Search Results (479)

Al–15Sn–5Pb (vol.%) alloy was fabricated by the Laser Powder Bed Fusion (LPBF) method at laser scanning speeds of 0.8, 1.0, and 1.2 m/s and laser powers ranging from 70 to 130 W. The samples were synthesized from a mixture of elemental powders using an ONSINT AM150 3D printer under a flowing argon atmosphere. The structure and mechanical properties under compression tests of the produced material were investigated as a function of the volumetric laser energy density (E) during LPBF. It has been established that low laser energy density during LPBF results in incomplete melting of aluminum particles and a non-uniform distribution of soft inclusions within the material. Increasing the energy density ensures a significantly more uniform distribution of the phases, resulting in the formation of a fine-grained three-phase alloy. It was established that both the ductility and strength of the alloy improve with the increase in E until a critical value is reached. As a result, at E ≥ 48 J·mm⁻³, the ultimate strength of the alloy reaches 100 ± 5 MPa, and its deformation before fracture is 15 ± 1%. Substituting one quarter of the tin volume with lead results in a significant increase in the ductility of the LPBF-fabricated aluminum alloy. Full article

This work reports the design, fabrication, and validation of a modular ergonomic saddle for rehabilitation cycling, developed through a combined additive manufacturing approach. The saddle consists of a metallic support produced by Laser Powder Bed Fusion (LPBF) in AISI 316L stainless steel and a polymeric ergonomic covering fabricated via Selective Laser Sintering (SLS) using thermoplastic polyurethane (TPU). A preliminary material screening between TPU and polypropylene (PP) was conducted, with TPU selected for its superior elastic response, energy dissipation, and more favourable SLS processability, as confirmed by thermal analyses. A series of gyroid lattice configurations with varying cell sizes and wall thicknesses were designed and mechanically tested. Cyclic testing under both stress- and displacement-controlled conditions demonstrated that the configuration with 8 mm cell size and 0.3 mm wall thickness provided the best balance between compliance and stability, showing minimal permanent deformation after 10,000 cycles and stable force response under repeated displacements. Finite Element Method (FEM) simulations, parameterized using experimentally derived elastic and density data, correlated well with the mechanical results, correlated with the mechanical results, supporting comparative stiffness evaluation. Moreover, a cost model focused on the customizable TPU component confirmed the economic viability of the modular approach, where the metallic base remains a reusable standard. Finally, the modular saddle was fabricated and successfully mounted on a cycle ergometer, demonstrating functional feasibility. Full article

This study explores the application of lattice structures as internal support architectures in the fabrication of Inconel 718 components via Laser Powder Bed Fusion (L-PBF), building upon previous research on beam-based FCCZ supports. Two representative lattice typologies were investigated: the node and beam-based FCCZ (face centered cubic with Z direction reinforcement struts) structure and the triply periodic minimal surface (TPMS) Schoen Gyroid cell. The aim was to assess how the transition from a discrete beam-node architecture to a continuous surface topology influences manufacturability, thermal stability, and mechanical performance. Finite Element Method (FEM) simulations in Ansys accurately predicted distortions and residual stresses during the L-PBF process, showing strong agreement with stereomicroscope measurements. Specifically, the maximum directional deformation reached 0.32 mm for the FCCZ sample versus 0.17 mm for the Gyroid, with corresponding peak residual stresses of 1328 MPa and 940 MPa, respectively. After fabrication, the samples underwent solution treatment and double aging according to AMS 2774 and AMS 5662 standards. Vickers microhardness increased from about 320 HV0.3 in the as-built condition to 500 HV0.3 after heat treatment (+55%), with overall porosity remaining below 1%. Microstructural analysis using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) revealed that heat treatment partially homogenized the microstructure but did not achieve complete recrystallization, leaving localized dendritic regions and undissolved Laves phases, particularly near the lattice. The precipitation of γ′ and δ phases enhanced hardness and mechanical uniformity, as confirmed by Vickers microhardness testing. Quantitatively, the Gyroid topology exhibited approximately 40% lower deformation and defect density than the FCCZ structure, confirming its superior manufacturability and thermal stability. These findings provide practical guidance for selecting lattice topologies for support architectures in L-PBF Inconel 718 components where thermal stability and shape preservation during build are critical. Full article

We report on the effect of hot isostatic pressing combined with solution and ageing treatment in different sequences on the mechanical properties of Inconel 718 specimens, which in turn have been fabricated by a hybrid additive manufacturing approach. The latter combines conventional laser powder bed fusion and in-situ high speed milling, yielding superior surface quality as being quantified by $R_{\mathrm{a}}$ about 1 μm. In a comparative study between hybrid additively manufactured parts and those built without milling, we find that, in general, any combination of heat treatment leads to a higher ultimate tensile strength and an improved endurance limit, while, however, hot isostatic pressing affects these figures of merit most. In addition, metallographic analysis reveals increased density and hardness for hot isostatic pressed parts due to precipitation hardening. These improvements of the mechanical properties are found to be even more pronounced when the printed parts are manufactured by the hybrid additive approach, i.e., for parts with improved surface conditions. Full article

The present study investigated the microstructure, processability, and mechanical strength of an AlSi9Mg-20vol.%SiC composite to assess its processing and mechanical performance during the laser powder bed fusion process. A simple laser surface remelting approach was adopted to simulate laser-based rapid solidification. The results revealed that this composite generally exhibited good laser processability, and the samples with the highest laser energy density and lowest scan speed possessed the best processability owing to the elimination of microcracks and pores. After laser processing, all the samples displayed a fine Al-Si cellular structure accompanied by in-situ formed fine needle-shaped Al₄SiC₄ particles. Increasing laser energy density considerably increased the area fraction of the Al₄SiC₄. The T5 aging treatment preserved the fine cellular structure and promoted the precipitation of a large number of Si nanoparticles and MgSi precipitates. During T6 solid solution treatment, the Si networks were broken down into coarse Si particles, disintegrating the cellular structure and reducing the strength. The T5 treatment was identified as the most suitable post-heat treatment for enhancing the microhardness and strength of the composite. Compared to conventionally laser-processed AlSi10Mg alloys, the AlSi9Mg-20vol.%SiC composite exhibited a significant increase in microhardness and yield strength. Full article

Porosity characterization in metallic alloys is a fundamental aspect of materials engineering due to its influence on mechanical and structural properties. This study presents a method based on digital image processing for detecting and analyzing porosity in the AlSi10Mg aluminum alloy, additively manufactured using laser powder bed fusion (L-PBF). X-ray computed tomography, segmentation algorithms and filtering techniques were employed to identify and quantify the porosity present in the material’s microstructure. The research demonstrates that combining numerical methods with qualitative analysis provides a comprehensive understanding of porosity characteristics. Notably, the effectiveness of the proposed image processing methods was validated by comparing the results with actual material density measurements. However, challenges such as the need for proper calibration and potential imaging artifacts affecting accuracy were identified. This study represents a significant advancement in materials engineering, offering a detailed methodology for porosity analysis in aluminum alloys that not only enhances quality control and process optimization, but also improves segmentation accuracy and facilitates the reliable detection of small and interconnected pores in complex additively manufactured geometries. Full article

Multiaxial low-cycle fatigue (MLCF) behavior of laser powder bed fused (L-PBF) Ti-6Al-4V was systematically investigated with four building direction (BD) in this paper. Proportional and non-proportional strain-controlled MLCF tests characterized cyclic softening and fracture mechanisms. L-PBF Ti-6Al-4V exhibits three-stage cyclic softening with occasional initial hardening, while non-proportional softening predominates, contrasting with conventional titanium alloys. Macro-micro characterization reveals that defect density and cleavage morphology strongly influence fatigue performance across BD. Fatigue life was predicted using analytical models (FS and KBMP) and a hybrid physics- and data-driven VAE-ANN model. While the KBMP model improves predictions over FS, both fail to fully account for BD effects. Incorporating macro-micro features, the VAE-ANN model achieves highly accurate MLCF life predictions within 10% error. These results highlight the critical roles of BD and microstructural characteristics in governing the MLCF behavior of L-PBF Ti-6Al-4V. Full article

As the most commercially developed metal additive process, laser powder bed fusion (LPBF) is vital to advancing several industry sectors, enabling high-precision part production across aerospace, biomedical, and manufacturing industries. Al 7075 alloy offers low density and high-specific strength yet faces LPBF challenges such as hot cracking and porosity due to rapid solidification, thermal gradients, and a wide freezing range. To address these challenges, this study proposes an integrated computational and experimental framework to enhance the LPBF processability of Al 7xxx alloys by compositional modification. Using the Calculation of Phase Diagram approach, printable Al 7xxx compositions were designed by adding grain refiners (V and/or Ti) and a eutectic solidification enhancer (Mg) to Al 7075 alloy to enable grain refinement and eutectic solidification. Subsequent LPBF experiments and characterization tests, such as metallography (scanning electron microscopy), energy-dispersive X-ray spectroscopy, X-ray diffraction, and X-ray micro-computed tomography, confirmed the production of refined microstructures with reduced defects. This study contributes to existing approaches for producing high-quality Al 7xxx alloy parts without significant compositional deviations using an integrated computational and experimental approach. Finally, aligning with the Materials Genome Initiative, this study contributes to the development and industrial adoption of advanced materials. Full article

Ti-6Al-4V, a popular biomedical alloy, is increasingly fabricated by additive manufacturing methods, like laser powder bed fusion (LPBF). However, rapid thermal cycling and steep temperature gradients often induce mechanical degradation, corrosion, and wear. To address these challenges, laser surface modification is explored. This study investigates the microstructure and corrosion behaviour (simulated body fluid, 37 °C) of LPBF and wrought Ti-6Al-4V after laser surface melting (LSM) treatment. LSM produced modified layers of 1250–1350 µm (LPBF) and 1530–1600 µm (wrought), with gradients from remelted dendrites to acicular martensite. Microhardness in the layers increased to 655–680 HV due to lattice expansion, crystallite refinement, and higher dislocation density. However, LSM-treated alloys showed higher corrosion rates and weaker passive films, attributed to increased surface roughness, martensite formation, residual stresses, and microstructural inhomogeneity. Aluminium silicate surface films/residues further compromised passivity. Nevertheless, both LSM-LPBF and LSM-wrought specimens displayed low corrosion current densities (10⁻⁴ mA/cm²), true passivity (10⁻³–10⁻⁴ mA/cm²), and high resistance to localised corrosion. After cyclic polarisation, rutile-rich TiO₂ surface films with aluminium silicate hydrates were observed. LSM-LPBF specimens showed slightly inferior general corrosion resistance compared to LSM-wrought counterparts, due to pronounced surface texture variations, phase/composition differences, higher microstrains and dislocation density. Full article

Ti65 high-temperature titanium alloy, known for its exceptional high-temperature mechanical properties and oxidation resistance, demonstrates considerable potential for aerospace applications. Nevertheless, conventional manufacturing techniques are often inadequate for achieving high design freedom and fabricating complex geometries. This study presents a systematic investigation into the process optimization, microstructure characterization, and mechanical performance of Ti65 alloy produced by laser powder bed fusion (LPBF). Via meticulously designed single-track, multi-track, and bulk sample experiments, the influences of laser power (P), scanning speed (V), and hatch spacing (h) on molten pool behavior, defect formation, microstructural evolution, and surface roughness were thoroughly examined. The results indicate that under optimized parameters, the specimens attain ultra-high dimensional accuracy, with a near-full density (>99.99%) and reduced surface roughness (Ra = 3.9 ± 1.3 μm). Inadequate energy input (low P or high V) led to lack-of-fusion defects, whereas excessive energy (high P or low V) resulted in keyhole porosity. Microstructural analysis revealed that the rapid solidification inherent to LPBF promotes the formation of fine acicular α′-phase (0.236–0.274 μm), while elevated laser power or reduced scanning speed facilitated the development of coarse lamellar α′-martensite (0.525–0.645 μm). Tensile tests demonstrated that samples produced under the optimized parameters exhibit high ultimate tensile strength (1489 ± 7.5 MPa), yield strength (1278 ± 5.2 MPa), and satisfactory elongation (5.7 ± 0.15%), alongside elevated microhardness (446.7 ± 1.7 HV_0.2). The optimized microstructure thereby enables the simultaneous achievement of high density and superior mechanical properties. The fundamental mechanism is attributed to precise control over volumetric energy density, which governs melt pool mode, defect generation, and solidification kinetics, thereby tailoring the resultant microstructure. This study offers valuable insights into defect suppression, microstructure control, and process optimization for LPBF-fabricated Ti65 alloy, facilitating its application in high-temperature structural components. Full article

In situ process monitoring systems (IPMSs) are rapidly gaining importance in quality assurance of laser powder bed fusion (L-PBF) parts, yet standardized methods for their objective evaluation are lacking. This study introduces a novel, system-independent assessment method for IPMSs based on a specially designed Energy Step Cube (ESC) test specimen. The ESC enables systematic variation in volumetric energy density (VED) by adjusting laser scan speed, without disclosing complete process parameters. Two industrially relevant IPMSs—PrintRite3D by Divergent and Trumpf’s integrated system—were evaluated using the ESC approach with AlSi10Mg as the test material. System performance was assessed based on sensitivity to VED changes and correlation with actual porosity, determined by metallographic analysis. Results revealed significant differences in sensitivity and effective observation windows between the systems. PrintRite3D demonstrated higher sensitivity to small VED changes, while the Trumpf system showed a broader stable observation range. The study highlights the challenges in establishing relationships between IPMS signals and resulting part properties, currently restricting their standalone use for quality assurance. This work establishes a foundation for standardized IPMS evaluation in additive manufacturing, offering valuable insights for technology advancement and enabling objective comparisons between various IPMSs, thereby promoting innovation in this field. Full article

To develop a cost-effective titanium alloy tailored for laser powder bed fusion (LPBF), a novel Ti-5.2Al-5Fe (wt.%) dual-phase alloy was designed and fabricated in this study. The composition was optimized for low density (4.4 g/cm³), high yield strength (1052 MPa), and suitable β-phase stability ([Mo]_eq = 9.3%). The alloy demonstrated excellent formability, achieving high densification (porosity ≤ 2%) and hardness (>400 HV) over a wide volumetric energy density range (48–204 J/mm³). The Al element inhibited balling by improving melt pool wettability, while the Fe element synergistically promoted densification by lowering the liquidus temperature. The as-built microstructure comprised α and β phases, with the α-phase content increasing significantly from 25.4% to 60.8% with higher energy density. While all samples exhibited high tensile strength (>1290 MPa), ductility was limited (<2.6%). EBSD analysis identified the α-phase as the primary carrier of micro-residual stress, with a high density of “zero-solution” points, low-angle grain boundaries, and KAM values. This indicates severe stress concentration from rapid solidification and phase transformation, elucidating the fundamental reason for the low ductility. This study provides systematic insights from composition design to microscopic mechanisms for designing LPBF-dedicated titanium alloys with a wide process window. Full article

The application of laser powder bed fusion (LPBF) to 7xxx-series aluminum alloys is fundamentally limited by hot cracking and porosity. This study demonstrates that adding 5 wt.% AlCoCrFeNi_2.1 high-entropy alloy (HEA) particles to 7075 aluminum alloy (AA7075) powder can effectively mitigate these issues. Microstructural characterization revealed that the HEA particles remained largely intact and formed a strong metallurgical bond with the α-Al matrix. Scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS) analysis confirmed that this bonding is facilitated via the in situ formation of new intermetallic phases at the particle/matrix interface. X-ray diffraction (XRD) identified these phases as primarily Al₅Co₂ and Fe₃Ni₂. A key consequence of this reinforced interface is a significant change in cracking behavior; optical microscopy (OM) showed that long, continuous cracks typical of AA7075 were replaced by shorter, deflected cracks in the composite. While porosity was not eliminated, the addition of HEA stabilized the process, yielding a consistent density improvement of 0.5–1.5% across the processing window. This microstructural modification resulted in a substantial ~64% increase in average microhardness, which increased from 96.41 ± 9.81 HV_0.5 to 158.46 ± 11.33 HV_0.5. These results indicate that HEA reinforcement is a promising route for engineering the microstructure and improving the LPBF processability of high-strength aluminum alloys. Full article

Laser powder bed fusion (LPBF) technology offers an effective approach for fabricating high-performance superelastic NiTi alloys. This study achieved Ni_51.9Ti_48.1 alloys with outstanding superelastic properties through a triple optimization design of the initial powder composition, printing process parameters, and post-processing. The phase transformation behavior and microstructure of the alloys were systematically investigated. The results indicate that as energy density increases, the size and quantity of pore defects in LPBF-fabricated Ni_51.9Ti_48.1 alloys increase, phase transformation temperatures rise, and hardness conversely decreases. Ni_51.9Ti_48.1 alloys produced at lower energy densities exhibit fewer dislocations. After annealing at 600 °C, Ni₄Ti₃ and R phases form internally, resulting in a maximum superelasticity of 6.64%. Conversely, Ni_51.9Ti_48.1 alloys produced at higher energy densities exhibited a large number of dislocations and formed subgrains after annealing at 600 °C. Additionally, due to the high void volume fraction, they demonstrated deteriorated superelasticity. Full article

In this study, crack-free M2 high-speed steel (HSS) was successfully fabricated by laser powder bed fusion (L-PBF) using a relatively high substrate preheating temperature of 260 °C. The influence of the resulting microstructure on the hardness and tensile properties along the build direction was thoroughly investigated. The results demonstrate that M2 HSS achieves a relative density of 99.6% when processed with a laser power of 280 W and a scanning speed of 0.8 m s⁻¹. The microstructure predominantly consists of fine martensite, along with retained austenite, lower bainite, and a small quantity of eutectic carbide. With increasing build height (from 0 to 9 mm), the fraction of lower bainite decreases from 32.1 to 13.1%, while the austenite content increases from 0.9 to 29.1%. These microstructural changes lead to a gradual reduction in the material’s strength along the build direction. Specifically, the hardness and tensile strength decrease from 845 HV_0.3 and 1520 MPa to 745 HV_0.3 and 1251 MPa, respectively. Additionally, the elongation varies between 2.6% and 3.3% across the different build heights. Full article