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Search Results (936)

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Keywords = unconfined compressive strength

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24 pages, 2660 KB  
Article
Determination of Mohr–Coulomb Failure Criterion of Cement-Treated Materials Using Mixture Design Properties
by Mario Castaneda-Lopez, Thomas Lenoir, Luc Thorel and Jean-Pierre Sanfratello
Infrastructures 2025, 10(10), 267; https://doi.org/10.3390/infrastructures10100267 - 9 Oct 2025
Abstract
The compressive, tensile, and shear strength properties of two cement-stabilized soils (CSS) treated with 2% to 4% of cement are investigated for several different curing times at several densities. The measured Mohr–Coulomb (MC) shear strength features, cohesion (c), and friction angle [...] Read more.
The compressive, tensile, and shear strength properties of two cement-stabilized soils (CSS) treated with 2% to 4% of cement are investigated for several different curing times at several densities. The measured Mohr–Coulomb (MC) shear strength features, cohesion (c), and friction angle (φ) are compared with values reported in the literature for similar materials and are subject to debate depending on the estimation methods used. In addition, an alternative geometric criterion based on indirect tensile strength (ITS) and unconfined compressive strength (UCS) is evaluated. The results show that the value of c determined using the alternative criterion is slightly higher than the value of c measured using the direct shear (DS) test. A relationship between mixture variables and c is established and validated by combining numerical and experimental approaches. The friction angle appears to be constant, independent of mixture parameters. This parameter is underestimated using the geometric approach. Full article
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28 pages, 11514 KB  
Article
Effects of Carbon–Magnesium Reactions on the Physical and Mechanical Properties of Lightweight Carbonated Stabilized Soil
by Li Shao, Wangcheng Yu, Qinglong You, Suran Wang, Xi Du, Bin He, Shichao Tao, Honghui Ding and Chao Bao
Buildings 2025, 15(19), 3571; https://doi.org/10.3390/buildings15193571 - 3 Oct 2025
Viewed by 289
Abstract
Global urbanization has led to massive generation of high-water-content waste slurry, creating serious environmental challenges. Conventional treatment methods are costly and unsustainable, while cement-based foamed lightweight soils typically exhibit low strength and limited CO2 sequestration. To address this issue, this study proposes [...] Read more.
Global urbanization has led to massive generation of high-water-content waste slurry, creating serious environmental challenges. Conventional treatment methods are costly and unsustainable, while cement-based foamed lightweight soils typically exhibit low strength and limited CO2 sequestration. To address this issue, this study proposes a novel stabilization pathway by integrating a MgO–mineral powder–carbide slag composite binder with CO2 foaming–carbonation. The approach enables simultaneous slurry lightweighting, strength enhancement, and CO2 fixation. A series of laboratory tests were conducted to evaluate flowability, density, compressive strength, and deformation characteristics of the carbonated lightweight stabilized slurry. Microstructural analyses, including SEM and XRD, were used to reveal the formation of carbonate phases and pore structures. The results showed that MgO content strongly promoted carbonation, leading to denser microstructures and higher strength, while mineral powder and carbide slag optimized workability and pore stability. Orthogonal testing indicated that a mix with 25% mineral powder, 12.5% MgO, and 7.5% carbide slag achieved the best performance, with unconfined compressive strength up to 0.48 MPa after carbonation. Compared with conventional cement- or GGBS-based foamed lightweight soils, the proposed system exhibits superior strength development, improved pore stability, and enhanced CO2 sequestration potential. These findings demonstrate the feasibility of recycling high-water-content waste slurry into value-added construction materials while contributing to carbon reduction targets. This study not only provides a sustainable solution for waste slurry management but also offers new insights into the integration of CO2 mineralization into geotechnical engineering practice. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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25 pages, 8960 KB  
Article
Analysis on Durability of Bentonite Slurry–Steel Slag Foam Concrete Under Wet–Dry Cycles
by Guosheng Xiang, Feiyang Shao, Hongri Zhang, Yunze Bai, Yuan Fang, Youjun Li, Ling Li and Yang Ming
Buildings 2025, 15(19), 3550; https://doi.org/10.3390/buildings15193550 - 2 Oct 2025
Viewed by 292
Abstract
Wet–dry cycles are a key factor aggravating the durability degradation of foam concrete. To address this issue, this study prepared bentonite slurry–steel slag foam concrete (with steel slag and cement as main raw materials, and bentonite slurry as admixture) using the physical foaming [...] Read more.
Wet–dry cycles are a key factor aggravating the durability degradation of foam concrete. To address this issue, this study prepared bentonite slurry–steel slag foam concrete (with steel slag and cement as main raw materials, and bentonite slurry as admixture) using the physical foaming method. Based on 7-day unconfined compressive strength tests with different mix proportions, the optimal mix proportion was determined as follows: mass ratio of bentonite to water 1:15, steel slag content 10%, and mass fraction of bentonite slurry 5%. Based on this optimal mix proportion, dry–wet cycle tests were carried out in both water and salt solution environments to systematically analyze the improvement effect of steel slag and bentonite slurry on the durability of foam concrete. The results show the following: steel slag can act as fine aggregate to play a skeleton role; after fully mixing with cement paste, it wraps the outer wall of foam, which not only reduces foam breakage but also inhibits the formation of large pores inside the specimen; bentonite slurry can densify the interface transition zone, improve the toughness of foam concrete, and inhibit the initiation and propagation of matrix cracks during the dry–wet cycle process; the composite addition of the two can significantly enhance the water erosion resistance and salt solution erosion resistance of foam concrete. The dry–wet cycle in the salt solution environment causes more severe erosion damage to foam concrete. The main reason is that, after chloride ions invade the cement matrix, they erode hydration products and generate expansive substances, thereby aggravating the matrix damage. Scanning Electron Microscopy (SEM) analysis shows that, whether in water environment or salt solution environment, the fractal dimension of foam concrete decreased slightly with an increasing number of wet–dry cycle times. Based on fractal theory, this study established a compressive strength–porosity prediction model and a dense concrete compressive strength–dry–wet cycle times prediction model, and both models were validated against experimental data from other researchers. The research results can provide technical support for the development of durable foam concrete in harsh environments and the high-value utilization of steel slag solid waste, and are applicable to civil engineering lightweight porous material application scenarios requiring resistance to dry–wet cycle erosion, such as wall bodies and subgrade filling. Full article
(This article belongs to the Section Building Structures)
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25 pages, 24516 KB  
Article
Strength Development and Durability of Cement-Stabilized Tropical Clay–Quarry Dust Mixtures for Pavement Construction
by Obinna Uzodimma Ubani, Esdras Ngezahayo, Charles Malachy O. Nwaiwu and Chidozie Maduabuchukwu Nwakaire
Sustainability 2025, 17(19), 8825; https://doi.org/10.3390/su17198825 - 2 Oct 2025
Viewed by 459
Abstract
Road and pavement construction require huge volumes of borrowed soils in addition to the foundation soils. Unfortunately, not all soils are suitable for construction purposes. Soil stabilization is a fundamental technique used to enhance the engineering properties of weak ground/soil to meet the [...] Read more.
Road and pavement construction require huge volumes of borrowed soils in addition to the foundation soils. Unfortunately, not all soils are suitable for construction purposes. Soil stabilization is a fundamental technique used to enhance the engineering properties of weak ground/soil to meet the demands of large infrastructure projects, such as roads. It is in this regard that this study investigates the strength development, durability, and effectiveness of cement and quarry dust as stabilizers to enhance the geotechnical properties of a weak tropical clay soil. Cement was added in the range of 0% to 10% while quarry dust was used to partially replace soil in the range of 0% to 50%. The results show significant improvements in the Atterberg limits and strength properties of the tropical clay. The liquid limit reduced from 43.2% to 25.1% while the plasticity index reduced from 17.6% to 10.2% at 50% quarry dust and 10% cement content. Similarly, the maximum dry unit weight increased from 17.4 kN/m3 to 21.3 kN/m3 while the optimum moisture content decreased from 17.1% to 12.9%. The maximum soaked CBR value was 172%, representing a 1497% enhancement over untreated soil. Also, the maximum unconfined compressive strength (UCS) reached 2566 kN/m2 at 28 days of curing, representing a 1793.73% increase when compared to the untreated soil. Cement content was found to be the predominant factor influencing strength development. The study shows that cement–quarry dust blends compacted at high energy can be adopted in sustainable road construction. Full article
(This article belongs to the Section Sustainable Materials)
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24 pages, 11795 KB  
Article
Effects of Sodium Chloride in Soil Stabilization: Improving the Behavior of Clay Deposits in Northern Cartagena, Colombia
by Jair Arrieta Baldovino, Jesús David Torres Parra and Yamid E. Nuñez de la Rosa
Sustainability 2025, 17(19), 8715; https://doi.org/10.3390/su17198715 - 28 Sep 2025
Viewed by 266
Abstract
This research evaluates the stabilization of a clay collected from the northern expansion zone of Cartagena de Indias, Colombia. Laboratory analyses, including particle size distribution, Atterberg limits, compaction, specific gravity, and XRF/XRD, classified the soil as a highly plastic clay (CH) with moderate [...] Read more.
This research evaluates the stabilization of a clay collected from the northern expansion zone of Cartagena de Indias, Colombia. Laboratory analyses, including particle size distribution, Atterberg limits, compaction, specific gravity, and XRF/XRD, classified the soil as a highly plastic clay (CH) with moderate dispersivity, as confirmed by pinhole and crumb tests. The soil was treated with 3–9% lime, with and without the addition of NaCl (0% and 2%), and tested for unconfined compressive strength (qu), small-strain stiffness (Go), and microstructural properties under curing periods of 14 and 28 days at two compaction densities. Results showed that lime significantly improved mechanical behavior, while the inclusion of NaCl further enhanced qu (up to 185%) and Go (up to 3-fold), particularly at higher lime contents and curing times. Regression models demonstrated that both qu and Go follow power-type relationships with the porosity-to-lime index, with consistent exponents (−4.75 and −5.23, respectively) and high coefficients of determination (R2 > 0.79). Normalization of the data yielded master curves with R2 values above 0.90, confirming the robustness of the porosity-to-lime framework as a predictive tool. The Go/qu ratio obtained (3737.4) falls within the range reported for cemented geomaterials, reinforcing its relevance for comparative analysis. SEM observations revealed the transition from a porous, weakly aggregated structure to a dense matrix filled with C–S–H and C–A–H gels, corroborating the macro–micro correlation. Overall, the combined use of lime and NaCl effectively converts dispersive clays into non-dispersive, mechanically improved geomaterials, providing a practical and sustainable approach for stabilizing problematic coastal soils in tropical environments. Full article
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15 pages, 3903 KB  
Article
Stabilization of Ultrafine Iron Tailings with Acrylic–Styrene Copolymer for Sustainable Geotechnical Applications
by Matheus Machado Lopes, José Wilson dos Santos Ferreira and Michéle Dal Toé Casagrande
Polymers 2025, 17(19), 2624; https://doi.org/10.3390/polym17192624 - 28 Sep 2025
Viewed by 220
Abstract
Considerable research in recent years has examined the reuse of tailings; however, the lack of particle cohesion limits their application as construction materials. Therefore, this study assessed the stabilization of ultrafine iron ore tailings using an acrylic–styrene copolymer. Geotechnical characterization and polymer dosage, [...] Read more.
Considerable research in recent years has examined the reuse of tailings; however, the lack of particle cohesion limits their application as construction materials. Therefore, this study assessed the stabilization of ultrafine iron ore tailings using an acrylic–styrene copolymer. Geotechnical characterization and polymer dosage, hydromechanical and microstructural tests were carried out, including unconfined compressive strength (UCS), permeability, scanning electron microscopy (SEM) and microtomography (μCT). The polymer effectively enhanced the mechanical behavior of the tailings, increasing the UCS from 49 kPa for untreated material to 2114 kPa and 3324 kPa for 30% and 40% polymer content, respectively. A robust power-law model (R2 ≥ 0.90), based on the porosity/volumetric polymer index (η/Pᵢᵥ), was developed to predict strength, showing that mechanical gains can be achieved by increasing either polymer content or dry density, as supported by statistical analyses. Permeability remained on the order of 10−6 cm/s regardless of polymer addition, indicating that the polymer does not fill voids but instead acts as a binding agent, as confirmed by SEM and μCT analyses. Overall, this study establishes a technically feasible and sustainable approach for tailings management, highlighting the potential of polymer stabilization to turn environmentally challenging tailings into functional geotechnical materials. Full article
(This article belongs to the Section Polymer Composites and Nanocomposites)
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23 pages, 4205 KB  
Article
The Effects of Waste Tire Materials and Aerated Concrete Additives for Innovative Soil Stabilization
by Harun Devlet and Ertuğrul Ordu
Buildings 2025, 15(19), 3488; https://doi.org/10.3390/buildings15193488 - 26 Sep 2025
Viewed by 345
Abstract
Soil stabilization is a key process in geotechnical engineering, particularly for expansive clay soils that exhibit low strength and high volume-change potential. This study examines the use of waste tire powder (WTP) and autoclaved aerated concrete powder (ACP) as sustainable soil additives to [...] Read more.
Soil stabilization is a key process in geotechnical engineering, particularly for expansive clay soils that exhibit low strength and high volume-change potential. This study examines the use of waste tire powder (WTP) and autoclaved aerated concrete powder (ACP) as sustainable soil additives to improve mechanical performance while promoting sustainable waste recycling. Clayey soils from the Çorlu/Tekirdağ region were blended with varying proportions of WTP and ACP, and their properties were evaluated through Standard Proctor compaction, unconfined compressive strength (UCS), and California bearing ratio (CBR) tests. The results showed that UCS increased from 3.7 MPa to 4.5 MPa with 5% ACP, while CBR values rose from 21.3% to 29.8% with 17% ACP addition. Incorporating 2% WTP enhanced elasticity and reduced brittleness, although higher WTP contents (4%) lowered cohesion and strength. The optimum formulation, 2% WTP + 5% ACP, produced balanced improvements in strength, stiffness, and deformation resistance. The novelty of this research lies in establishing a hybrid stabilization mechanism that combines the elastic contribution of WTP with the pozzolanic bonding of ACP. Beyond technical improvements, recycling these industrial by-products mitigates environmental pollution, reduces disposal costs, and provides economic benefits. Thus, this study advances both the scientific understanding and practical application of sustainable soil stabilization. Full article
(This article belongs to the Section Building Materials, and Repair & Renovation)
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22 pages, 11691 KB  
Article
Sustainable Integrated Approach to Waste Treatment in Automotive Industry: Solidification/Stabilization, Valorization, and Techno-Economic Assessment
by Marija Štulović, Dragana Radovanović, Zoran Anđić, Nela Vujović, Jelena Ivanović, Sanja Jevtić and Željko Kamberović
Sustainability 2025, 17(19), 8553; https://doi.org/10.3390/su17198553 - 23 Sep 2025
Viewed by 472
Abstract
An integrated approach to waste management is based on efficient and safe methods for waste prevention, recycling, and safe waste treatment. In accordance with these principles, in this study, non-hazardous aluminosilicate waste (dust and sand) was used in the solidification/stabilization (S/S) treatment of [...] Read more.
An integrated approach to waste management is based on efficient and safe methods for waste prevention, recycling, and safe waste treatment. In accordance with these principles, in this study, non-hazardous aluminosilicate waste (dust and sand) was used in the solidification/stabilization (S/S) treatment of hazardous waste (coating, emulsion, and sludge) from the automotive industry. Also, the oily component of the waste was valorized and investigated for energy recovery through co-incineration. The two S/S processes were proposed and their sustainability was assessed by utilizing all types of waste generated in the same plant, obtaining stabilized material suitable for safe disposal and oil phases for further valorization, and by techno-economic analysis. The efficiency of the S/S processes was evaluated by measuring unconfined compressive strength, hydraulic conductivity, density, and the EN 12457-4 standard leaching test of S/S products, along with XRD, SEM-EDS, and TG-DTG analyses. The possibility of using the oil phase was assessed based on its calorific value. The techno-economic assessment compared the investments, operating costs, and potential savings of both treatment scenarios. The results show that an integrated approach enables safe waste immobilization and resource recovery, contributing to environmental protection and economic benefits. Full article
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21 pages, 11856 KB  
Article
A Strategy to Optimize the Mechanical Properties and Microstructure of Loess by Nano-Modified Soil Stabilizer
by Baofeng Lei, Xingchen Zhang, Henghui Fan, Shijian Wu, Changzhi Zhao, Wenbo Ni and Changhao Liu
Materials 2025, 18(19), 4435; https://doi.org/10.3390/ma18194435 - 23 Sep 2025
Viewed by 250
Abstract
With the increasing demand for soil modification technologies in the field of civil engineering, this study employed cement-stabilized soil and MBER (Material Becoming Earth into Rock) stabilized soil as controls to investigate the modification effects of an N-MBER (nanosilica reinforced MBER) stabilizer on [...] Read more.
With the increasing demand for soil modification technologies in the field of civil engineering, this study employed cement-stabilized soil and MBER (Material Becoming Earth into Rock) stabilized soil as controls to investigate the modification effects of an N-MBER (nanosilica reinforced MBER) stabilizer on the mechanical properties and microstructure of loess. The mechanical and water stability characteristics of N-MBER-stabilized loess under varying moisture contents and compaction degrees were analyzed through unconfined compressive strength (UCS) tests, softening coefficient tests, falling-head permeability tests, and wet–dry cycle tests. Combined with scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and nuclear magnetic resonance (NMR) techniques, the underlying mechanism of the N-MBER stabilizer in loess stabilization was thoroughly revealed. The results indicate that the N-MBER stabilizer significantly enhances the UCS and softening coefficient of loess. Particularly, under conditions of 28-day curing, a moisture content of 16%, and a compaction degree of 1, the compressive strength achieves a local optimum value of 3.68 MPa. Compared to soils stabilized with MBER stabilizers and cement stabilizers, the N-MBER-stabilized loess exhibits superior water resistance and microstructural density, with a significant reduction in the proportion of pore defects. Specifically, after five wet–dry cycles at a curing age of 28 days, the strength loss rates for MBER-stabilized soil and cement-stabilized soil were 24.4% and 27.54%, respectively, while that for N-MBER-stabilized soil was 18.23%, demonstrating its enhanced water resistance. Additionally, compared to cement-stabilized soil, the N-MBER-stabilized soil exhibited a 21.63% reduction in total pore number, with a 41.64% reduction specifically in large pores. The extremely small particle size and large specific surface area of the nanomaterial enable more effective interactions with soil particles, promoting hydration reactions. The resulting ettringite (AFt) and three-dimensional networked C-S-H gel tightly interweave with soil particles, forming a stable cemented structure. Compared to traditional concrete roads, stabilized soil roads enable the utilization of locally available materials and demonstrate a significant cost advantage. This study provides theoretical support and experimental evidence for the application of nanomaterials in loess improvement engineering. Full article
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25 pages, 3707 KB  
Review
Research Review of Reaction Mechanism and Mechanical Properties of Chemically Solidified Silt
by Zhuojun Xu, Xiaolong Xie, Min He, Zhengdong Luo, Jingjing Wu, Jia Bin, Liuyiyi Yang and Benben Zhang
Buildings 2025, 15(18), 3431; https://doi.org/10.3390/buildings15183431 - 22 Sep 2025
Viewed by 394
Abstract
Dredged silt, characterized by high moisture content, low shear strength, and poor permeability, presents significant challenges for direct engineering application, leading to excessive land occupation and unsustainable resource management. To address these issues, solidification-lightweight composite technology has emerged as a promising approach to [...] Read more.
Dredged silt, characterized by high moisture content, low shear strength, and poor permeability, presents significant challenges for direct engineering application, leading to excessive land occupation and unsustainable resource management. To address these issues, solidification-lightweight composite technology has emerged as a promising approach to transform dredged silt into sustainable geo-materials. This review systematically evaluates international research progress on silt solidification, focusing on (1) the chemical reaction mechanisms of varied solidification agents, (2) the quantitative effects of key factors (e.g., agent dosage, curing time, and organic content) on the mechanical properties (unconfined compressive strength and shear strength) of treated silt, and (3) a critical discussion on technological limitations and future research directions. The findings provide insights for optimizing treatment protocols and advancing large-scale applications. Full article
(This article belongs to the Special Issue Research on Structural Analysis and Design of Civil Structures)
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22 pages, 4132 KB  
Article
Sustainable Stabilization of Clay Soil Using Lime and Oryza sativa-Waste-Derived Dried Solid Digestate
by Arunthathi Sendilvadivelu, Balaji Dhandapani, Sivapriya Vijayasimhan and Surya Prakash Pauldurai Kalaiselvi
Sustainability 2025, 17(18), 8447; https://doi.org/10.3390/su17188447 - 20 Sep 2025
Viewed by 500
Abstract
Clay-rich soils are stabilized using fly ash, cement, lime, or solid waste with chemical activators to improve strength and reduce moisture-induced settlement. This study explores the stabilization of clay using lime and dried solid digestate (DSD) derived from food waste to improve its [...] Read more.
Clay-rich soils are stabilized using fly ash, cement, lime, or solid waste with chemical activators to improve strength and reduce moisture-induced settlement. This study explores the stabilization of clay using lime and dried solid digestate (DSD) derived from food waste to improve its strength. A clay sample was treated with varying proportions of DSD (1–5%) along with 4.5% lime, by dry weight of soil. Samples were compacted at optimum moisture content and cured for periods of 0, 7, 14, and 28 days. The improvement in geotechnical behavior was assessed through Atterberg limits, unconfined compressive strength (UCS), and microscopic analyses, including X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier-transform infrared spectroscopy (FTIR). Compared with untreated clay (62.03 kPa), the results show that adding 2% DSD and lime significantly increased compressive strength (446.5 kPa) and decreased plasticity by 69%. X-ray fluorescence (XRF) analysis revealed that the lime contained 81% of high calcium oxide (CaO), which supports pozzolanic and carbonation processes, whereas DSD served as a supplementary additive. Hence, the integration of DSD in soil stabilization offers a dual benefit: enhancing geotechnical performance and promoting environmental sustainability by diverting food waste from landfills and supporting circular resource use. Full article
(This article belongs to the Special Issue Solid Waste Management and Sustainable Environmental Remediation)
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17 pages, 3162 KB  
Article
Experimental Study on Mechanical and Structural Properties of Enzyme-Induced Carbonate Precipitation Solidified Soil Under Freeze–Thaw Cycles
by Fan Yu and Weiquan Zhao
Appl. Sci. 2025, 15(18), 10226; https://doi.org/10.3390/app151810226 - 19 Sep 2025
Viewed by 290
Abstract
Enzyme-induced carbonate precipitation (EICP), an environmentally friendly geotechnical reinforcement method, is commonly adopted in water conservancy infrastructure, like reservoir bank slopes. Currently, limited studies have been performed on the mechanical and structural properties of EICP-solidified soil (ES) under freeze–thaw (F-T) cycles. In this [...] Read more.
Enzyme-induced carbonate precipitation (EICP), an environmentally friendly geotechnical reinforcement method, is commonly adopted in water conservancy infrastructure, like reservoir bank slopes. Currently, limited studies have been performed on the mechanical and structural properties of EICP-solidified soil (ES) under freeze–thaw (F-T) cycles. In this study, a series of unconfined compressive strength (UCS) tests were performed to investigate the strength degradation characteristics and failure modes of ES and untreated soil (US) under a various number of F-T cycles. The “freeze–thaw structural parameter Mσ” and “initial freeze–thaw structural parameter Mp” were established to study the structural evolution laws of ES with strain and number of F-T cycles. Finally, the effect of F-T cycles on the microscopic pore structure of soil was investigated. The results indicated that the ES exhibited good strength retention capabilities subjected to F-T cycles. After one F-T cycle, the strength loss rate of the US was as high as 69.33%, while that of the ES was only 64.69% after 15 F-T cycles. The “freeze–thaw structural parameter Mσ” and the “initial freeze–thaw structural parameter Mp” presented the enhancement degree of structural strength and stabilization of ES under F-T cycles. The Mσ with strain could be divided into three stages. The nonlinear fitting results regarding the Mp showed a negative logarithmic relationship with the number of F-T cycles. With various F-T cycles, the pore area ratio of ES increased by an average of 0.603%, lower than that of US, 1.19%. After 10 to 15 F-T cycles, the Feret diameter reduction in ES was only 0.015 μm, which was 7% of the US, verifying the macroscopic test results. In the design of the reservoir slope, Mp and Mσ can be used to evaluate the deterioration of mechanical and structural properties after freeze–thaw disturbance, and to predict the stress and deformation response. Full article
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20 pages, 4193 KB  
Article
Influence of Carboxylated Styrene–Butadiene Rubber on Gas Migration Resistance and Fluid Loss in Cement Slurries
by Guru Prasad Panda, Thotakura Vamsi Nagaraju, Gottumukkala Sri Bala and Saride Lakshmi Ganesh
ChemEngineering 2025, 9(5), 100; https://doi.org/10.3390/chemengineering9050100 - 19 Sep 2025
Viewed by 296
Abstract
The majority of downhole monitoring methods currently available for well cement projects, which are used to assess the quality of cement placement and monitor well integrity over time, are primarily qualitative in nature and rely on surface signs. Obviously, there is a need [...] Read more.
The majority of downhole monitoring methods currently available for well cement projects, which are used to assess the quality of cement placement and monitor well integrity over time, are primarily qualitative in nature and rely on surface signs. Obviously, there is a need for a practical quantitative downhole monitoring method to ensure proper cement placement and long-term performance. One potential resolution to address this enduring problem would involve enhancing the designs of the cement slurry and transforming the cement into durable downhole logging equipment, thereby facilitating real-time observation of operations. To address this issue, in this work, carboxylated styrene butadiene rubber (XSBR) polymer-treated cement was used to understand the gas migration and fluid loss mechanism. The experimental findings indicate that the electrical resistivity of polymer-treated cement is significantly influenced by applied loads and stresses. The unconfined compressive strength test with XSBR-blended cement showed a significant improvement from 22.5 MPa to 33.31 MPa when XSBR increased from 0% to 3%. Additionally, in the high pressure and high temperature (HPHT) chamber, the latex polymer used as a migration additive control, the total fluid loss is found to be about 59.2 mL under 30 min of testing. Also, to emulate the accuracy, nonlinear predictive models based on the resistivity index correlation were developed to forecast polymer-treated cement performance for all the tests performed in this study. Hence, the utilization of polymer-treated cement systems proves to be a valuable method for monitoring the placement and post-placement performance of cement, as well as for visualizing real-time operational issues associated with cementing. This will also allow operators to provide immediate solutions, saving time and operational costs. Full article
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18 pages, 2527 KB  
Article
Geotechnical Performance of Lateritic Soil Subgrades Stabilized with Agro-Industrial Waste: An Experimental Assessment and ANN-Based Predictive Modelling
by Nabanita Daimary, Devabrata Sarmah, Arup Bhattacharjee, Utpal Barman and Manob Jyoti Saikia
Geotechnics 2025, 5(3), 65; https://doi.org/10.3390/geotechnics5030065 - 15 Sep 2025
Viewed by 438
Abstract
The increasing difficulty of handling industrial and agricultural wastes has generated interest in reusing materials such as Cement Kiln Dust (CKD) and Rice Husk Ash (RHA) for sustainable soil stabilization. This study examined the enhancement of lateritic soil with the incorporation of CKD [...] Read more.
The increasing difficulty of handling industrial and agricultural wastes has generated interest in reusing materials such as Cement Kiln Dust (CKD) and Rice Husk Ash (RHA) for sustainable soil stabilization. This study examined the enhancement of lateritic soil with the incorporation of CKD (0–12%) and RHA (0–25%) by weight. An integrated experimental and Artificial Neural Network (ANN) methodology was utilized to evaluate and forecast geotechnical features. Laboratory assessments were conducted to measure Atterberg limits, Maximum Dry Density (MDD), Optimum Moisture Content (OMC), and Unconfined Compressive Strength (UCS) at 0, 7, and 28 days of curing. The results indicated significant enhancements in soil characteristics with CKD-RHA combinations. Artificial Neural Network models, including GELU, LOGSIG-3, and Leaky ReLU activation functions, accurately predicted the UCS, MDD, and OMC, achieving R2 values as high as 0.980. This work underscores the efficacy of CKD-RHA mixtures in improving soil stability and the promise of ANN models as excellent prediction instruments, fostering sustainable and economical construction methodologies. Full article
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34 pages, 15017 KB  
Article
Alkali-Activated Stabilization of Silt Soil Using Garlic Husk Ash: Mechanical, Microstructural, and Durability Performance
by Mehmet Ugur Yılmazoglu
Appl. Sci. 2025, 15(18), 9944; https://doi.org/10.3390/app15189944 - 11 Sep 2025
Viewed by 472
Abstract
This study aims to evaluate the usability of agricultural wastes such as rice husk ash (RHA) and garlic husk ash (GHA) in improving silt soils by the alkali activation method. During the stabilization process, samples prepared with binder systems containing sodium hydroxide (SH) [...] Read more.
This study aims to evaluate the usability of agricultural wastes such as rice husk ash (RHA) and garlic husk ash (GHA) in improving silt soils by the alkali activation method. During the stabilization process, samples prepared with binder systems containing sodium hydroxide (SH) and sodium silicate (SS) at different SH/SS ratios (1, 3, and 9) and additive rates (0%, 4.5%, and 9%) were cured in two different curing environments (cured at ambient temperature—AC and cured in oven at 35 °C—OC) for 7, 28, 56, and 90 days. Mechanical behavior was evaluated by unconfined compressive strength (UCS) and unconsolidated-undrained triaxial compression (UU) tests; environmental strength was analyzed by 25 and 50 cycles of freeze–thaw (F–T) tests. Microstructure development was investigated by SEM and XRD analyses, while sustainability assessment was carried out with carbon footprint (kg·CO2/kg) and carbon efficiency (CI) parameters. The findings showed that mixtures containing 9% RHA and a high SH/SS ratio provided high strength in both AC and OC environments. While using GHA alone provided limited mechanical performance, it increased the binding capacity by creating a synergistic effect when used with RHA. Oven-curing environment increased the speed of pozzolanic reactions and the development of the binder phase, resulting in denser microstructures. In addition, the RHA additive played a critical role in maintaining the resistance against freeze–thaw cycles. Carbon emission analyses revealed that SH and SS had high carbon loads, while RHA and GHA additives provided environmentally sustainable solutions with low carbon footprint and high strength. As a result, alkaline activation systems with RHA and GHA additives offer a strong alternative for sustainable soil improvement applications with high strength and environmental durability. Full article
(This article belongs to the Special Issue Emerging Technologies of Sustainable Building Materials)
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