New Nano-Crystalline Hydroxyapatite-Polycarboxy/Sulfo Betaine Hybrid Materials: Synthesis and Characterization
Abstract
:1. Introduction
2. Results
2.1. Synthesis: Effect of the Incorporation of the Polymers in the Synthesis Medium
2.2. Materials Characterization: Chemical Composition, Microstructure and Morphology
2.3. Material Characterization: Infrared and Raman Spectroscopic Analyses
2.4. In Vitro Test Using Artificial Saliva
3. Discussion
4. Materials and Methods
4.1. Synthesis of Polymer-Free and Hybrid Materials
4.2. Characterization
4.2.1. Chemical Analysis
4.2.2. Powder X-ray Diffraction Analysis
4.2.3. Differential Thermal Thermogravimetry–Mass Spectrometry Analysis (DTA-TG-MS)
4.2.4. Transmission Electron Microscopy (TEM)
4.2.5. Infrared Spectroscopy (IR)
4.2.6. Raman Spectroscopy
4.2.7. In Vitro Tests Using Artificial Saliva
5. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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Material | Ca (mmol g−1) | P (mmol g−1) | Ca/P |
---|---|---|---|
Polymer-free | 8.76 ± 0.03 | 5.38 ± 0.02 | 1.63 ± 0.02 |
Hybrid (PSB) | 4.07 ± 0.01 | 2.43 ± 0.01 | 1.67 ± 0.01 |
Hybrid (PCB) | 5.12 ± 0.02 | 2.99 ± 0.02 | 1.71 ± 0.02 |
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Díaz-Cuenca, A.; Sezanova, K.; Gergulova, R.; Rabadjieva, D.; Ruseva, K. New Nano-Crystalline Hydroxyapatite-Polycarboxy/Sulfo Betaine Hybrid Materials: Synthesis and Characterization. Molecules 2024, 29, 930. https://doi.org/10.3390/molecules29050930
Díaz-Cuenca A, Sezanova K, Gergulova R, Rabadjieva D, Ruseva K. New Nano-Crystalline Hydroxyapatite-Polycarboxy/Sulfo Betaine Hybrid Materials: Synthesis and Characterization. Molecules. 2024; 29(5):930. https://doi.org/10.3390/molecules29050930
Chicago/Turabian StyleDíaz-Cuenca, Aránzazu, Kostadinka Sezanova, Rumiana Gergulova, Diana Rabadjieva, and Konstans Ruseva. 2024. "New Nano-Crystalline Hydroxyapatite-Polycarboxy/Sulfo Betaine Hybrid Materials: Synthesis and Characterization" Molecules 29, no. 5: 930. https://doi.org/10.3390/molecules29050930