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15 pages, 5933 KB  
Article
Experimental Study on Proppant Transport and Distribution in Asymmetric Branched Fractures
by Zhitian Lu, Hai Qu, Ying Liu, Zhonghua Liu, Su Liu, Pengcheng Zhang and Kaige You
Processes 2025, 13(11), 3482; https://doi.org/10.3390/pr13113482 - 30 Oct 2025
Abstract
Hydraulic fracturing is a key technique for creating complex fractures in unconventional reservoirs to enhance energy recovery. Asymmetric branched fractures, as fundamental units, are widely observed in complex fracture networks. Effective proppant distribution within such structures is critical but remains poorly understood. To [...] Read more.
Hydraulic fracturing is a key technique for creating complex fractures in unconventional reservoirs to enhance energy recovery. Asymmetric branched fractures, as fundamental units, are widely observed in complex fracture networks. Effective proppant distribution within such structures is critical but remains poorly understood. To investigate this, a rough-walled slot with two branches was developed, where asymmetry was introduced by inserting plates with different geometries on one side. The results show that the structural asymmetry between the left and right branches can significantly induce non-uniform transport and irregular sand bed morphology. Reducing the height and width of branch fractures increases fluid velocity, limiting proppant settling within the branch. As the flow area decreases, the fluid velocity increases, driving more proppant through the branch toward the distal fracture region. Injection pressure increases as the flow area of the branch fracture decreases. At a height ratio of 0.25, sand plugging and ineffective proppant placement probably occur within the natural fracture. When the branch is located at the upper section, proppants hardly settle to form a bed, leading to closure of the fracture. The study provides new insights into optimizing proppant placement in complex fractures. Full article
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15 pages, 2799 KB  
Article
An Experimental Study on the Effects of Pre-Chamber Geometry on the Combustion Characteristics of Ammonia/Air Mixtures Using Turbulent Jet-Post Spark Ignition Strategy
by Yichen Gao, Xipu Zhang, Yang Cao, Jiashen Zhang, Rongjie Li, Huimin Wu, Shijun Dong and Zhaowen Wang
Energies 2025, 18(21), 5659; https://doi.org/10.3390/en18215659 - 28 Oct 2025
Abstract
As a carbon-free fuel, ammonia faces challenges in engine applications due to its low flame propagation speed and high ignition energy. The pre-chamber turbulent jet-post spark ignition strategy (TJ-PSI) has been proven effective in accelerating the combustion of stoichiometric ammonia/air mixtures. This study [...] Read more.
As a carbon-free fuel, ammonia faces challenges in engine applications due to its low flame propagation speed and high ignition energy. The pre-chamber turbulent jet-post spark ignition strategy (TJ-PSI) has been proven effective in accelerating the combustion of stoichiometric ammonia/air mixtures. This study investigates the effects of orifice configuration on the combustion characteristics of stoichiometric ammonia/air premixed mixtures under TJ-PSI mode. Experiments are performed in a constant-volume combustion vessel filled with stoichiometric ammonia/air mixtures, and the spark plug used to trigger the ignition of the mixture in the main chamber is located downstream of the pre-chamber turbulent jet flow. With pre-chamber volume maintained constant, pre-chambers with different orifice numbers (Φ1.4 mm × 1, Φ1.4 mm × 4, Φ1.4 mm × 6) and orifice diameters (Φ4.0 mm × 1) are tested, along with varying time intervals (TI) between the main chamber and pre-chamber spark timings. Experimental results show that the pre-chamber with single large orifice (Φ4.0 mm × 1) produces jet flames but offers limited combustion enhancement. In contrast, a single small orifice (Φ1.4 mm) generates flameless turbulent jets, which reduce combustion duration by 53% compared to the large-orifice case. This improvement is attributed to the pre-chamber jet enhancing turbulence in the main chamber, whereas larger orifices yield lower turbulence intensity. Although multi-orifice configurations provide less pronounced enhancement compared to the single-orifice case, they effectively prevent flame kernel extinction at short TIs (e.g., 10 ms). Consequently, the total combustion duration from pre-chamber spark to the end of main chamber combustion can be significantly shortened. Full article
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34 pages, 15906 KB  
Article
Investigation of the Relationship Between Reservoir Sensitivity and Injectivity Impedance in Low-Permeability Reservoirs
by Baolei Liu, Youqi Wang, Hongmin Yu, Xiang Li and Lingfeng Zhao
Processes 2025, 13(10), 3283; https://doi.org/10.3390/pr13103283 - 14 Oct 2025
Viewed by 339
Abstract
In low-permeability reservoirs, studying reservoir sensitivity is crucial for optimizing water flooding, as it identifies detrimental mineral-fluid interactions that can cause formation damage and reduce injection efficiency. However, existing diagnostic methods for sensitivity-induced damage rely on post-facto pressure monitoring and lack a quantitative [...] Read more.
In low-permeability reservoirs, studying reservoir sensitivity is crucial for optimizing water flooding, as it identifies detrimental mineral-fluid interactions that can cause formation damage and reduce injection efficiency. However, existing diagnostic methods for sensitivity-induced damage rely on post-facto pressure monitoring and lack a quantitative relationship between sensitivity factors and water injectivity impairment. Furthermore, correlating microscale interactions with macroscopic injectivity parameters remains challenging, causing current models to inadequately represent actual injection behavior. This study combines microscopic techniques (e.g., SEM, XRD, NMR) with macroscopic core flooding experiments under various sensitivity-inducing conditions to analyze the influence of reservoir mineral composition on flow capacity, evaluate formation sensitivity, and assess the dynamic impact on water injectivity. The quantitative relationship between clay minerals and injectivity impairment in low-permeability reservoirs is also investigated. The results indicate that flow capacity is predominantly governed by the type and content of sensitive minerals. In water-sensitive reservoirs, water injection induces clay swelling and migration, leading to flow path reconfiguration and water-blocking effects. In salt-sensitive formations, high-salinity water promotes salt precipitation within pore throats, reducing permeability. In velocity-sensitive formations, fine particle migration causes flow resistance to initially increase slightly and then gradually decline with continued injection. Acidizing generally enhances pore connectivity but induces pore-throat plugging in chlorite-rich reservoirs. Alkaline fluids can exacerbate heterogeneity and generate precipitates, though appropriate concentrations may improve connectivity. Under low effective stress, rock dilation increases porosity and permeability, while elevated stress causes compaction, increasing flow impedance. Full article
(This article belongs to the Special Issue Advanced Strategies in Enhanced Oil Recovery: Theory and Technology)
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30 pages, 28571 KB  
Article
Research on the Mechanism and Characteristics of Gel–Microbial Composite Oil Displacement in Hypertonic Heavy Oil Reservoirs
by Baolei Liu, Xiang Li, Hongbo Wang and Xiang Liu
Gels 2025, 11(10), 818; https://doi.org/10.3390/gels11100818 - 12 Oct 2025
Viewed by 242
Abstract
To address the limitations of traditional chemical flooding—such as high cost, environmental impact, and formation damage—and the challenges of standalone microbial flooding—including preferential channeling, microbial loss, and limited sweep efficiency—this study develops a novel composite system for a high-permeability heavy oil reservoir. The [...] Read more.
To address the limitations of traditional chemical flooding—such as high cost, environmental impact, and formation damage—and the challenges of standalone microbial flooding—including preferential channeling, microbial loss, and limited sweep efficiency—this study develops a novel composite system for a high-permeability heavy oil reservoir. The system integrates a 3% scleroglucan + 1% phenolic resin gel (ICRG) with Bacillus licheniformis (ZY-1) and a surfactant. Core flooding and two-dimensional physical simulation experiments reveal a synergistic mechanism: The robust and biocompatible ICRG gel effectively plugs dominant flow paths, increasing displacement pressure fourfold to divert subsequent fluids. The injected strain ZY-1 then metabolizes hydrocarbons, producing biosurfactants that reduce oil–water interfacial tension by 61.9% and crude oil viscosity by 65%, thereby enhancing oil mobility. This combined approach of conformance control and enhanced oil displacement resulted in a significant increase in ultimate oil recovery, achieving 15% and 20% in one-dimensional and two-dimensional models, respectively, demonstrating its substantial potential for improving heavy oil production. Full article
(This article belongs to the Special Issue Polymer Gels for Oil Recovery and Industry Applications)
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20 pages, 3712 KB  
Article
Analysis of Control Factors for Sensitivity of Coalbed Methane Reservoirs
by Peng Li, Cong Zhang, Bin Fan, Jie Zhang and Zhongxiang Zhao
Processes 2025, 13(10), 3133; https://doi.org/10.3390/pr13103133 - 29 Sep 2025
Viewed by 575
Abstract
Formation damage sensitivity is a primary constraint on productivity in coalbed methane (CBM) reservoirs. Conventional experimental methods, which often employ crushed or plug coal samples, disrupt the natural fracture network, thereby overestimating matrix damage and underestimating fracture-related damage. In this study, synchronous comparative [...] Read more.
Formation damage sensitivity is a primary constraint on productivity in coalbed methane (CBM) reservoirs. Conventional experimental methods, which often employ crushed or plug coal samples, disrupt the natural fracture network, thereby overestimating matrix damage and underestimating fracture-related damage. In this study, synchronous comparative experiments were conducted using raw coal and briquette coal cores, integrated with scanning electron microscopy (SEM) and nuclear magnetic resonance (NMR) analyses to characterize coal composition and pore structure. This approach elucidates the underlying mechanisms controlling reservoir sensitivity. The main findings are as follows: The dual-sample comparative system reveals substantial deviations in traditional experimental assessments. Due to post-dissolution compaction, briquette coal samples overestimate acid sensitivity while underestimating water sensitivity. Stress sensitivity is primarily attributed to the irreversible compression of natural fractures. Differences in acid sensitivity are governed by structural integrity: mineral dissolution leads to collapse in briquette coal, whereas fractures help maintain stability in raw coal. Raw coal exhibits a lower critical flow rate for velocity sensitivity and undergoes significant water sensitivity damage below 1 MPa. Both sample types show weak alkaline sensitivity, with damage acceleration observed within the pH range of 7 to 10. Full article
(This article belongs to the Section Energy Systems)
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28 pages, 11872 KB  
Article
Research on the Dynamic Characteristics of a Gas Purification Pipeline Robot in Goafs
by Hongwei Yan, Yaohui Ma, Hongmei Wei, Ziming Kou, Haojie Ren and Guorui Wang
Machines 2025, 13(10), 889; https://doi.org/10.3390/machines13100889 - 29 Sep 2025
Viewed by 289
Abstract
Gas monitoring and dust control in coal mine goafs are critical for ensuring safe and efficient production. To address the challenges posed by dust accumulation from mechanized mining and ventilation systems, this study designs a spiral-driven gas purification pipeline robot integrating a wet [...] Read more.
Gas monitoring and dust control in coal mine goafs are critical for ensuring safe and efficient production. To address the challenges posed by dust accumulation from mechanized mining and ventilation systems, this study designs a spiral-driven gas purification pipeline robot integrating a wet dust removal mechanism. The robot features a modular structure, including a spiral drive, a plugging and extraction system, and a wet dust removal unit, to enhance pipeline adaptability and dust removal performance. Dynamic modeling reveals that the robot’s speed increases with the deflection angle of the driving wheel, with optimal performance observed at a 45° angle. The analysis of the rolling friction, medium resistance, and deflection angle indicates that reducing the angle improves the obstacle-crossing ability. Numerical simulations of gas migration in the goaf identify a high dust concentration at the air outlet and show that flow velocity significantly affects dust removal efficiency. Simulation and prototype testing confirm stable robot operation at deflection angles of between 30° and 90° and effective crossing of 5 mm barriers. Optimal dust removal is achieved with a 5 m/s flow velocity, 0.6 MPa water mist pressure, and 400 mm chord grid spacing, providing both theoretical and practical guidance for gas monitoring and dust control in coal mine goafs. Full article
(This article belongs to the Section Robotics, Mechatronics and Intelligent Machines)
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15 pages, 3391 KB  
Article
A Method of Analyzing the Component Reactions of an Overall Reaction: Autothermal Reforming of Acetic Acid Example
by James Manganaro, Yujia Liu, Jiazhun Huang, Bi Chen and Adeniyi Lawal
Processes 2025, 13(10), 3112; https://doi.org/10.3390/pr13103112 - 28 Sep 2025
Viewed by 339
Abstract
Using Excel and its Solver feature, a novel method of analyzing the component reactions of an overall reaction is outlined. As an example, autothermal reforming (300–700 °C) of acetic acid (AA), a significant component of pyrolysis oil, was considered. The overall reaction can [...] Read more.
Using Excel and its Solver feature, a novel method of analyzing the component reactions of an overall reaction is outlined. As an example, autothermal reforming (300–700 °C) of acetic acid (AA), a significant component of pyrolysis oil, was considered. The overall reaction can be viewed as comprising five individual reactions: reforming, oxidation, water–gas shift, reverse Boudouard, and methanation. A laboratory apparatus was set up in which acetic acid, air, and water were continuously fed to a BASF dual-layer catalytic reactor in plug flow at 1 atm. For this setup, it is easy to construct a material balance in Excel in which five factors, fi, are defined which represent the fraction of reactant going to each of the individual five reactions. Using the Solver feature of Excel, it can readily be determined which of the five factors fi produce the best match of the calculated exit gas composition with the measured gas concentrations for CO, CO2, H2, CH4, and O2. Furthermore, a program such as GasEq or Aspen can then be used to calculate the theoretical equilibrium gas composition at a given condition. Using this equilibrium gas composition and Solver, the individual (fi)equilb can be calculated. Thus, the ratio fi/(fi)equilb is an indication of how close each component reaction is to equilibrium. In this way, an idea is gained of which of the individual component reactions need to be improved or inhibited or if operating parameters should be adjusted. For the specific case of autothermal reforming of acetic acid, the steam reforming reaction requires at least 600 °C to approach equilibrium. In contrast, the oxidation reaction goes to equilibrium throughout the temperature range, completely consuming oxygen. The water–gas shift reaction appears to approach equilibrium to the extent of 71–90% throughout the temperature range. The reverse Boudouard reaction is favored at lower temperatures; in fact, coking was predicted and found at the low temperature of 300 °C. Full article
(This article belongs to the Section Chemical Processes and Systems)
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19 pages, 4766 KB  
Article
Experimental Study on Migration Characteristics and Profile Control Performance of Gel Foam in Fractured-Vuggy Reservoir
by Yan Xin, Binfei Li, Jingyu Zhang, Bo Wang, Aojue Liu and Zhaomin Li
Gels 2025, 11(10), 768; https://doi.org/10.3390/gels11100768 - 24 Sep 2025
Viewed by 356
Abstract
Gel foam exhibits excellent applicability in fractured-vuggy reservoirs, effectively plugging flow channels and enhancing oil recovery. However, due to the harsh high-temperature environment and the complex and variable fracture-vuggy structure in reservoirs, gel foam may undergo structural changes during its migration, which can [...] Read more.
Gel foam exhibits excellent applicability in fractured-vuggy reservoirs, effectively plugging flow channels and enhancing oil recovery. However, due to the harsh high-temperature environment and the complex and variable fracture-vuggy structure in reservoirs, gel foam may undergo structural changes during its migration, which can affect its flow properties and plugging efficiency. Therefore, investigating the migration characteristics of gel foam in fractured reservoirs through visual experiments is of significant practical importance. In this study, migration experiments with different foam systems were conducted using the visualized vuggy model. The migration stability of foam was characterized by combining the sweep range and liquid drainage rate, and the impact of temperature on the migration characteristics of gel foam was explored. Additionally, a profile control experiment was performed using the fractured-vuggy network model, analyzing and summarizing its mechanisms for enhancing oil recovery in fractured-vuggy reservoirs. The results showed that, in the vuggy model, compared with ordinary foam and polymer foam, gel foam showed a lower drainage rate, higher foam retention rate and wider sweep range, and could form stable plugging in fractured-vuggy reservoirs. An increased temperature accelerated the thermal expansion of gas and changes in liquid film characteristics, which led to the expansion of foam migration speed and sweep range. Although a high temperature increased the liquid drainage rate of foam, it was still lower than 3%, and the corresponding foam retention rate was higher than 97%. In addition, the gel foam had a strong profile control ability, which effectively regulated the gas migration path and improved the utilization degree of remaining oil. Compared with the first gas flooding, the recovery of subsequent gas flooding was increased by 18.85%, and the final recovery of the model reached 81.51%. Comprehensive analysis revealed that the mechanism of enhanced oil recovery by gel foam mainly included density control, foam regeneration, flow redirection, stable plugging, and deep displacement by stable gel foam. These mechanisms worked synergistically to contribute to increased recovery. The research results fully demonstrate the application advantages of gel foam in fractured-vuggy reservoirs. Full article
(This article belongs to the Special Issue Polymer Gels for the Oil and Gas Industry)
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29 pages, 4303 KB  
Article
Revisiting Tundish Flow Characterization: A Combined Eulerian-Lagrangian Study on the Effects of Dams, Baffles, and Side-Wall Inclination
by Ali Mostafazade Abolmaali, Mohamad Bayat, Venkata Karthik Nadimpalli, Thomas Dahmen and Jesper Hattel
Materials 2025, 18(18), 4392; https://doi.org/10.3390/ma18184392 - 20 Sep 2025
Viewed by 446
Abstract
This study aims to use Computational Fluid Dynamics (CFD) analysis to improve inclusion removal efficiency in tundishes used in the steelmaking industry, with the broader goal of promoting more sustainable steel production and supporting circular economy objectives by producing cleaner steel. Inclusions are [...] Read more.
This study aims to use Computational Fluid Dynamics (CFD) analysis to improve inclusion removal efficiency in tundishes used in the steelmaking industry, with the broader goal of promoting more sustainable steel production and supporting circular economy objectives by producing cleaner steel. Inclusions are non-metallic particles, such as alumina, that enter the tundish with the molten steel and travel through it; if not removed, they can exit through the nozzles and adversely affect the mechanical properties of the final product and process yield. An existing tundish design is modified using three passive techniques, including adding a vertical dam, adding a horizontal baffle, and inclining the side walls, to assess their influence on fluid flow behavior and inclusion removal. Residence time distribution (RTD) analysis is employed to evaluate flow characteristics via key metrics such as dead zone and plug flow volume fractions, as well as plug-to-dead and plug-to-mixed flow ratios. In parallel, a discrete phase model (DPM) analysis is conducted to track inclusion trajectories for particles ranging from 5 to 80 μm. Results show that temperature gradients due to heat losses significantly influence flow patterns via buoyancy-driven circulation, changing RTD characteristics. Among the tested modifications, inclining the side walls proves most effective, achieving average inclusion removal improvements of 8% (Case B1) and 19% (Case B2), albeit with increased heat loss due to greater top surface exposure. Vertical dam and horizontal baffle, despite showing favorable RTD metrics, generally reduce the inclusion removal rate, highlighting a disconnect between RTD-based predictions and DPM-based outcomes. These findings demonstrate the limitations of relying solely on RTD metrics for evaluating tundish performance and suggest that DPM analysis is essential for a more accurate assessment of inclusion removal capability. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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15 pages, 2376 KB  
Article
Dry Iron Ore Fluidization, Flowability, and Handling: Supporting Dry Processing of Iron Ores and Guiding Industrial Designing
by Benito Barbabela e Silva, Anderson de Araújo Soares, Monica Guimarães Vieira, Rogério Ruiz, Arthur Pinto Chaves and Maurício Guimarães Bergerman
Minerals 2025, 15(9), 998; https://doi.org/10.3390/min15090998 - 19 Sep 2025
Viewed by 909
Abstract
Renewed interest in dry processing has arisen due to challenges in water management. In dry iron ore beneficiation, flowability of bulk solids is a key concern, leading to issues like plugging and clogging in bins and chutes. Handling also faces challenges from environmental [...] Read more.
Renewed interest in dry processing has arisen due to challenges in water management. In dry iron ore beneficiation, flowability of bulk solids is a key concern, leading to issues like plugging and clogging in bins and chutes. Handling also faces challenges from environmental regulations, particularly regarding dust emissions. Enclosed conveyor technologies, such as air-assisted conveyors that use fluidization, offer effective solutions, though the maximum particle size that can be conveyed is a limitation that needs consideration. This paper examines how the size and chemical composition of bulk iron ore materials affect their handling behavior. By employing Geldart’s and Jenike’s methods, this document provides technical parameters and recommendations, which are lacking in the current literature, for the designing of dry processing plants. Findings indicate that ultrafines can have a flow function as low as 2.05, indicating cohesive behavior even when dried, while fluidization tests support these characteristics. In contrast, coarser fractions are easy for free-flowing materials. Samples with a top size of 0.5 mm fall between sand-like and spoutable groups in Geldart’s classification. Denser materials did not fluidize, while less dense ones did. Thus, air slides should avoid handling materials at this threshold and focus on finer materials. This paper offers guidance for designing dry processing plants to address handling bottlenecks. Full article
(This article belongs to the Section Mineral Processing and Extractive Metallurgy)
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16 pages, 10863 KB  
Article
Pinless Friction Stir Spot Welding of Pure Copper: Process, Microstructure, and Mechanical Properties
by Xu Zhang, Xiaole Ge, Igor Kolupaev, Zhuangzhuang Shan and Hongfeng Wang
Crystals 2025, 15(9), 804; https://doi.org/10.3390/cryst15090804 - 12 Sep 2025
Viewed by 403
Abstract
Pure copper joints (PCJs) were fabricated using pinless friction stir spot welding (P-FSSW), a solid-state welding technique, to investigate the influence of plunge depth, rotational speed, and dwell time on PCJ performance. Thermal cycles under different welding parameters were recorded, while the microstructure [...] Read more.
Pure copper joints (PCJs) were fabricated using pinless friction stir spot welding (P-FSSW), a solid-state welding technique, to investigate the influence of plunge depth, rotational speed, and dwell time on PCJ performance. Thermal cycles under different welding parameters were recorded, while the microstructure at various locations within the welded zone was characterized using electron backscatter diffraction (EBSD). The microhardness and tensile–shear force (T-SF) of the PCJs were evaluated, and the fracture types together with fracture evolution were analyzed. The experimental results reveal that, under the combined effect of thermal cycles and mechanical stirring, subgrains in the welded zone transformed into recrystallized grains, whereas intense material flow contributed to an increased fraction of deformed grains. At the Hook region and the interface between the upper and lower sheets, grains were tightly bonded, resulting in effective metallurgical joining. Higher microhardness values were observed in the stir zone (SZ), whereas lower values appeared in the heat-affected zone beneath the interface. With increasing plunge depth, rotational speed, and dwell time, the T-SF of the PCJs first increased and then decreased, achieving a relatively high value at a plunge depth of 0.4 mm, a rotational speed of 1500 rpm, and a dwell time of 9 s. The fracture types of the PCJs were shear fracture and plug fracture, with the Hook region identified as the weakest zone. Full article
(This article belongs to the Special Issue Metallurgy-Processing-Properties Relationship of Metallic Materials)
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15 pages, 4991 KB  
Article
Robust Angio-Vasculogenic Properties of 3D-Cultured Dual GCP-2/PDGF-β Gene-Edited Human ASCs
by Seongho Han, Sang Joon An and Sung-Whan Kim
Int. J. Mol. Sci. 2025, 26(17), 8425; https://doi.org/10.3390/ijms26178425 - 29 Aug 2025
Viewed by 597
Abstract
Adipose-derived mesenchymal stem cells (ASCs) have great potential in regenerative medicine due to their abundance and innate multi-lineage differentiation potential. However, the therapeutic efficacy of ASCs is often compromised by poor microenvironmental conditions in the damaged tissues after transplantation. In this study, we [...] Read more.
Adipose-derived mesenchymal stem cells (ASCs) have great potential in regenerative medicine due to their abundance and innate multi-lineage differentiation potential. However, the therapeutic efficacy of ASCs is often compromised by poor microenvironmental conditions in the damaged tissues after transplantation. In this study, we generated and assessed genetically modified ASCs that expressed granulocyte chemotactic protein-2 (GCP-2) and platelet-derived growth factor-β (PDGF-β). The results revealed that three-dimensional (3D)-cultured ASCs overexpressing GCP-2 and PDGF-β (3D-A/GP) yielded a significant increase in proangiogenic gene expression, cell migration, and endothelial tube formation in vitro. Moreover, the Matrigel plug assay revealed that 3D-A/GP formed functional blood vessels, and 3D-A/GP injection in a hind limb ischemia (HLI) model revealed higher blood flow recovery, limb salvage, and capillary density and lower apoptosis in mice, compared to the controls. Notably, 3D-A/GP exhibited differentiation into endothelial-like cells and upregulated expression of angiogenic factors in ischemic limb tissue. Our results highlight the value of using a combination of genetic engineering and 3D culture systems to improve the therapeutic effect of ASCs in terms of angiogenesis-dependent tissue repair. The dual modulation of GCP-2 and PDGF-β, in combination with 3D culture, presents a new and synergistic opportunity to maximize the use of ASC-based therapies for ischemic diseases and other regenerative medicine applications. Full article
(This article belongs to the Section Molecular Biology)
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19 pages, 3213 KB  
Article
Experimental Investigation of Deformable Gel Particles (DGPs) for Plugging Pan-Connected Interlayer Channels in High-Water-Cut Reservoirs
by Wenjing Zhao, Jing Wang, Tianjiang Wu, Ronald Omara Erik, Zhongyang Qi and Huiqing Liu
Gels 2025, 11(9), 686; https://doi.org/10.3390/gels11090686 - 27 Aug 2025
Viewed by 494
Abstract
Pan-connected interlayers are widely present in oil reservoirs, forming flow channels at different positions. However, conventional profile control agents struggle to plug deep interlayer channels in reservoirs, limiting the swept volume of injected water. Additionally, a clear methodology for physically simulating pan-connected reservoirs [...] Read more.
Pan-connected interlayers are widely present in oil reservoirs, forming flow channels at different positions. However, conventional profile control agents struggle to plug deep interlayer channels in reservoirs, limiting the swept volume of injected water. Additionally, a clear methodology for physically simulating pan-connected reservoirs with interlayer channels and calculating interchannel flow rates remains lacking. In this study, a physical model of pan-connected interlayer reservoirs was constructed to carry out deformable gel particles (DGPs) plugging experiments on interlayer channels. A mass conservation-based flow rate calculation method for interlayer channels with iterative solution was proposed, revealing the variation law of interlayer channel flow rates during DGP injection and subsequent water flooding. Finally, oil displacement and DGP profile control experiments in pan-connected interlayer reservoirs were conducted. The study shows that during DGP injection, injected water enters the potential layer through interlayer channels in the middle and front of the water-channeling layer and bypasses back to the water-channeling layer through channels near the production well. With the increase in DGP injection volume, the flow rate of each channel increases. During subsequent water flooding, DGP breakage leads to a rapid decline in its along-path plugging capability, so water bypasses back to the water-channeling layer from the potential layer through all interlayer channels. As the DGP injection volume increases, the flow rate of each channel decreases. Large-volume DGPs can regulate interlayer channeling reservoirs in the high water cut stage. Its effectiveness mechanism involves particle migration increasing the interlayer pressure difference, which drives injected water to sweep from the water-channeling layer to the potential layer through interlayer channels, improving oil recovery by 19.74%. The flow characteristics of interlayer channels during DGP injection play a positive role in oil displacement, so the oil recovery degree in this process is greater than that in the subsequent water flooding stage under each injection volume condition. The core objective of this study is to investigate the plugging mechanism of DGPs in pan-connected interlayer channels of high-water-cut reservoirs, establish a method to quantify interlayer flow rates, and reveal how DGPs regulate flow redistribution to enhance oil recovery. Full article
(This article belongs to the Special Issue Applications of Gels for Enhanced Oil Recovery)
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12 pages, 1145 KB  
Article
Solvent Extraction of Rare-Earth Elements (REEs) from Lignite Coal In Situ
by Ian K. Feole and Bruce C. Folkedahl
Fuels 2025, 6(3), 61; https://doi.org/10.3390/fuels6030061 - 19 Aug 2025
Viewed by 649
Abstract
Plugs of lignite coal from multiple formations were subjected to a series of tests to determine the amount of rare-earth elements (REEs) to be extracted from coal in an in situ mining operation. These tests were used to determine if extraction of REEs [...] Read more.
Plugs of lignite coal from multiple formations were subjected to a series of tests to determine the amount of rare-earth elements (REEs) to be extracted from coal in an in situ mining operation. These tests were used to determine if extraction of REEs and other critical minerals in an in situ environment would be possible for future attempts as an alternative to extraction mining. The tests involved subjecting whole lignite coal plugs from the Twin Butte coal seams in North Dakota to flow-through tests of water, and concentrations of 1.0 M ammonium nitrate, 1.0 M and 1.5 M sulfuric acid, and 1.0 M and 1.5 M hydrochloric acid (HCl) solvents at different concentrations and combinations. The flow-through testing was conducted by alternating the solvent and water flow-through to simulate an in situ mining scenario. The samples were analyzed for their concentrations of REEs (lanthanum [La], cerium [Ce], praseodymium [Pr], neodymium [Nd], samarium [Sm], europium [Eu], gadolinium [Gd], terbium [Tb], dysprosium [Dy], holmium [Ho], erbium [Er], thulium [Tm], ytterbium [Yb], lutetium [Lu], yttrium [Y], and scandium [Sc], as well as germanium [Ge] and cobalt [Co], manganese [Mn], nickel [Ni], and barium [Ba]). Results from the testing showed that REEs were extracted in concentrations that were on average higher using sulfuric acid (8.9%) than with HCl (5.8%), which had a higher recovery than ammonium nitrate. Tests were performed over a standard time interval for comparison between solvents, while a second set of testing was done to determine recovery rates of REEs and critical minerals under certain static and constant flow-through times to determine extraction in relation to time. Critical minerals had a higher recovery rate than the REEs across all tests, with a slightly higher recovery of light REEs over heavy REEs. Full article
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14 pages, 2295 KB  
Article
Design of Novel Hydraulic Drive Cleaning Equipment for Well Maintenance
by Zhongrui Ji, Qi Feng, Shupei Li, Zhaoxuan Li and Yi Pan
Processes 2025, 13(8), 2424; https://doi.org/10.3390/pr13082424 - 31 Jul 2025
Viewed by 474
Abstract
Deep drilling and horizontal wells, as important means of unconventional oil and gas development, face problems with the high energy consumption but low removal efficiency of traditional well washing equipment, the uneven cleaning of horizontal well intervals, and an insufficient degree of automation. [...] Read more.
Deep drilling and horizontal wells, as important means of unconventional oil and gas development, face problems with the high energy consumption but low removal efficiency of traditional well washing equipment, the uneven cleaning of horizontal well intervals, and an insufficient degree of automation. This paper proposes a novel hydraulic drive well washing device which consists of two main units. The wellbore cleaning unit comprises a hydraulic drive cutting–flushing module, a well cleaning mode-switching module, and a filter storage module. The unit uses hydraulic and mechanical forces to perform combined cleaning to prevent mud and sand from settling. By controlling the flow direction of the well washing fluid, it can directly switch between normal and reverse washing modes in the downhole area, and at the same time, it can control the working state of corresponding modules. The assembly control unit includes the chain lifting module and the arm assembly module, which can lift and move the device through the chain structure, allow for the rapid assembly of equipment through the use of a mechanical arm, and protect the reliability of equipment through the use of a centering structure. The device converts some of the hydraulic power into mechanical force, effectively improving cleaning and plugging removal efficiency, prolonging the downhole continuous working time of equipment, reducing manual operation requirements, and comprehensively improving cleaning efficiency and energy utilization efficiency. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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Figure 1

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