950 °C compared to at 850 °C. The measured hardness of the boronized surface layers varied between 1963.7 HV and 219.3 HV, decreasing from the boronized layer toward the base material. The optimal parameters for wear resistance and hardness were found to be a temperature of 950 °C and a duration of 8 h, facilitating the formation of FeB and Fe₂B phases, which significantly enhanced the steel’s mechanical properties. This research provides valuable insights into the boronizing process and establishes a foundation for the optimizing of surface treatments to extend the lifespan and performance of medium-carbon steels in industrial use. Full article